######################################## # Heteronuclear T1 relaxation values # ######################################## save_2H_R1_pyruvate_1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 2H_R1_pyruvate_1 _Heteronucl_T1_list.Entry_ID 15144 _Heteronucl_T1_list.ID 1 _Heteronucl_T1_list.Sample_condition_list_ID 1 _Heteronucl_T1_list.Sample_condition_list_label $pyruvate_sample_condition_1 _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Dz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details 'temperatures 10C' _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 'methyl 2H R1' . . . 15144 1 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 8 8 LEU HD1 H 2 15.92 00.17 . . . . . 15144 1 2 . 1 1 8 8 LEU HD2 H 2 24.69 00.38 . . . . . 15144 1 3 . 1 1 9 9 VAL HG1 H 2 40.14 00.77 . . . . . 15144 1 4 . 1 1 9 9 VAL HG2 H 2 17.62 00.36 . . . . . 15144 1 5 . 1 1 10 10 LEU HD1 H 2 28.30 00.61 . . . . . 15144 1 6 . 1 1 10 10 LEU HD2 H 2 23.46 00.30 . . . . . 15144 1 7 . 1 1 12 12 LEU HD1 H 2 16.21 00.11 . . . . . 15144 1 8 . 1 1 12 12 LEU HD2 H 2 26.37 00.19 . . . . . 15144 1 9 . 1 1 23 23 VAL HG1 H 2 45.62 00.78 . . . . . 15144 1 10 . 1 1 23 23 VAL HG2 H 2 42.88 00.92 . . . . . 15144 1 11 . 1 1 30 30 ILE HG2 H 2 18.31 00.99 . . . . . 15144 1 12 . 1 1 31 31 LEU HD1 H 2 37.12 00.53 . . . . . 15144 1 13 . 1 1 31 31 LEU HD2 H 2 19.82 00.33 . . . . . 15144 1 14 . 1 1 33 33 LEU HD1 H 2 18.05 00.38 . . . . . 15144 1 15 . 1 1 33 33 LEU HD2 H 2 19.83 00.19 . . . . . 15144 1 16 . 1 1 34 34 LEU HD1 H 2 23.11 00.23 . . . . . 15144 1 17 . 1 1 34 34 LEU HD2 H 2 25.56 00.61 . . . . . 15144 1 18 . 1 1 44 44 VAL HG1 H 2 41.91 00.58 . . . . . 15144 1 19 . 1 1 44 44 VAL HG2 H 2 32.61 00.51 . . . . . 15144 1 20 . 1 1 46 46 VAL HG1 H 2 29.76 00.26 . . . . . 15144 1 21 . 1 1 46 46 VAL HG2 H 2 27.39 00.30 . . . . . 15144 1 22 . 1 1 53 53 VAL HG1 H 2 53.14 01.39 . . . . . 15144 1 23 . 1 1 53 53 VAL HG2 H 2 51.78 00.76 . . . . . 15144 1 24 . 1 1 56 56 ALA HB H 2 28.52 01.63 . . . . . 15144 1 25 . 1 1 58 58 VAL HG1 H 2 28.80 00.20 . . . . . 15144 1 26 . 1 1 58 58 VAL HG2 H 2 31.35 00.39 . . . . . 15144 1 27 . 1 1 61 61 LEU HD1 H 2 16.65 00.22 . . . . . 15144 1 28 . 1 1 61 61 LEU HD2 H 2 19.69 00.34 . . . . . 15144 1 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_2H_R1_pyruvate_2 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 2H_R1_pyruvate_2 _Heteronucl_T1_list.Entry_ID 15144 _Heteronucl_T1_list.ID 2 _Heteronucl_T1_list.Sample_condition_list_ID 2 _Heteronucl_T1_list.Sample_condition_list_label $pyruvate_sample_condition_2 _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Dz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details 'temperatures 17C' _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 'methyl 2H R1' . . . 