################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chem_shift_list_1 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chem_shift_list_1 _Assigned_chem_shift_list.Entry_ID 15936 _Assigned_chem_shift_list.ID 1 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_all _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err 0.02 _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err 0.2 _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details 'M1 is deleted in the expression system.' _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 1 '2D 1H-15N HSQC' . . . 15936 1 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 SER H H 1 8.344 0.02 . 1 . . . . 3 SER H . 15936 1 2 . 1 1 3 3 SER N N 15 115.101 0.2 . 1 . . . . 3 SER N . 15936 1 3 . 1 1 4 4 SER H H 1 8.299 0.02 . 1 . . . . 4 SER H . 15936 1 4 . 1 1 4 4 SER N N 15 116.919 0.2 . 1 . . . . 4 SER N . 15936 1 5 . 1 1 6 6 HIS H H 1 8.525 0.02 . 1 . . . . 6 HIS H . 15936 1 6 . 1 1 6 6 HIS N N 15 119.965 0.2 . 1 . . . . 6 HIS N . 15936 1 7 . 1 1 7 7 HIS H H 1 8.331 0.02 . 1 . . . . 7 HIS H . 15936 1 8 . 1 1 7 7 HIS N N 15 118.149 0.2 . 1 . . . . 7 HIS N . 15936 1 9 . 1 1 8 8 HIS H H 1 8.664 0.02 . 1 . . . . 8 HIS H . 15936 1 10 . 1 1 8 8 HIS N N 15 119.987 0.2 . 1 . . . . 8 HIS N . 15936 1 11 . 1 1 9 9 HIS H H 1 8.735 0.02 . 1 . . . . 9 HIS H . 15936 1 12 . 1 1 9 9 HIS N N 15 121.102 0.2 . 1 . . . . 9 HIS N . 15936 1 13 . 1 1 10 10 HIS H H 1 8.707 0.02 . 1 . . . . 10 HIS H . 15936 1 14 . 1 1 10 10 HIS N N 15 121.802 0.2 . 1 . . . . 10 HIS N . 15936 1 15 . 1 1 11 11 SER H H 1 8.517 0.02 . 1 . . . . 11 SER H . 15936 1 16 . 1 1 11 11 SER N N 15 118.986 0.2 . 1 . . . . 11 SER N . 15936 1 17 . 1 1 12 12 SER H H 1 8.546 0.02 . 1 . . . . 12 SER H . 15936 1 18 . 1 1 12 12 SER N N 15 118.427 0.2 . 1 . . . . 12 SER N . 15936 1 19 . 1 1 13 13 GLY H H 1 8.390 0.02 . 1 . . . . 13 GLY H . 15936 1 20 . 1 1 13 13 GLY N N 15 110.589 0.2 . 1 . . . . 13 GLY N . 15936 1 21 . 1 1 14 14 LEU H H 1 8.114 0.02 . 1 . . . . 14 LEU H . 15936 1 22 . 1 1 14 14 LEU N N 15 121.919 0.2 . 1 . . . . 14 LEU N . 15936 1 23 . 1 1 15 15 VAL H H 1 8.207 0.02 . 1 . . . . 15 VAL H . 15936 1 24 . 1 1 15 15 VAL N N 15 123.670 0.2 . 1 . . . . 15 VAL N . 15936 1 25 . 1 1 17 17 ARG H H 1 8.463 0.02 . 1 . . . . 17 ARG H . 15936 1 26 . 1 1 17 17 ARG N N 15 122.016 0.2 . 1 . . . . 17 ARG N . 15936 1 27 . 1 1 18 18 GLY H H 1 8.436 0.02 . 1 . . . . 18 GLY H . 15936 1 28 . 