######################################## # Heteronuclear T2 relaxation values # ######################################## save_2H_R2_pyruvate_1 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 2H_R2_pyruvate_1 _Heteronucl_T2_list.Entry_ID 15144 _Heteronucl_T2_list.ID 1 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $pyruvate_sample_condition_1 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Dx _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details 'temperatures 10C' _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 2 'methyl 2H R2' . . . 15144 1 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 8 8 LEU HD1 H 2 068.32 001.64 . . . . . . . 15144 1 2 . 1 1 8 8 LEU HD2 H 2 085.41 001.92 . . . . . . . 15144 1 3 . 1 1 9 9 VAL HG1 H 2 110.60 002.16 . . . . . . . 15144 1 4 . 1 1 9 9 VAL HG2 H 2 081.63 002.21 . . . . . . . 15144 1 5 . 1 1 10 10 LEU HD1 H 2 086.41 002.44 . . . . . . . 15144 1 6 . 1 1 10 10 LEU HD2 H 2 075.04 001.56 . . . . . . . 15144 1 7 . 1 1 12 12 LEU HD1 H 2 073.83 002.22 . . . . . . . 15144 1 8 . 1 1 12 12 LEU HD2 H 2 087.97 004.60 . . . . . . . 15144 1 9 . 1 1 23 23 VAL HG1 H 2 071.09 001.80 . . . . . . . 15144 1 10 . 1 1 23 23 VAL HG2 H 2 069.90 001.48 . . . . . . . 15144 1 11 . 1 1 30 30 ILE HG2 H 2 090.84 004.00 . . . . . . . 15144 1 12 . 1 1 31 31 LEU HD1 H 2 063.24 002.28 . . . . . . . 15144 1 13 . 1 1 31 31 LEU HD2 H 2 048.41 001.28 . . . . . . . 15144 1 14 . 1 1 33 33 LEU HD1 H 2 078.88 001.23 . . . . . . . 15144 1 15 . 1 1 33 33 LEU HD2 H 2 086.53 001.87 . . . . . . . 15144 1 16 . 1 1 34 34 LEU HD1 H 2 076.99 001.82 . . . . . . . 15144 1 17 . 1 1 34 34 LEU HD2 H 2 081.63 003.03 . . . . . . . 15144 1 18 . 1 1 44 44 VAL HG1 H 2 114.55 003.10 . . . . . . . 15144 1 19 . 1 1 44 44 VAL HG2 H 2 109.53 000.86 . . . . . . . 15144 1 20 . 1 1 46 46 VAL HG1 H 2 082.58 001.34 . . . . . . . 15144 1 21 . 1 1 46 46 VAL HG2 H 2 080.72 000.66 . . . . . . . 15144 1 22 . 1 1 53 53 VAL HG1 H 2 128.77 002.89 . . . . . . . 15144 1 23 . 1 1 53 53 VAL HG2 H 2 112.63 002.87 . . . . . . . 15144 1 24 . 1 1 56 56 ALA HB H 2 115.75 007.41 . . . . . . . 15144 1 25 . 1 1 58 58 VAL HG1 H 2 090.17 002.46 . . . . . . . 15144 1 26 . 1 1 58 58 VAL HG2 H 2 101.02 002.59 . . . . . . . 15144 1 27 . 1 1 61 61 LEU HD1 H 2 054.07 000.75 . . . . . . . 15144 1 28 . 1 1 61 61 LEU HD2 H 2 055.85 000.95 . . . . . . . 