15144 2 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 8 8 LEU HD1 H 2 15.61 00.27 . . . . . 15144 2 2 . 1 1 8 8 LEU HD2 H 2 24.73 00.30 . . . . . 15144 2 3 . 1 1 9 9 VAL HG1 H 2 38.47 00.31 . . . . . 15144 2 4 . 1 1 9 9 VAL HG2 H 2 17.94 00.29 . . . . . 15144 2 5 . 1 1 10 10 LEU HD1 H 2 26.49 00.14 . . . . . 15144 2 6 . 1 1 10 10 LEU HD2 H 2 23.24 00.19 . . . . . 15144 2 7 . 1 1 12 12 LEU HD1 H 2 15.96 00.19 . . . . . 15144 2 8 . 1 1 12 12 LEU HD2 H 2 25.30 00.41 . . . . . 15144 2 9 . 1 1 23 23 VAL HG1 H 2 41.43 00.68 . . . . . 15144 2 10 . 1 1 23 23 VAL HG2 H 2 39.35 00.30 . . . . . 15144 2 11 . 1 1 30 30 ILE HG2 H 2 17.36 00.55 . . . . . 15144 2 12 . 1 1 31 31 LEU HD1 H 2 31.78 00.29 . . . . . 15144 2 13 . 1 1 31 31 LEU HD2 H 2 18.55 00.17 . . . . . 15144 2 14 . 1 1 33 33 LEU HD1 H 2 17.88 00.38 . . . . . 15144 2 15 . 1 1 33 33 LEU HD2 H 2 19.21 00.22 . . . . . 15144 2 16 . 1 1 34 34 LEU HD1 H 2 22.24 00.19 . . . . . 15144 2 17 . 1 1 34 34 LEU HD2 H 2 24.11 00.46 . . . . . 15144 2 18 . 1 1 44 44 VAL HG1 H 2 37.41 00.38 . . . . . 15144 2 19 . 1 1 44 44 VAL HG2 H 2 32.33 00.54 . . . . . 15144 2 20 . 1 1 46 46 VAL HG1 H 2 28.81 00.27 . . . . . 15144 2 21 . 1 1 46 46 VAL HG2 H 2 26.43 00.38 . . . . . 15144 2 22 . 1 1 53 53 VAL HG1 H 2 48.46 00.70 . . . . . 15144 2 23 . 1 1 53 53 VAL HG2 H 2 47.59 01.18 . . . . . 15144 2 24 . 1 1 56 56 ALA HB H 2 30.37 03.55 . . . . . 15144 2 25 . 1 1 58 58 VAL HG1 H 2 27.25 00.17 . . . . . 15144 2 26 . 1 1 58 58 VAL HG2 H 2 29.08 00.41 . . . . . 15144 2 27 . 1 1 61 61 LEU HD1 H 2 16.22 00.21 . . . . . 15144 2 28 . 1 1 61 61 LEU HD2 H 2 18.75 00.24 . . . . . 15144 2 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_2H_R1_pyruvate_3 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 2H_R1_pyruvate_3 _Heteronucl_T1_list.Entry_ID 15144 _Heteronucl_T1_list.ID 3 _Heteronucl_T1_list.Sample_condition_list_ID 3 _Heteronucl_T1_list.Sample_condition_list_label $pyruvate_sample_condition_3 _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Dz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details 'temperatures 24C' _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 'methyl 2H R1' . . . 15144 3 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 8 8 LEU HD1 H 2 16.41 00.24 . . . . . 15144 3 2 . 1 1 8 8 LEU HD2 H 2 22.98 00.24 . . . . . 15144 3 3 . 1 1 9 9 VAL HG1 H 2 35.52 00.62 . . . . . 15144 3 4 . 1 1 9 9 VAL HG2 H 2 18.51 00.24 . . . . . 15144 3 5 . 1 1 10 10 LEU HD1 H 2 24.78 00.27 . . . . . 15144 3 6 . 1 1 10 10 LEU HD2 H 2 22.06 00.24 . . . . . 15144 3 7 . 1 1 12 12 LEU HD1 H 2 16.12 00.17 . . . . . 15144 3 8 . 1 1 12 12 LEU HD2 H 2 24.86 00.42 . . . . . 