1 1 18 18 GLY N N 15 110.288 0.2 . 1 . . . . 18 GLY N . 15936 1 29 . 1 1 19 19 SER H H 1 8.177 0.02 . 1 . . . . 19 SER H . 15936 1 30 . 1 1 19 19 SER N N 15 115.311 0.2 . 1 . . . . 19 SER N . 15936 1 31 . 1 1 20 20 HIS H H 1 8.585 0.02 . 1 . . . . 20 HIS H . 15936 1 32 . 1 1 20 20 HIS N N 15 120.181 0.2 . 1 . . . . 20 HIS N . 15936 1 33 . 1 1 21 21 MET H H 1 8.335 0.02 . 1 . . . . 21 MET H . 15936 1 34 . 1 1 21 21 MET N N 15 121.414 0.2 . 1 . . . . 21 MET N . 15936 1 35 . 1 1 22 22 LEU H H 1 8.276 0.02 . 1 . . . . 22 LEU H . 15936 1 36 . 1 1 22 22 LEU N N 15 123.681 0.2 . 1 . . . . 22 LEU N . 15936 1 37 . 1 1 23 23 GLU H H 1 8.275 0.02 . 1 . . . . 23 GLU H . 15936 1 38 . 1 1 23 23 GLU N N 15 121.658 0.2 . 1 . . . . 23 GLU N . 15936 1 39 . 1 1 24 24 LEU H H 1 8.233 0.02 . 1 . . . . 24 LEU H . 15936 1 40 . 1 1 24 24 LEU N N 15 125.128 0.2 . 1 . . . . 24 LEU N . 15936 1 41 . 1 1 26 26 LEU H H 1 8.300 0.02 . 1 . . . . 26 LEU H . 15936 1 42 . 1 1 26 26 LEU N N 15 122.215 0.2 . 1 . . . . 26 LEU N . 15936 1 43 . 1 1 27 27 ASP H H 1 8.435 0.02 . 1 . . . . 27 ASP H . 15936 1 44 . 1 1 27 27 ASP N N 15 119.531 0.2 . 1 . . . . 27 ASP N . 15936 1 45 . 1 1 28 28 SER H H 1 8.225 0.02 . 1 . . . . 28 SER H . 15936 1 46 . 1 1 28 28 SER N N 15 116.466 0.2 . 1 . . . . 28 SER N . 15936 1 47 . 1 1 29 29 ALA H H 1 8.294 0.02 . 1 . . . . 29 ALA H . 15936 1 48 . 1 1 29 29 ALA N N 15 125.498 0.2 . 1 . . . . 29 ALA N . 15936 1 49 . 1 1 30 30 THR H H 1 8.087 0.02 . 1 . . . . 30 THR H . 15936 1 50 . 1 1 30 30 THR N N 15 112.660 0.2 . 1 . . . . 30 THR N . 15936 1 51 . 1 1 31 31 THR H H 1 8.062 0.02 . 1 . . . . 31 THR H . 15936 1 52 . 1 1 31 31 THR N N 15 116.061 0.2 . 1 . . . . 31 THR N . 15936 1 53 . 1 1 32 32 GLU H H 1 8.313 0.02 . 1 . . . . 32 GLU H . 15936 1 54 . 1 1 32 32 GLU N N 15 122.186 0.2 . 1 . . . . 32 GLU N . 15936 1 55 . 1 1 33 33 SER H H 1 8.253 0.02 . 1 . . . . 33 SER H . 15936 1 56 . 1 1 33 33 SER N N 15 116.639 0.2 . 1 . . . . 33 SER N . 15936 1 57 . 1 1 34 34 LEU H H 1 8.124 0.02 . 1 . . . . 34 LEU H . 15936 1 58 . 1 1 34 34 LEU N N 15 123.829 0.2 . 1 . . . . 34 LEU N . 15936 1 59 . 1 1 35 35 ARG H H 1 8.067 0.02 . 1 . . . . 35 ARG H . 15936 1 60 . 1 1 35 35 ARG N N 15 121.114 0.2 . 1 . . . . 35 ARG N . 15936 1 61 . 1 1 36 36 ALA H H 1 8.130 0.02 . 1 . . . . 36 ALA H . 15936 1 62 . 1 1 36 36 ALA N N 15 124.466 0.2 . 1 . . . . 36 ALA N . 15936 1 63 . 1 1 37 37 ALA H H 1 8.170 0.02 . 1 . . . . 37 ALA H . 15936 1 64 . 