15144 1 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_2H_R2_pyruvate_2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 2H_R2_pyruvate_2 _Heteronucl_T2_list.Entry_ID 15144 _Heteronucl_T2_list.ID 2 _Heteronucl_T2_list.Sample_condition_list_ID 2 _Heteronucl_T2_list.Sample_condition_list_label $pyruvate_sample_condition_2 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Dx _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details 'temperatures 17C' _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 2 'methyl 2H R2' . . . 15144 2 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 8 8 LEU HD1 H 2 062.96 000.77 . . . . . . . 15144 2 2 . 1 1 8 8 LEU HD2 H 2 075.61 001.10 . . . . . . . 15144 2 3 . 1 1 9 9 VAL HG1 H 2 095.89 002.47 . . . . . . . 15144 2 4 . 1 1 9 9 VAL HG2 H 2 074.87 001.10 . . . . . . . 15144 2 5 . 1 1 10 10 LEU HD1 H 2 074.05 002.00 . . . . . . . 15144 2 6 . 1 1 10 10 LEU HD2 H 2 068.20 000.62 . . . . . . . 15144 2 7 . 1 1 12 12 LEU HD1 H 2 066.67 000.84 . . . . . . . 15144 2 8 . 1 1 12 12 LEU HD2 H 2 077.25 001.73 . . . . . . . 15144 2 9 . 1 1 23 23 VAL HG1 H 2 066.83 000.84 . . . . . . . 15144 2 10 . 1 1 23 23 VAL HG2 H 2 066.20 000.39 . . . . . . . 15144 2 11 . 1 1 30 30 ILE HG2 H 2 076.72 002.21 . . . . . . . 15144 2 12 . 1 1 31 31 LEU HD1 H 2 055.07 000.68 . . . . . . . 15144 2 13 . 1 1 31 31 LEU HD2 H 2 042.43 000.61 . . . . . . . 15144 2 14 . 1 1 33 33 LEU HD1 H 2 071.32 001.97 . . . . . . . 15144 2 15 . 1 1 33 33 LEU HD2 H 2 073.43 000.88 . . . . . . . 15144 2 16 . 1 1 34 34 LEU HD1 H 2 069.62 001.01 . . . . . . . 15144 2 17 . 1 1 34 34 LEU HD2 H 2 068.62 000.74 . . . . . . . 15144 2 18 . 1 1 44 44 VAL HG1 H 2 102.31 001.79 . . . . . . . 15144 2 19 . 1 1 44 44 VAL HG2 H 2 097.75 001.60 . . . . . . . 15144 2 20 . 1 1 46 46 VAL HG1 H 2 075.65 000.70 . . . . . . . 15144 2 21 . 1 1 46 46 VAL HG2 H 2 073.08 000.63 . . . . . . . 15144 2 22 . 1 1 53 53 VAL HG1 H 2 111.20 001.72 . . . . . . . 15144 2 23 . 1 1 53 53 VAL HG2 H 2 107.12 001.54 . . . . . . . 15144 2 24 . 1 1 56 56 ALA HB H 2 100.55 003.26 . . . . . . . 15144 2 25 . 1 1 58 58 VAL HG1 H 2 080.62 001.93 . . . . . . . 15144 2 26 . 1 1 58 58 VAL HG2 H 2 085.59 001.80 . . . . . . . 15144 2 27 . 1 1 61 61 LEU HD1 H 2 049.38 000.43 . . . . . . . 15144 2 28 . 1 1 61 61 LEU HD2 H 2 051.70 001.02 . . . . . . . 15144 2 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_2H_R2_pyruvate_3 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 2H_R2_pyruvate_3 _Heteronucl_T2_list.Entry_ID 15144 _Heteronucl_T2_list.ID 3 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $pyruvate_sample_condition_3 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Dx _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details 'temperatures 24C' _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 2 'methyl 2H R2' . . . 