15144 3 9 . 1 1 23 23 VAL HG1 H 2 36.68 00.39 . . . . . 15144 3 10 . 1 1 23 23 VAL HG2 H 2 34.75 00.43 . . . . . 15144 3 11 . 1 1 30 30 ILE HG2 H 2 19.20 00.57 . . . . . 15144 3 12 . 1 1 31 31 LEU HD1 H 2 27.18 00.29 . . . . . 15144 3 13 . 1 1 31 31 LEU HD2 H 2 16.76 00.11 . . . . . 15144 3 14 . 1 1 33 33 LEU HD1 H 2 18.24 00.20 . . . . . 15144 3 15 . 1 1 33 33 LEU HD2 H 2 19.90 00.44 . . . . . 15144 3 16 . 1 1 34 34 LEU HD1 H 2 20.86 00.15 . . . . . 15144 3 17 . 1 1 34 34 LEU HD2 H 2 22.70 00.34 . . . . . 15144 3 18 . 1 1 44 44 VAL HG1 H 2 34.19 00.51 . . . . . 15144 3 19 . 1 1 44 44 VAL HG2 H 2 32.48 00.62 . . . . . 15144 3 20 . 1 1 46 46 VAL HG1 H 2 27.92 00.40 . . . . . 15144 3 21 . 1 1 46 46 VAL HG2 H 2 25.57 00.42 . . . . . 15144 3 22 . 1 1 53 53 VAL HG1 H 2 45.07 00.87 . . . . . 15144 3 23 . 1 1 53 53 VAL HG2 H 2 43.43 00.44 . . . . . 15144 3 24 . 1 1 56 56 ALA HB H 2 27.72 02.25 . . . . . 15144 3 25 . 1 1 58 58 VAL HG1 H 2 26.39 00.35 . . . . . 15144 3 26 . 1 1 58 58 VAL HG2 H 2 27.28 00.32 . . . . . 15144 3 27 . 1 1 61 61 LEU HD1 H 2 16.14 00.18 . . . . . 15144 3 28 . 1 1 61 61 LEU HD2 H 2 17.89 00.20 . . . . . 15144 3 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_2H_R1_pyruvate_4 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 2H_R1_pyruvate_4 _Heteronucl_T1_list.Entry_ID 15144 _Heteronucl_T1_list.ID 4 _Heteronucl_T1_list.Sample_condition_list_ID 4 _Heteronucl_T1_list.Sample_condition_list_label $pyruvate_sample_condition_4 _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Dz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details 'temperatures 30C' _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 'methyl 2H R1' . . . 15144 4 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 8 8 LEU HD1 H 2 16.06 00.25 . . . . . 15144 4 2 . 1 1 8 8 LEU HD2 H 2 23.98 00.24 . . . . . 15144 4 3 . 1 1 9 9 VAL HG1 H 2 33.28 00.41 . . . . . 15144 4 4 . 1 1 9 9 VAL HG2 H 2 18.38 00.31 . . . . . 15144 4 5 . 1 1 10 10 LEU HD1 H 2 24.77 00.47 . . . . . 15144 4 6 . 1 1 10 10 LEU HD2 H 2 20.40 00.23 . . . . . 15144 4 7 . 1 1 12 12 LEU HD1 H 2 16.58 00.28 . . . . . 15144 4 8 . 1 1 12 12 LEU HD2 H 2 23.61 00.41 . . . . . 15144 4 9 . 1 1 23 23 VAL HG1 H 2 34.45 00.56 . . . . . 15144 4 10 . 1 1 23 23 VAL HG2 H 2 33.02 00.53 . . . . . 15144 4 11 . 1 1 30 30 ILE HG2 H 2 19.92 00.44 . . . . . 15144 4 12 . 1 1 31 31 LEU HD1 H 2 23.98 00.39 . . . . . 15144 4 13 . 1 1 31 31 LEU HD2 H 2 15.75 00.17 . . . . . 15144 4 14 . 1 1 33 33 LEU HD1 H 2 18.39 00.48 . . . . . 15144 4 15 . 1 1 33 33 LEU HD2 H 2 19.91 00.18 . . . . . 15144 4 16 . 1 1 34 34 LEU HD1 H 2 20.34 00.25 . . . . . 15144 4 17 . 1 1 34 34 LEU HD2 H 2 21.52 00.52 . . . . . 15144 4 18 . 