1 1 37 37 ALA N N 15 122.806 0.2 . 1 . . . . 37 ALA N . 15936 1 65 . 1 1 38 38 THR H H 1 7.958 0.02 . 1 . . . . 38 THR H . 15936 1 66 . 1 1 38 38 THR N N 15 112.339 0.2 . 1 . . . . 38 THR N . 15936 1 67 . 1 1 39 39 HIS H H 1 8.416 0.02 . 1 . . . . 39 HIS H . 15936 1 68 . 1 1 39 39 HIS N N 15 119.940 0.2 . 1 . . . . 39 HIS N . 15936 1 69 . 1 1 40 40 ASP H H 1 8.473 0.02 . 1 . . . . 40 ASP H . 15936 1 70 . 1 1 40 40 ASP N N 15 120.536 0.2 . 1 . . . . 40 ASP N . 15936 1 71 . 1 1 41 41 VAL H H 1 8.150 0.02 . 1 . . . . 41 VAL H . 15936 1 72 . 1 1 41 41 VAL N N 15 121.179 0.2 . 1 . . . . 41 VAL N . 15936 1 73 . 1 1 42 42 LEU H H 1 8.189 0.02 . 1 . . . . 42 LEU H . 15936 1 74 . 1 1 42 42 LEU N N 15 124.627 0.2 . 1 . . . . 42 LEU N . 15936 1 75 . 1 1 43 43 ALA H H 1 8.084 0.02 . 1 . . . . 43 ALA H . 15936 1 76 . 1 1 43 43 ALA N N 15 124.263 0.2 . 1 . . . . 43 ALA N . 15936 1 77 . 1 1 44 44 GLY H H 1 8.263 0.02 . 1 . . . . 44 GLY H . 15936 1 78 . 1 1 44 44 GLY N N 15 107.590 0.2 . 1 . . . . 44 GLY N . 15936 1 79 . 1 1 45 45 LEU H H 1 7.972 0.02 . 1 . . . . 45 LEU H . 15936 1 80 . 1 1 45 45 LEU N N 15 121.590 0.2 . 1 . . . . 45 LEU N . 15936 1 81 . 1 1 46 46 THR H H 1 8.028 0.02 . 1 . . . . 46 THR H . 15936 1 82 . 1 1 46 46 THR N N 15 113.796 0.2 . 1 . . . . 46 THR N . 15936 1 83 . 1 1 47 47 ALA H H 1 8.335 0.02 . 1 . . . . 47 ALA H . 15936 1 84 . 1 1 47 47 ALA N N 15 124.969 0.2 . 1 . . . . 47 ALA N . 15936 1 85 . 1 1 48 48 ARG H H 1 8.186 0.02 . 1 . . . . 48 ARG H . 15936 1 86 . 1 1 48 48 ARG N N 15 118.707 0.2 . 1 . . . . 48 ARG N . 15936 1 87 . 1 1 49 49 GLU H H 1 7.996 0.02 . 1 . . . . 49 GLU H . 15936 1 88 . 1 1 49 49 GLU N N 15 119.675 0.2 . 1 . . . . 49 GLU N . 15936 1 89 . 1 1 50 50 ALA H H 1 8.305 0.02 . 1 . . . . 50 ALA H . 15936 1 90 . 1 1 50 50 ALA N N 15 123.422 0.2 . 1 . . . . 50 ALA N . 15936 1 91 . 1 1 51 51 LYS H H 1 7.966 0.02 . 1 . . . . 51 LYS H . 15936 1 92 . 1 1 51 51 LYS N N 15 119.335 0.2 . 1 . . . . 51 LYS N . 15936 1 93 . 1 1 52 52 VAL H H 1 7.843 0.02 . 1 . . . . 52 VAL H . 15936 1 94 . 1 1 52 52 VAL N N 15 120.180 0.2 . 1 . . . . 52 VAL N . 15936 1 95 . 1 1 53 53 LEU H H 1 8.087 0.02 . 1 . . . . 53 LEU H . 15936 1 96 . 1 1 53 53 LEU N N 15 123.565 0.2 . 1 . . . . 53 LEU N . 15936 1 97 . 1 1 54 54 ARG H H 1 8.112 0.02 . 1 . . . . 54 ARG H . 15936 1 98 . 1 1 54 54 ARG N N 15 119.763 0.2 . 1 . . . . 54 ARG N . 15936 1 99 . 1 1 55 55 MET H H 1 8.135 0.02 . 1 . . . . 55 MET H . 15936 1 100 . 