15144 3 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 8 8 LEU HD1 H 2 053.96 000.55 . . . . . . . 15144 3 2 . 1 1 8 8 LEU HD2 H 2 062.92 001.07 . . . . . . . 15144 3 3 . 1 1 9 9 VAL HG1 H 2 077.14 001.58 . . . . . . . 15144 3 4 . 1 1 9 9 VAL HG2 H 2 063.01 000.92 . . . . . . . 15144 3 5 . 1 1 10 10 LEU HD1 H 2 062.95 001.13 . . . . . . . 15144 3 6 . 1 1 10 10 LEU HD2 H 2 057.69 000.45 . . . . . . . 15144 3 7 . 1 1 12 12 LEU HD1 H 2 057.93 000.82 . . . . . . . 15144 3 8 . 1 1 12 12 LEU HD2 H 2 065.83 001.85 . . . . . . . 15144 3 9 . 1 1 23 23 VAL HG1 H 2 056.53 000.58 . . . . . . . 15144 3 10 . 1 1 23 23 VAL HG2 H 2 054.57 000.67 . . . . . . . 15144 3 11 . 1 1 30 30 ILE HG2 H 2 060.61 001.02 . . . . . . . 15144 3 12 . 1 1 31 31 LEU HD1 H 2 044.83 001.09 . . . . . . . 15144 3 13 . 1 1 31 31 LEU HD2 H 2 034.77 000.31 . . . . . . . 15144 3 14 . 1 1 33 33 LEU HD1 H 2 059.81 000.73 . . . . . . . 15144 3 15 . 1 1 33 33 LEU HD2 H 2 066.09 000.87 . . . . . . . 15144 3 16 . 1 1 34 34 LEU HD1 H 2 057.96 000.58 . . . . . . . 15144 3 17 . 1 1 34 34 LEU HD2 H 2 060.99 000.81 . . . . . . . 15144 3 18 . 1 1 44 44 VAL HG1 H 2 087.80 001.06 . . . . . . . 15144 3 19 . 1 1 44 44 VAL HG2 H 2 082.77 001.73 . . . . . . . 15144 3 20 . 1 1 46 46 VAL HG1 H 2 063.61 000.66 . . . . . . . 15144 3 21 . 1 1 46 46 VAL HG2 H 2 062.52 000.91 . . . . . . . 15144 3 22 . 1 1 53 53 VAL HG1 H 2 097.81 001.51 . . . . . . . 15144 3 23 . 1 1 53 53 VAL HG2 H 2 093.05 000.60 . . . . . . . 15144 3 24 . 1 1 56 56 ALA HB H 2 076.70 003.89 . . . . . . . 15144 3 25 . 1 1 58 58 VAL HG1 H 2 068.97 000.71 . . . . . . . 15144 3 26 . 1 1 58 58 VAL HG2 H 2 071.10 001.10 . . . . . . . 15144 3 27 . 1 1 61 61 LEU HD1 H 2 042.40 000.99 . . . . . . . 15144 3 28 . 1 1 61 61 LEU HD2 H 2 043.26 000.31 . . . . . . . 15144 3 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_2H_R2_pyruvate_4 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 2H_R2_pyruvate_4 _Heteronucl_T2_list.Entry_ID 15144 _Heteronucl_T2_list.ID 4 _Heteronucl_T2_list.Sample_condition_list_ID 4 _Heteronucl_T2_list.Sample_condition_list_label $pyruvate_sample_condition_4 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Dx _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details 'temperatures 30C' _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 2 'methyl 2H R2' . . . 15144 4 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 8 8 LEU HD1 H 2 048.34 000.72 . . . . . . . 15144 4 2 . 