1 1 44 44 VAL HG1 H 2 32.84 00.40 . . . . . 15144 4 19 . 1 1 44 44 VAL HG2 H 2 30.89 00.53 . . . . . 15144 4 20 . 1 1 46 46 VAL HG1 H 2 27.07 00.23 . . . . . 15144 4 21 . 1 1 46 46 VAL HG2 H 2 25.11 00.25 . . . . . 15144 4 22 . 1 1 53 53 VAL HG1 H 2 43.22 01.27 . . . . . 15144 4 23 . 1 1 53 53 VAL HG2 H 2 42.20 00.80 . . . . . 15144 4 24 . 1 1 56 56 ALA HB H 2 29.90 01.46 . . . . . 15144 4 25 . 1 1 58 58 VAL HG1 H 2 26.13 00.57 . . . . . 15144 4 26 . 1 1 58 58 VAL HG2 H 2 25.48 00.45 . . . . . 15144 4 27 . 1 1 61 61 LEU HD1 H 2 15.37 00.38 . . . . . 15144 4 28 . 1 1 61 61 LEU HD2 H 2 17.00 00.46 . . . . . 15144 4 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_2H_R1_glucose_1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 2H_R1_glucose_1 _Heteronucl_T1_list.Entry_ID 15144 _Heteronucl_T1_list.ID 5 _Heteronucl_T1_list.Sample_condition_list_ID 5 _Heteronucl_T1_list.Sample_condition_list_label $glucose_sample_condition_1 _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Dz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details 'temperatures 10C' _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 'methyl 2H R1' . . . 15144 5 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 1 1 MET HE H 2 04.24 00.13 . . . . . 15144 5 2 . 1 1 4 4 THR HG2 H 2 30.20 00.22 . . . . . 15144 5 3 . 1 1 8 8 LEU HD1 H 2 15.19 00.20 . . . . . 15144 5 4 . 1 1 8 8 LEU HD2 H 2 26.46 01.13 . . . . . 15144 5 5 . 1 1 9 9 VAL HG1 H 2 38.99 00.36 . . . . . 15144 5 6 . 1 1 9 9 VAL HG2 H 2 17.04 00.22 . . . . . 15144 5 7 . 1 1 10 10 LEU HD1 H 2 26.83 02.78 . . . . . 15144 5 8 . 1 1 10 10 LEU HD2 H 2 24.44 00.53 . . . . . 15144 5 9 . 1 1 11 11 ALA HB H 2 55.44 01.47 . . . . . 15144 5 10 . 1 1 12 12 LEU HD1 H 2 15.62 00.54 . . . . . 15144 5 11 . 1 1 12 12 LEU HD2 H 2 27.29 01.21 . . . . . 15144 5 12 . 1 1 23 23 VAL HG1 H 2 45.12 00.60 . . . . . 15144 5 13 . 1 1 23 23 VAL HG2 H 2 42.03 00.21 . . . . . 15144 5 14 . 1 1 24 24 THR HG2 H 2 39.53 00.86 . . . . . 15144 5 15 . 1 1 25 25 MET HE H 2 10.12 00.29 . . . . . 15144 5 16 . 1 1 30 30 ILE HG2 H 2 18.92 00.42 . . . . . 15144 5 17 . 1 1 30 30 ILE HD1 H 2 15.65 00.12 . . . . . 15144 5 18 . 1 1 32 32 THR HG2 H 2 35.31 00.95 . . . . . 15144 5 19 . 1 1 33 33 LEU HD1 H 2 17.21 00.25 . . . . . 15144 5 20 . 1 1 33 33 LEU HD2 H 2 20.88 00.67 . . . . . 15144 5 21 . 1 1 34 34 LEU HD1 H 2 23.28 00.46 . . . . . 15144 5 22 . 1 1 34 34 LEU HD2 H 2 25.85 01.36 . . . . . 15144 5 23 . 1 1 37 37 THR HG2 H 2 26.19 00.18 . . . . . 15144 5 24 . 1 1 44 44 VAL HG1 H 2 39.56 00.89 . . . . . 15144 5 25 . 1 1 44 44 VAL HG2 H 2 34.06 00.72 . . . . . 15144 5 26 . 1 1 46 46 VAL HG1 H 2 30.13 00.42 . . . . . 15144 5 27 . 1 1 46 46 VAL HG2 H 2 27.69 00.33 . . . . . 15144 5 28 . 