1 1 55 55 MET N N 15 120.668 0.2 . 1 . . . . 55 MET N . 15936 1 101 . 1 1 56 56 ARG H H 1 8.057 0.02 . 1 . . . . 56 ARG H . 15936 1 102 . 1 1 56 56 ARG N N 15 120.992 0.2 . 1 . . . . 56 ARG N . 15936 1 103 . 1 1 57 57 PHE H H 1 8.155 0.02 . 1 . . . . 57 PHE H . 15936 1 104 . 1 1 57 57 PHE N N 15 120.164 0.2 . 1 . . . . 57 PHE N . 15936 1 105 . 1 1 58 58 GLY H H 1 8.167 0.02 . 1 . . . . 58 GLY H . 15936 1 106 . 1 1 58 58 GLY N N 15 110.014 0.2 . 1 . . . . 58 GLY N . 15936 1 107 . 1 1 59 59 ILE H H 1 7.882 0.02 . 1 . . . . 59 ILE H . 15936 1 108 . 1 1 59 59 ILE N N 15 119.212 0.2 . 1 . . . . 59 ILE N . 15936 1 109 . 1 1 60 60 ASP H H 1 8.517 0.02 . 1 . . . . 60 ASP H . 15936 1 110 . 1 1 60 60 ASP N N 15 122.096 0.2 . 1 . . . . 60 ASP N . 15936 1 111 . 1 1 61 61 MET H H 1 8.297 0.02 . 1 . . . . 61 MET H . 15936 1 112 . 1 1 61 61 MET N N 15 120.867 0.2 . 1 . . . . 61 MET N . 15936 1 113 . 1 1 62 62 ASN H H 1 8.346 0.02 . 1 . . . . 62 ASN H . 15936 1 114 . 1 1 62 62 ASN N N 15 119.127 0.2 . 1 . . . . 62 ASN N . 15936 1 115 . 1 1 63 63 THR H H 1 8.015 0.02 . 1 . . . . 63 THR H . 15936 1 116 . 1 1 63 63 THR N N 15 113.901 0.2 . 1 . . . . 63 THR N . 15936 1 117 . 1 1 64 64 ASP H H 1 8.336 0.02 . 1 . . . . 64 ASP H . 15936 1 118 . 1 1 64 64 ASP N N 15 120.850 0.2 . 1 . . . . 64 ASP N . 15936 1 119 . 1 1 65 65 TYR H H 1 8.033 0.02 . 1 . . . . 65 TYR H . 15936 1 120 . 1 1 65 65 TYR N N 15 120.864 0.2 . 1 . . . . 65 TYR N . 15936 1 121 . 1 1 66 66 THR H H 1 7.955 0.02 . 1 . . . . 66 THR H . 15936 1 122 . 1 1 66 66 THR N N 15 114.903 0.2 . 1 . . . . 66 THR N . 15936 1 123 . 1 1 67 67 LEU H H 1 8.008 0.02 . 1 . . . . 67 LEU H . 15936 1 124 . 1 1 67 67 LEU N N 15 123.081 0.2 . 1 . . . . 67 LEU N . 15936 1 125 . 1 1 68 68 GLU H H 1 8.108 0.02 . 1 . . . . 68 GLU H . 15936 1 126 . 1 1 68 68 GLU N N 15 120.412 0.2 . 1 . . . . 68 GLU N . 15936 1 127 . 1 1 69 69 GLU H H 1 8.125 0.02 . 1 . . . . 69 GLU H . 15936 1 128 . 1 1 69 69 GLU N N 15 120.533 0.2 . 1 . . . . 69 GLU N . 15936 1 129 . 1 1 70 70 VAL H H 1 8.024 0.02 . 1 . . . . 70 VAL H . 15936 1 130 . 1 1 70 70 VAL N N 15 120.367 0.2 . 1 . . . . 70 VAL N . 15936 1 131 . 1 1 71 71 GLY H H 1 8.379 0.02 . 1 . . . . 71 GLY H . 15936 1 132 . 1 1 71 71 GLY N N 15 111.499 0.2 . 1 . . . . 71 GLY N . 15936 1 133 . 1 1 72 72 LYS H H 1 8.105 0.02 . 1 . . . . 72 LYS H . 15936 1 134 . 1 1 72 72 LYS N N 15 120.799 0.2 . 1 . . . . 72 LYS N . 15936 1 135 . 1 1 73 73 GLN H H 1 8.332 0.02 . 