1 1 8 8 LEU HD2 H 2 057.58 000.88 . . . . . . . 15144 4 3 . 1 1 9 9 VAL HG1 H 2 072.11 001.16 . . . . . . . 15144 4 4 . 1 1 9 9 VAL HG2 H 2 057.48 000.82 . . . . . . . 15144 4 5 . 1 1 10 10 LEU HD1 H 2 055.36 001.75 . . . . . . . 15144 4 6 . 1 1 10 10 LEU HD2 H 2 048.23 001.18 . . . . . . . 15144 4 7 . 1 1 12 12 LEU HD1 H 2 049.71 001.41 . . . . . . . 15144 4 8 . 1 1 12 12 LEU HD2 H 2 056.35 001.13 . . . . . . . 15144 4 9 . 1 1 23 23 VAL HG1 H 2 049.69 000.85 . . . . . . . 15144 4 10 . 1 1 23 23 VAL HG2 H 2 047.81 001.23 . . . . . . . 15144 4 11 . 1 1 30 30 ILE HG2 H 2 059.45 003.12 . . . . . . . 15144 4 12 . 1 1 31 31 LEU HD1 H 2 038.44 001.00 . . . . . . . 15144 4 13 . 1 1 31 31 LEU HD2 H 2 029.84 000.64 . . . . . . . 15144 4 14 . 1 1 33 33 LEU HD1 H 2 053.47 000.98 . . . . . . . 15144 4 15 . 1 1 33 33 LEU HD2 H 2 056.90 000.96 . . . . . . . 15144 4 16 . 1 1 34 34 LEU HD1 H 2 051.00 001.26 . . . . . . . 15144 4 17 . 1 1 34 34 LEU HD2 H 2 054.11 001.34 . . . . . . . 15144 4 18 . 1 1 44 44 VAL HG1 H 2 078.96 001.60 . . . . . . . 15144 4 19 . 1 1 44 44 VAL HG2 H 2 071.54 001.34 . . . . . . . 15144 4 20 . 1 1 46 46 VAL HG1 H 2 055.87 000.69 . . . . . . . 15144 4 21 . 1 1 46 46 VAL HG2 H 2 055.91 000.24 . . . . . . . 15144 4 22 . 1 1 53 53 VAL HG1 H 2 085.63 001.99 . . . . . . . 15144 4 23 . 1 1 53 53 VAL HG2 H 2 082.14 000.55 . . . . . . . 15144 4 24 . 1 1 56 56 ALA HB H 2 070.93 007.16 . . . . . . . 15144 4 25 . 1 1 58 58 VAL HG1 H 2 060.90 001.21 . . . . . . . 15144 4 26 . 1 1 58 58 VAL HG2 H 2 063.94 000.52 . . . . . . . 15144 4 27 . 1 1 61 61 LEU HD1 H 2 037.67 001.03 . . . . . . . 15144 4 28 . 1 1 61 61 LEU HD2 H 2 037.19 001.22 . . . . . . . 15144 4 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_2H_R2_glucose_1 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 2H_R2_glucose_1 _Heteronucl_T2_list.Entry_ID 15144 _Heteronucl_T2_list.ID 5 _Heteronucl_T2_list.Sample_condition_list_ID 5 _Heteronucl_T2_list.Sample_condition_list_label $glucose_sample_condition_1 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Dx _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details 'temperatures 10C' _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 4 'methyl 2H R2' . . . 15144 5 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 1 1 MET HE H 2 002.81 001.09 . . . . . . . 15144 5 2 . 1 1 4 4 THR HG2 H 2 056.36 001.64 . . . . . . . 15144 5 3 . 1 1 8 8 LEU HD1 H 2 078.80 002.01 . . . . . . . 15144 5 4 . 1 1 8 8 LEU HD2 H 2 118.41 016.31 . . . . . . . 15144 5 5 . 1 1 9 9 VAL HG1 H 2 119.05 003.50 . . . . . . . 