1 1 53 53 VAL HG1 H 2 50.65 00.51 . . . . . 15144 5 29 . 1 1 53 53 VAL HG2 H 2 57.65 01.17 . . . . . 15144 5 30 . 1 1 55 55 ALA HB H 2 63.32 02.21 . . . . . 15144 5 31 . 1 1 56 56 ALA HB H 2 32.75 00.65 . . . . . 15144 5 32 . 1 1 58 58 VAL HG1 H 2 27.42 00.51 . . . . . 15144 5 33 . 1 1 58 58 VAL HG2 H 2 32.74 00.43 . . . . . 15144 5 34 . 1 1 61 61 LEU HD1 H 2 16.43 00.18 . . . . . 15144 5 35 . 1 1 61 61 LEU HD2 H 2 20.01 00.71 . . . . . 15144 5 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_2H_R1_glucose_2 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 2H_R1_glucose_2 _Heteronucl_T1_list.Entry_ID 15144 _Heteronucl_T1_list.ID 6 _Heteronucl_T1_list.Sample_condition_list_ID 6 _Heteronucl_T1_list.Sample_condition_list_label $glucose_sample_condition_2 _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Dz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details 'temperatures 17C' _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 3 'methyl 2H R1' . . . 15144 6 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 1 1 MET HE H 2 03.81 00.24 . . . . . 15144 6 2 . 1 1 4 4 THR HG2 H 2 27.67 00.30 . . . . . 15144 6 3 . 1 1 8 8 LEU HD1 H 2 14.62 00.50 . . . . . 15144 6 4 . 1 1 8 8 LEU HD2 H 2 23.32 00.52 . . . . . 15144 6 5 . 1 1 9 9 VAL HG1 H 2 36.00 00.66 . . . . . 15144 6 6 . 1 1 9 9 VAL HG2 H 2 17.06 00.27 . . . . . 15144 6 7 . 1 1 10 10 LEU HD1 H 2 28.68 01.60 . . . . . 15144 6 8 . 1 1 10 10 LEU HD2 H 2 21.80 00.35 . . . . . 15144 6 9 . 1 1 11 11 ALA HB H 2 49.01 00.98 . . . . . 15144 6 10 . 1 1 12 12 LEU HD1 H 2 14.91 00.53 . . . . . 15144 6 11 . 1 1 12 12 LEU HD2 H 2 24.37 01.69 . . . . . 15144 6 12 . 1 1 23 23 VAL HG1 H 2 39.60 00.61 . . . . . 15144 6 13 . 1 1 23 23 VAL HG2 H 2 38.02 00.46 . . . . . 15144 6 14 . 1 1 24 24 THR HG2 H 2 34.29 00.44 . . . . . 15144 6 15 . 1 1 25 25 MET HE H 2 11.27 00.41 . . . . . 15144 6 16 . 1 1 30 30 ILE HG2 H 2 18.48 00.35 . . . . . 15144 6 17 . 1 1 30 30 ILE HD1 H 2 15.62 00.30 . . . . . 15144 6 18 . 1 1 32 32 THR HG2 H 2 32.43 01.07 . . . . . 15144 6 19 . 1 1 33 33 LEU HD1 H 2 17.18 00.85 . . . . . 15144 6 20 . 1 1 33 33 LEU HD2 H 2 18.90 00.52 . . . . . 15144 6 21 . 1 1 34 34 LEU HD1 H 2 20.68 00.44 . . . . . 15144 6 22 . 1 1 34 34 LEU HD2 H 2 23.25 02.03 . . . . . 15144 6 23 . 1 1 37 37 THR HG2 H 2 24.88 00.55 . . . . . 15144 6 24 . 1 1 44 44 VAL HG1 H 2 36.38 00.62 . . . . . 15144 6 25 . 1 1 44 44 VAL HG2 H 2 30.93 00.60 . . . . . 15144 6 26 . 1 1 46 46 VAL HG1 H 2 27.84 00.32 . . . . . 15144 6 27 . 1 1 46 46 VAL HG2 H 2 26.41 00.44 . . . . . 15144 6 28 . 1 1 53 53 VAL HG1 H 2 47.58 00.65 . . . . . 15144 6 29 . 1 1 53 53 VAL HG2 H 2 47.72 00.54 . . . . . 15144 6 30 . 1 1 55 55 ALA HB H 2 54.11 01.06 . . . . . 