1 . . . . 73 GLN H . 15936 1 136 . 1 1 73 73 GLN N N 15 119.990 0.2 . 1 . . . . 73 GLN N . 15936 1 137 . 1 1 75 75 ASP H H 1 8.268 0.02 . 1 . . . . 75 ASP H . 15936 1 138 . 1 1 75 75 ASP N N 15 120.654 0.2 . 1 . . . . 75 ASP N . 15936 1 139 . 1 1 76 76 VAL H H 1 8.089 0.02 . 1 . . . . 76 VAL H . 15936 1 140 . 1 1 76 76 VAL N N 15 120.663 0.2 . 1 . . . . 76 VAL N . 15936 1 141 . 1 1 77 77 THR H H 1 8.093 0.02 . 1 . . . . 77 THR H . 15936 1 142 . 1 1 77 77 THR N N 15 117.041 0.2 . 1 . . . . 77 THR N . 15936 1 143 . 1 1 78 78 ARG H H 1 8.144 0.02 . 1 . . . . 78 ARG H . 15936 1 144 . 1 1 78 78 ARG N N 15 122.155 0.2 . 1 . . . . 78 ARG N . 15936 1 145 . 1 1 79 79 GLU H H 1 8.138 0.02 . 1 . . . . 79 GLU H . 15936 1 146 . 1 1 79 79 GLU N N 15 119.545 0.2 . 1 . . . . 79 GLU N . 15936 1 147 . 1 1 80 80 ARG H H 1 8.228 0.02 . 1 . . . . 80 ARG H . 15936 1 148 . 1 1 80 80 ARG N N 15 121.609 0.2 . 1 . . . . 80 ARG N . 15936 1 149 . 1 1 81 81 ILE H H 1 8.039 0.02 . 1 . . . . 81 ILE H . 15936 1 150 . 1 1 81 81 ILE N N 15 121.221 0.2 . 1 . . . . 81 ILE N . 15936 1 151 . 1 1 82 82 ARG H H 1 8.219 0.02 . 1 . . . . 82 ARG H . 15936 1 152 . 1 1 82 82 ARG N N 15 123.581 0.2 . 1 . . . . 82 ARG N . 15936 1 153 . 1 1 83 83 GLN H H 1 8.242 0.02 . 1 . . . . 83 GLN H . 15936 1 154 . 1 1 83 83 GLN N N 15 121.261 0.2 . 1 . . . . 83 GLN N . 15936 1 155 . 1 1 84 84 ILE H H 1 8.191 0.02 . 1 . . . . 84 ILE H . 15936 1 156 . 1 1 84 84 ILE N N 15 122.410 0.2 . 1 . . . . 84 ILE N . 15936 1 157 . 1 1 85 85 GLU H H 1 8.359 0.02 . 1 . . . . 85 GLU H . 15936 1 158 . 1 1 85 85 GLU N N 15 123.227 0.2 . 1 . . . . 85 GLU N . 15936 1 159 . 1 1 86 86 ALA H H 1 8.236 0.02 . 1 . . . . 86 ALA H . 15936 1 160 . 1 1 86 86 ALA N N 15 124.542 0.2 . 1 . . . . 86 ALA N . 15936 1 161 . 1 1 87 87 LYS H H 1 8.085 0.02 . 1 . . . . 87 LYS H . 15936 1 162 . 1 1 87 87 LYS N N 15 119.727 0.2 . 1 . . . . 87 LYS N . 15936 1 163 . 1 1 88 88 ALA H H 1 8.048 0.02 . 1 . . . . 88 ALA H . 15936 1 164 . 1 1 88 88 ALA N N 15 123.804 0.2 . 1 . . . . 88 ALA N . 15936 1 165 . 1 1 89 89 LEU H H 1 8.014 0.02 . 1 . . . . 89 LEU H . 15936 1 166 . 1 1 89 89 LEU N N 15 120.962 0.2 . 1 . . . . 89 LEU N . 15936 1 167 . 1 1 90 90 ARG H H 1 8.134 0.02 . 1 . . . . 90 ARG H . 15936 1 168 . 1 1 90 90 ARG N N 15 121.068 0.2 . 1 . . . . 90 ARG N . 15936 1 169 . 1 1 91 91 LYS H H 1 8.109 0.02 . 1 . . . . 91 LYS H . 15936 1 170 . 1 1 91 91 LYS N N 15 121.824 0.2 . 1 . . . . 91 LYS N . 15936 1 171 . 