15144 5 6 . 1 1 9 9 VAL HG2 H 2 092.11 000.55 . . . . . . . 15144 5 7 . 1 1 10 10 LEU HD1 H 2 090.79 005.67 . . . . . . . 15144 5 8 . 1 1 10 10 LEU HD2 H 2 086.79 003.43 . . . . . . . 15144 5 9 . 1 1 11 11 ALA HB H 2 140.53 001.26 . . . . . . . 15144 5 10 . 1 1 12 12 LEU HD1 H 2 080.83 003.16 . . . . . . . 15144 5 11 . 1 1 12 12 LEU HD2 H 2 079.48 008.59 . . . . . . . 15144 5 12 . 1 1 23 23 VAL HG1 H 2 078.03 001.68 . . . . . . . 15144 5 13 . 1 1 23 23 VAL HG2 H 2 075.76 000.56 . . . . . . . 15144 5 14 . 1 1 24 24 THR HG2 H 2 131.70 005.22 . . . . . . . 15144 5 15 . 1 1 25 25 MET HE H 2 086.49 001.47 . . . . . . . 15144 5 16 . 1 1 30 30 ILE HG2 H 2 093.05 002.88 . . . . . . . 15144 5 17 . 1 1 30 30 ILE HD1 H 2 043.73 000.79 . . . . . . . 15144 5 18 . 1 1 32 32 THR HG2 H 2 101.47 001.90 . . . . . . . 15144 5 19 . 1 1 33 33 LEU HD1 H 2 087.50 004.03 . . . . . . . 15144 5 20 . 1 1 33 33 LEU HD2 H 2 086.60 004.55 . . . . . . . 15144 5 21 . 1 1 34 34 LEU HD1 H 2 084.56 001.84 . . . . . . . 15144 5 22 . 1 1 34 34 LEU HD2 H 2 069.89 005.41 . . . . . . . 15144 5 23 . 1 1 37 37 THR HG2 H 2 086.39 000.98 . . . . . . . 15144 5 24 . 1 1 44 44 VAL HG1 H 2 117.15 007.89 . . . . . . . 15144 5 25 . 1 1 44 44 VAL HG2 H 2 116.25 002.00 . . . . . . . 15144 5 26 . 1 1 46 46 VAL HG1 H 2 087.25 001.16 . . . . . . . 15144 5 27 . 1 1 46 46 VAL HG2 H 2 089.90 000.54 . . . . . . . 15144 5 28 . 1 1 53 53 VAL HG1 H 2 134.05 003.09 . . . . . . . 15144 5 29 . 1 1 53 53 VAL HG2 H 2 151.29 003.18 . . . . . . . 15144 5 30 . 1 1 55 55 ALA HB H 2 152.49 002.67 . . . . . . . 15144 5 31 . 1 1 56 56 ALA HB H 2 115.47 002.08 . . . . . . . 15144 5 32 . 1 1 58 58 VAL HG1 H 2 097.62 001.65 . . . . . . . 15144 5 33 . 1 1 58 58 VAL HG2 H 2 112.03 003.33 . . . . . . . 15144 5 34 . 1 1 61 61 LEU HD1 H 2 055.70 001.84 . . . . . . . 15144 5 35 . 1 1 61 61 LEU HD2 H 2 069.78 003.91 . . . . . . . 15144 5 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_2H_R2_glucose_2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 2H_R2_glucose_2 _Heteronucl_T2_list.Entry_ID 15144 _Heteronucl_T2_list.ID 6 _Heteronucl_T2_list.Sample_condition_list_ID 6 _Heteronucl_T2_list.Sample_condition_list_label $glucose_sample_condition_2 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Dx _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details 'temperatures 17C' _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 4 'methyl 2H R2' . . . 15144 6 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 1 1 MET HE H 2 004.12 001.69 . . . . . . . 15144 6 2 . 