15144 6 31 . 1 1 56 56 ALA HB H 2 29.90 00.28 . . . . . 15144 6 32 . 1 1 58 58 VAL HG1 H 2 26.04 00.27 . . . . . 15144 6 33 . 1 1 58 58 VAL HG2 H 2 28.68 00.51 . . . . . 15144 6 34 . 1 1 61 61 LEU HD1 H 2 16.00 00.33 . . . . . 15144 6 35 . 1 1 61 61 LEU HD2 H 2 17.85 00.45 . . . . . 15144 6 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_2H_R1_glucose_3 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 2H_R1_glucose_3 _Heteronucl_T1_list.Entry_ID 15144 _Heteronucl_T1_list.ID 7 _Heteronucl_T1_list.Sample_condition_list_ID 7 _Heteronucl_T1_list.Sample_condition_list_label $glucose_sample_condition_3 _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Dz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details 'temperatures 24C' _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 3 'methyl 2H R1' . . . 15144 7 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 1 1 MET HE H 2 03.23 00.24 . . . . . 15144 7 2 . 1 1 4 4 THR HG2 H 2 25.79 00.25 . . . . . 15144 7 3 . 1 1 8 8 LEU HD1 H 2 15.07 00.17 . . . . . 15144 7 4 . 1 1 8 8 LEU HD2 H 2 22.89 01.14 . . . . . 15144 7 5 . 1 1 9 9 VAL HG1 H 2 34.21 00.30 . . . . . 15144 7 6 . 1 1 9 9 VAL HG2 H 2 17.92 00.22 . . . . . 15144 7 7 . 1 1 10 10 LEU HD1 H 2 25.09 01.72 . . . . . 15144 7 8 . 1 1 10 10 LEU HD2 H 2 21.35 00.47 . . . . . 15144 7 9 . 1 1 11 11 ALA HB H 2 44.65 00.19 . . . . . 15144 7 10 . 1 1 12 12 LEU HD1 H 2 15.32 00.34 . . . . . 15144 7 11 . 1 1 12 12 LEU HD2 H 2 22.74 01.27 . . . . . 15144 7 12 . 1 1 23 23 VAL HG1 H 2 35.78 00.41 . . . . . 15144 7 13 . 1 1 23 23 VAL HG2 H 2 34.21 00.25 . . . . . 15144 7 14 . 1 1 24 24 THR HG2 H 2 32.54 00.47 . . . . . 15144 7 15 . 1 1 25 25 MET HE H 2 12.38 00.21 . . . . . 15144 7 16 . 1 1 30 30 ILE HG2 H 2 18.89 00.30 . . . . . 15144 7 17 . 1 1 30 30 ILE HD1 H 2 14.51 00.26 . . . . . 15144 7 18 . 1 1 32 32 THR HG2 H 2 30.46 00.90 . . . . . 15144 7 19 . 1 1 33 33 LEU HD1 H 2 16.33 00.54 . . . . . 15144 7 20 . 1 1 33 33 LEU HD2 H 2 19.34 00.34 . . . . . 15144 7 21 . 1 1 34 34 LEU HD1 H 2 20.33 00.17 . . . . . 15144 7 22 . 1 1 34 34 LEU HD2 H 2 21.16 00.94 . . . . . 15144 7 23 . 1 1 37 37 THR HG2 H 2 24.86 00.55 . . . . . 15144 7 24 . 1 1 44 44 VAL HG1 H 2 32.94 00.35 . . . . . 15144 7 25 . 1 1 44 44 VAL HG2 H 2 30.66 00.46 . . . . . 15144 7 26 . 1 1 46 46 VAL HG1 H 2 27.06 00.18 . . . . . 15144 7 27 . 1 1 46 46 VAL HG2 H 2 24.73 00.29 . . . . . 15144 7 28 . 1 1 53 53 VAL HG1 H 2 44.04 00.28 . . . . . 15144 7 29 . 1 1 53 53 VAL HG2 H 2 43.70 00.61 . . . . . 15144 7 30 . 1 1 55 55 ALA HB H 2 50.20 00.72 . . . . . 15144 7 31 . 1 1 56 56 ALA HB H 2 28.23 00.16 . . . . . 15144 7 32 . 1 1 58 58 VAL HG1 H 2 25.16 00.31 . . . . . 15144 7 33 . 1 1 58 58 VAL HG2 H 2 27.15 00.33 . . . . . 