1 1 92 92 LEU H H 1 8.079 0.02 . 1 . . . . 92 LEU H . 15936 1 172 . 1 1 92 92 LEU N N 15 123.110 0.2 . 1 . . . . 92 LEU N . 15936 1 173 . 1 1 93 93 ARG H H 1 8.247 0.02 . 1 . . . . 93 ARG H . 15936 1 174 . 1 1 93 93 ARG N N 15 121.376 0.2 . 1 . . . . 93 ARG N . 15936 1 175 . 1 1 94 94 HIS H H 1 8.485 0.02 . 1 . . . . 94 HIS H . 15936 1 176 . 1 1 94 94 HIS N N 15 119.819 0.2 . 1 . . . . 94 HIS N . 15936 1 177 . 1 1 96 96 SER H H 1 8.489 0.02 . 1 . . . . 96 SER H . 15936 1 178 . 1 1 96 96 SER N N 15 116.972 0.2 . 1 . . . . 96 SER N . 15936 1 179 . 1 1 97 97 ARG H H 1 8.492 0.02 . 1 . . . . 97 ARG H . 15936 1 180 . 1 1 97 97 ARG N N 15 122.927 0.2 . 1 . . . . 97 ARG N . 15936 1 181 . 1 1 98 98 SER H H 1 8.331 0.02 . 1 . . . . 98 SER H . 15936 1 182 . 1 1 98 98 SER N N 15 116.347 0.2 . 1 . . . . 98 SER N . 15936 1 183 . 1 1 99 99 GLU H H 1 8.277 0.02 . 1 . . . . 99 GLU H . 15936 1 184 . 1 1 99 99 GLU N N 15 122.440 0.2 . 1 . . . . 99 GLU N . 15936 1 185 . 1 1 100 100 VAL H H 1 8.094 0.02 . 1 . . . . 100 VAL H . 15936 1 186 . 1 1 100 100 VAL N N 15 121.335 0.2 . 1 . . . . 100 VAL N . 15936 1 187 . 1 1 101 101 LEU H H 1 8.226 0.02 . 1 . . . . 101 LEU H . 15936 1 188 . 1 1 101 101 LEU N N 15 125.552 0.2 . 1 . . . . 101 LEU N . 15936 1 189 . 1 1 102 102 ARG H H 1 8.216 0.02 . 1 . . . . 102 ARG H . 15936 1 190 . 1 1 102 102 ARG N N 15 121.662 0.2 . 1 . . . . 102 ARG N . 15936 1 191 . 1 1 103 103 SER H H 1 8.121 0.02 . 1 . . . . 103 SER H . 15936 1 192 . 1 1 103 103 SER N N 15 116.149 0.2 . 1 . . . . 103 SER N . 15936 1 193 . 1 1 104 104 PHE H H 1 8.149 0.02 . 1 . . . . 104 PHE H . 15936 1 194 . 1 1 104 104 PHE N N 15 121.755 0.2 . 1 . . . . 104 PHE N . 15936 1 195 . 1 1 105 105 LEU H H 1 7.996 0.02 . 1 . . . . 105 LEU H . 15936 1 196 . 1 1 105 105 LEU N N 15 122.220 0.2 . 1 . . . . 105 LEU N . 15936 1 197 . 1 1 106 106 ASP H H 1 8.238 0.02 . 1 . . . . 106 ASP H . 15936 1 198 . 1 1 106 106 ASP N N 15 119.143 0.2 . 1 . . . . 106 ASP N . 15936 1 199 . 1 1 107 107 ASP H H 1 7.931 0.02 . 1 . . . . 107 ASP H . 15936 1 200 . 1 1 107 107 ASP N N 15 122.619 0.2 . 1 . . . . 107 ASP N . 15936 1 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chem_shift_list_2 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chem_shift_list_2 _Assigned_chem_shift_list.Entry_ID 15936 _Assigned_chem_shift_list.ID 2 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_all _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err 0.02 _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err 0.2 _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details 'M1 is deleted in the expression system.' _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 2 '2D 1H-15N HSQC' . . . 