1 1 4 4 THR HG2 H 2 047.54 001.44 . . . . . . . 15144 6 3 . 1 1 8 8 LEU HD1 H 2 063.16 001.11 . . . . . . . 15144 6 4 . 1 1 8 8 LEU HD2 H 2 077.78 001.11 . . . . . . . 15144 6 5 . 1 1 9 9 VAL HG1 H 2 095.30 002.04 . . . . . . . 15144 6 6 . 1 1 9 9 VAL HG2 H 2 077.73 001.79 . . . . . . . 15144 6 7 . 1 1 10 10 LEU HD1 H 2 083.25 003.69 . . . . . . . 15144 6 8 . 1 1 10 10 LEU HD2 H 2 071.00 000.84 . . . . . . . 15144 6 9 . 1 1 11 11 ALA HB H 2 118.30 001.97 . . . . . . . 15144 6 10 . 1 1 12 12 LEU HD1 H 2 068.26 001.48 . . . . . . . 15144 6 11 . 1 1 12 12 LEU HD2 H 2 067.98 004.22 . . . . . . . 15144 6 12 . 1 1 23 23 VAL HG1 H 2 063.92 001.68 . . . . . . . 15144 6 13 . 1 1 23 23 VAL HG2 H 2 062.18 001.42 . . . . . . . 15144 6 14 . 1 1 24 24 THR HG2 H 2 101.86 000.89 . . . . . . . 15144 6 15 . 1 1 25 25 MET HE H 2 073.77 001.33 . . . . . . . 15144 6 16 . 1 1 30 30 ILE HG2 H 2 080.01 001.71 . . . . . . . 15144 6 17 . 1 1 30 30 ILE HD1 H 2 036.54 000.94 . . . . . . . 15144 6 18 . 1 1 32 32 THR HG2 H 2 086.82 003.75 . . . . . . . 15144 6 19 . 1 1 33 33 LEU HD1 H 2 068.77 002.17 . . . . . . . 15144 6 20 . 1 1 33 33 LEU HD2 H 2 076.60 001.77 . . . . . . . 15144 6 21 . 1 1 34 34 LEU HD1 H 2 069.48 001.25 . . . . . . . 15144 6 22 . 1 1 34 34 LEU HD2 H 2 068.77 003.24 . . . . . . . 15144 6 23 . 1 1 37 37 THR HG2 H 2 072.17 002.37 . . . . . . . 15144 6 24 . 1 1 44 44 VAL HG1 H 2 104.87 001.50 . . . . . . . 15144 6 25 . 1 1 44 44 VAL HG2 H 2 095.24 001.36 . . . . . . . 15144 6 26 . 1 1 46 46 VAL HG1 H 2 073.15 001.30 . . . . . . . 15144 6 27 . 1 1 46 46 VAL HG2 H 2 074.32 000.92 . . . . . . . 15144 6 28 . 1 1 53 53 VAL HG1 H 2 111.17 002.47 . . . . . . . 15144 6 29 . 1 1 53 53 VAL HG2 H 2 112.42 002.03 . . . . . . . 15144 6 30 . 1 1 55 55 ALA HB H 2 123.47 002.53 . . . . . . . 15144 6 31 . 1 1 56 56 ALA HB H 2 098.09 001.71 . . . . . . . 15144 6 32 . 1 1 58 58 VAL HG1 H 2 080.01 001.45 . . . . . . . 15144 6 33 . 1 1 58 58 VAL HG2 H 2 085.68 002.26 . . . . . . . 15144 6 34 . 1 1 61 61 LEU HD1 H 2 049.39 001.20 . . . . . . . 15144 6 35 . 1 1 61 61 LEU HD2 H 2 048.49 002.67 . . . . . . . 15144 6 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_2H_R2_glucose_3 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 2H_R2_glucose_3 _Heteronucl_T2_list.Entry_ID 15144 _Heteronucl_T2_list.ID 7 _Heteronucl_T2_list.Sample_condition_list_ID 7 _Heteronucl_T2_list.Sample_condition_list_label $glucose_sample_condition_3 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Dx _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details 'temperatures 24C' _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 4 'methyl 2H R2' . . . 