15144 7 34 . 1 1 61 61 LEU HD1 H 2 15.72 00.09 . . . . . 15144 7 35 . 1 1 61 61 LEU HD2 H 2 17.19 00.48 . . . . . 15144 7 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_2H_R1_glucose_4 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 2H_R1_glucose_4 _Heteronucl_T1_list.Entry_ID 15144 _Heteronucl_T1_list.ID 8 _Heteronucl_T1_list.Sample_condition_list_ID 8 _Heteronucl_T1_list.Sample_condition_list_label $glucose_sample_condition_4 _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Dz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details 'temperatures 30C' _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 3 'methyl 2H R1' . . . 15144 8 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 1 1 MET HE H 2 02.84 00.06 . . . . . 15144 8 2 . 1 1 4 4 THR HG2 H 2 24.32 00.12 . . . . . 15144 8 3 . 1 1 8 8 LEU HD1 H 2 15.63 00.29 . . . . . 15144 8 4 . 1 1 8 8 LEU HD2 H 2 23.60 00.53 . . . . . 15144 8 5 . 1 1 9 9 VAL HG1 H 2 32.33 00.32 . . . . . 15144 8 6 . 1 1 9 9 VAL HG2 H 2 19.07 00.09 . . . . . 15144 8 7 . 1 1 10 10 LEU HD1 H 2 23.98 01.33 . . . . . 15144 8 8 . 1 1 10 10 LEU HD2 H 2 20.27 00.35 . . . . . 15144 8 9 . 1 1 11 11 ALA HB H 2 43.73 00.31 . . . . . 15144 8 10 . 1 1 12 12 LEU HD1 H 2 15.75 00.25 . . . . . 15144 8 11 . 1 1 12 12 LEU HD2 H 2 21.98 00.66 . . . . . 15144 8 12 . 1 1 23 23 VAL HG1 H 2 33.71 00.34 . . . . . 15144 8 13 . 1 1 23 23 VAL HG2 H 2 31.87 00.20 . . . . . 15144 8 14 . 1 1 24 24 THR HG2 H 2 31.19 00.68 . . . . . 15144 8 15 . 1 1 25 25 MET HE H 2 13.30 00.11 . . . . . 15144 8 16 . 1 1 30 30 ILE HG2 H 2 19.38 00.11 . . . . . 15144 8 17 . 1 1 30 30 ILE HD1 H 2 14.10 00.09 . . . . . 15144 8 18 . 1 1 32 32 THR HG2 H 2 29.17 00.55 . . . . . 15144 8 19 . 1 1 33 33 LEU HD1 H 2 18.34 00.68 . . . . . 15144 8 20 . 1 1 33 33 LEU HD2 H 2 19.52 00.34 . . . . . 15144 8 21 . 1 1 34 34 LEU HD1 H 2 19.42 00.14 . . . . . 15144 8 22 . 1 1 34 34 LEU HD2 H 2 21.23 00.35 . . . . . 15144 8 23 . 1 1 37 37 THR HG2 H 2 24.32 00.26 . . . . . 15144 8 24 . 1 1 44 44 VAL HG1 H 2 31.88 00.48 . . . . . 15144 8 25 . 1 1 44 44 VAL HG2 H 2 29.80 00.23 . . . . . 15144 8 26 . 1 1 46 46 VAL HG1 H 2 26.53 00.23 . . . . . 15144 8 27 . 1 1 46 46 VAL HG2 H 2 24.52 00.15 . . . . . 15144 8 28 . 1 1 53 53 VAL HG1 H 2 40.96 00.22 . . . . . 15144 8 29 . 1 1 53 53 VAL HG2 H 2 42.00 00.48 . . . . . 15144 8 30 . 1 1 55 55 ALA HB H 2 47.87 00.61 . . . . . 15144 8 31 . 1 1 56 56 ALA HB H 2 27.82 00.18 . . . . . 15144 8 32 . 1 1 58 58 VAL HG1 H 2 24.41 00.25 . . . . . 15144 8 33 . 1 1 58 58 VAL HG2 H 2 25.80 00.31 . . . . . 15144 8 34 . 1 1 61 61 LEU HD1 H 2 14.70 00.17 . . . . . 15144 8 35 . 1 1 61 61 LEU HD2 H 2 15.08 00.85 . . . . . 15144 8 stop_ save_