15936 2 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 SER N N 15 115.101 0.2 . 1 . . . . 3 SER H . 15936 2 2 . 1 1 3 3 SER H H 1 8.344 0.02 . 1 . . . . 3 SER N . 15936 2 3 . 1 1 4 4 SER N N 15 116.919 0.2 . 1 . . . . 4 SER H . 15936 2 4 . 1 1 4 4 SER H H 1 8.299 0.02 . 1 . . . . 4 SER N . 15936 2 5 . 1 1 6 6 HIS N N 15 119.965 0.2 . 1 . . . . 6 HIS H . 15936 2 6 . 1 1 6 6 HIS H H 1 8.525 0.02 . 1 . . . . 6 HIS N . 15936 2 7 . 1 1 7 7 HIS N N 15 118.149 0.2 . 1 . . . . 7 HIS H . 15936 2 8 . 1 1 7 7 HIS H H 1 8.331 0.02 . 1 . . . . 7 HIS N . 15936 2 9 . 1 1 8 8 HIS N N 15 119.987 0.2 . 1 . . . . 8 HIS H . 15936 2 10 . 1 1 8 8 HIS H H 1 8.664 0.02 . 1 . . . . 8 HIS N . 15936 2 11 . 1 1 9 9 HIS N N 15 121.102 0.2 . 1 . . . . 9 HIS H . 15936 2 12 . 1 1 9 9 HIS H H 1 8.735 0.02 . 1 . . . . 9 HIS N . 15936 2 13 . 1 1 10 10 HIS N N 15 121.802 0.2 . 1 . . . . 10 HIS H . 15936 2 14 . 1 1 10 10 HIS H H 1 8.707 0.02 . 1 . . . . 10 HIS N . 15936 2 15 . 1 1 11 11 SER N N 15 118.986 0.2 . 1 . . . . 11 SER H . 15936 2 16 . 1 1 11 11 SER H H 1 8.517 0.02 . 1 . . . . 11 SER N . 15936 2 17 . 1 1 12 12 SER N N 15 118.427 0.2 . 1 . . . . 12 SER H . 15936 2 18 . 1 1 12 12 SER H H 1 8.546 0.02 . 1 . . . . 12 SER N . 15936 2 19 . 1 1 13 13 GLY N N 15 110.589 0.2 . 1 . . . . 13 GLY H . 15936 2 20 . 1 1 13 13 GLY H H 1 8.390 0.02 . 1 . . . . 13 GLY N . 15936 2 21 . 1 1 14 14 LEU N N 15 121.919 0.2 . 1 . . . . 14 LEU H . 15936 2 22 . 1 1 14 14 LEU H H 1 8.114 0.02 . 1 . . . . 14 LEU N . 15936 2 23 . 1 1 15 15 VAL N N 15 123.647 0.2 . 1 . . . . 15 VAL H . 15936 2 24 . 1 1 15 15 VAL H H 1 8.202 0.02 . 1 . . . . 15 VAL N . 15936 2 25 . 1 1 17 17 ARG N N 15 122.016 0.2 . 1 . . . . 17 ARG H . 15936 2 26 . 1 1 17 17 ARG H H 1 8.463 0.02 . 1 . . . . 17 ARG N . 15936 2 27 . 1 1 18 18 GLY N N 15 110.288 0.2 . 1 . . . . 18 GLY H . 15936 2 28 . 1 1 18 18 GLY H H 1 8.436 0.02 . 1 . . . . 18 GLY N . 15936 2 29 . 1 1 19 19 SER N N 15 115.311 0.2 . 1 . . . . 19 SER H . 15936 2 30 . 1 1 19 19 SER H H 1 8.177 0.02 . 1 . . . . 19 SER N . 15936 2 31 . 1 1 20 20 HIS N N 15 120.181 0.2 . 1 . . . . 20 HIS H . 15936 2 32 . 1 1 20 20 HIS H H 1 8.585 0.02 . 1 . . . . 20 HIS N . 15936 2 33 . 1 1 21 21 MET N N 15 121.414 0.2 . 