15144 7 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 1 1 MET HE H 2 004.99 001.95 . . . . . . . 15144 7 2 . 1 1 4 4 THR HG2 H 2 040.15 001.77 . . . . . . . 15144 7 3 . 1 1 8 8 LEU HD1 H 2 056.11 000.91 . . . . . . . 15144 7 4 . 1 1 8 8 LEU HD2 H 2 071.93 001.64 . . . . . . . 15144 7 5 . 1 1 9 9 VAL HG1 H 2 083.63 001.26 . . . . . . . 15144 7 6 . 1 1 9 9 VAL HG2 H 2 068.53 001.32 . . . . . . . 15144 7 7 . 1 1 10 10 LEU HD1 H 2 070.40 003.74 . . . . . . . 15144 7 8 . 1 1 10 10 LEU HD2 H 2 058.69 001.37 . . . . . . . 15144 7 9 . 1 1 11 11 ALA HB H 2 104.20 002.15 . . . . . . . 15144 7 10 . 1 1 12 12 LEU HD1 H 2 056.77 001.14 . . . . . . . 15144 7 11 . 1 1 12 12 LEU HD2 H 2 058.09 005.94 . . . . . . . 15144 7 12 . 1 1 23 23 VAL HG1 H 2 054.32 001.40 . . . . . . . 15144 7 13 . 1 1 23 23 VAL HG2 H 2 054.00 000.80 . . . . . . . 15144 7 14 . 1 1 24 24 THR HG2 H 2 090.65 001.64 . . . . . . . 15144 7 15 . 1 1 25 25 MET HE H 2 062.98 001.46 . . . . . . . 15144 7 16 . 1 1 30 30 ILE HG2 H 2 068.45 001.34 . . . . . . . 15144 7 17 . 1 1 30 30 ILE HD1 H 2 033.49 000.60 . . . . . . . 15144 7 18 . 1 1 32 32 THR HG2 H 2 074.67 002.91 . . . . . . . 15144 7 19 . 1 1 33 33 LEU HD1 H 2 062.52 001.83 . . . . . . . 15144 7 20 . 1 1 33 33 LEU HD2 H 2 067.62 000.69 . . . . . . . 15144 7 21 . 1 1 34 34 LEU HD1 H 2 060.29 001.19 . . . . . . . 15144 7 22 . 1 1 34 34 LEU HD2 H 2 058.34 001.81 . . . . . . . 15144 7 23 . 1 1 37 37 THR HG2 H 2 062.01 001.55 . . . . . . . 15144 7 24 . 1 1 44 44 VAL HG1 H 2 090.61 001.63 . . . . . . . 15144 7 25 . 1 1 44 44 VAL HG2 H 2 082.59 001.07 . . . . . . . 15144 7 26 . 1 1 46 46 VAL HG1 H 2 065.03 001.26 . . . . . . . 15144 7 27 . 1 1 46 46 VAL HG2 H 2 063.42 001.00 . . . . . . . 15144 7 28 . 1 1 53 53 VAL HG1 H 2 098.78 001.12 . . . . . . . 15144 7 29 . 1 1 53 53 VAL HG2 H 2 095.90 001.79 . . . . . . . 15144 7 30 . 1 1 55 55 ALA HB H 2 107.78 000.91 . . . . . . . 15144 7 31 . 1 1 56 56 ALA HB H 2 083.81 001.86 . . . . . . . 15144 7 32 . 1 1 58 58 VAL HG1 H 2 069.81 001.91 . . . . . . . 15144 7 33 . 1 1 58 58 VAL HG2 H 2 077.58 000.84 . . . . . . . 15144 7 34 . 1 1 61 61 LEU HD1 H 2 043.30 001.49 . . . . . . . 15144 7 35 . 1 1 61 61 LEU HD2 H 2 041.46 003.10 . . . . . . . 15144 7 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_2H_R2_glucose_4 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 2H_R2_glucose_4 _Heteronucl_T2_list.Entry_ID 15144 _Heteronucl_T2_list.ID 8 _Heteronucl_T2_list.Sample_condition_list_ID 8 _Heteronucl_T2_list.Sample_condition_list_label $glucose_sample_condition_4 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Dx _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details 'temperatures 30C' _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 4 'methyl 2H R2' . . . 15144 8 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 1 1 MET HE H 2 004.51 001.52 . . . . . . . 15144 8 2 . 1 1 4 4 THR HG2 H 2 034.99 001.14 . . . . . . . 15144 8 3 . 1 1 8 8 LEU HD1 H 2 048.27 000.76 . . . . . . . 15144 8 4 . 1 1 8 8 LEU HD2 H 2 061.94 001.70 . . . . . . . 15144 8 5 . 1 1 9 9 VAL HG1 H 2 073.99 000.91 . . . . . . . 15144 8 6 . 1 1 9 9 VAL HG2 H 2 060.31 000.57 . . . . . . . 15144 8 7 . 1 1 10 10 LEU HD1 H 2 062.52 002.42 . . . . . . . 15144 8 8 . 1 1 10 10 LEU HD2 H 2 050.79 001.30 . . . . . . . 15144 8 9 . 1 1 11 11 ALA HB H 2 095.50 001.85 . . . . . . . 15144 8 10 . 1 1 12 12 LEU HD1 H 2 052.25 000.30 . . . . . . . 15144 8 11 . 1 1 12 12 LEU HD2 H 2 050.57 004.26 . . . . . . . 15144 8 12 . 1 1 23 23 VAL HG1 H 2 048.84 000.63 . . . . . . . 15144 8 13 . 1 1 23 23 VAL HG2 H 2 047.37 000.31 . . . . . . . 15144 8 14 . 1 1 24 24 THR HG2 H 2 080.78 000.95 . . . . . . . 15144 8 15 . 1 1 25 25 MET HE H 2 057.34 001.38 . . . . . . . 15144 8 16 . 1 1 30 30 ILE HG2 H 2 061.56 001.16 . . . . . . . 15144 8 17 . 1 1 30 30 ILE HD1 H 2 028.77 000.34 . . . . . . . 15144 8 18 . 1 1 32 32 THR HG2 H 2 067.15 002.33 . . . . . . . 15144 8 19 . 1 1 33 33 LEU HD1 H 2 054.25 002.02 . . . . . . . 15144 8 20 . 1 1 33 33 LEU HD2 H 2 059.72 000.55 . . . . . . . 15144 8 21 . 1 1 34 34 LEU HD1 H 2 053.95 000.70 . . . . . . . 15144 8 22 . 1 1 34 34 LEU HD2 H 2 052.04 002.24 . . . . . . . 15144 8 23 . 1 1 37 37 THR HG2 H 2 056.10 001.50 . . . . . . . 15144 8 24 . 1 1 44 44 VAL HG1 H 2 078.99 001.07 . . . . . . . 15144 8 25 . 1 1 44 44 VAL HG2 H 2 073.80 000.95 . . . . . . . 15144 8 26 . 1 1 46 46 VAL HG1 H 2 057.69 000.64 . . . . . . . 15144 8 27 . 1 1 46 46 VAL HG2 H 2 058.37 000.59 . . . . . . . 15144 8 28 . 1 1 53 53 VAL HG1 H 2 086.69 001.10 . . . . . . . 15144 8 29 . 1 1 53 53 VAL HG2 H 2 087.60 001.16 . . . . . . . 15144 8 30 . 1 1 55 55 ALA HB H 2 096.38 000.64 . . . . . . . 15144 8 31 . 1 1 56 56 ALA HB H 2 076.18 001.06 . . . . . . . 15144 8 32 . 1 1 58 58 VAL HG1 H 2 063.38 000.43 . . . . . . . 15144 8 33 . 1 1 58 58 VAL HG2 H 2 069.42 001.28 . . . . . . . 15144 8 34 . 1 1 61 61 LEU HD1 H 2 039.47 000.65 . . . . . . . 15144 8 35 . 1 1 61 61 LEU HD2 H 2 039.33 001.29 . . . . . . . 15144 8 stop_ save_