1 . . . . 21 MET H . 15936 2 34 . 1 1 21 21 MET H H 1 8.335 0.02 . 1 . . . . 21 MET N . 15936 2 35 . 1 1 22 22 LEU N N 15 123.681 0.2 . 1 . . . . 22 LEU H . 15936 2 36 . 1 1 22 22 LEU H H 1 8.276 0.02 . 1 . . . . 22 LEU N . 15936 2 37 . 1 1 23 23 GLU N N 15 121.658 0.2 . 1 . . . . 23 GLU H . 15936 2 38 . 1 1 23 23 GLU H H 1 8.275 0.02 . 1 . . . . 23 GLU N . 15936 2 39 . 1 1 24 24 LEU N N 15 125.128 0.2 . 1 . . . . 24 LEU H . 15936 2 40 . 1 1 24 24 LEU H H 1 8.233 0.02 . 1 . . . . 24 LEU N . 15936 2 41 . 1 1 26 26 LEU N N 15 122.212 0.2 . 1 . . . . 26 LEU H . 15936 2 42 . 1 1 26 26 LEU H H 1 8.296 0.02 . 1 . . . . 26 LEU N . 15936 2 43 . 1 1 27 27 ASP N N 15 119.522 0.2 . 1 . . . . 27 ASP H . 15936 2 44 . 1 1 27 27 ASP H H 1 8.433 0.02 . 1 . . . . 27 ASP N . 15936 2 45 . 1 1 28 28 SER N N 15 116.466 0.2 . 1 . . . . 28 SER H . 15936 2 46 . 1 1 28 28 SER H H 1 8.225 0.02 . 1 . . . . 28 SER N . 15936 2 47 . 1 1 29 29 ALA N N 15 125.498 0.2 . 1 . . . . 29 ALA H . 15936 2 48 . 1 1 29 29 ALA H H 1 8.294 0.02 . 1 . . . . 29 ALA N . 15936 2 49 . 1 1 30 30 THR N N 15 112.640 0.2 . 1 . . . . 30 THR H . 15936 2 50 . 1 1 30 30 THR H H 1 8.086 0.02 . 1 . . . . 30 THR N . 15936 2 51 . 1 1 31 31 THR N N 15 116.044 0.2 . 1 . . . . 31 THR H . 15936 2 52 . 1 1 31 31 THR H H 1 8.062 0.02 . 1 . . . . 31 THR N . 15936 2 53 . 1 1 32 32 GLU N N 15 122.186 0.2 . 1 . . . . 32 GLU H . 15936 2 54 . 1 1 32 32 GLU H H 1 8.313 0.02 . 1 . . . . 32 GLU N . 15936 2 55 . 1 1 33 33 SER N N 15 116.639 0.2 . 1 . . . . 33 SER H . 15936 2 56 . 1 1 33 33 SER H H 1 8.253 0.02 . 1 . . . . 33 SER N . 15936 2 57 . 1 1 34 34 LEU N N 15 123.806 0.2 . 1 . . . . 34 LEU H . 15936 2 58 . 1 1 34 34 LEU H H 1 8.123 0.02 . 1 . . . . 34 LEU N . 15936 2 59 . 1 1 35 35 ARG N N 15 121.022 0.2 . 1 . . . . 35 ARG H . 15936 2 60 . 1 1 35 35 ARG H H 1 8.059 0.02 . 1 . . . . 35 ARG N . 15936 2 61 . 1 1 36 36 ALA N N 15 124.443 0.2 . 1 . . . . 36 ALA H . 15936 2 62 . 1 1 36 36 ALA H H 1 8.127 0.02 . 1 . . . . 36 ALA N . 15936 2 63 . 1 1 37 37 ALA N N 15 122.771 0.2 . 1 . . . . 37 ALA H . 15936 2 64 . 1 1 37 37 ALA H H 1 8.167 0.02 . 1 . . . . 37 ALA N . 15936 2 65 . 1 1 38 38 THR N N 15 112.304 0.2 . 1 . . . . 38 THR H . 15936 2 66 . 1 1 38 38 THR H H 1 7.956 0.02 . 1 . . . . 38 THR N . 15936 2 67 . 1 1 39 39 HIS N N 15 119.926 0.2 . 1 . . . . 39 HIS H . 15936 2 68 . 1 1 39 39 HIS H H 1 8.415 0.02 . 1 . . . . 39 HIS N . 15936 2 69 . 1 1 40 40 ASP N N 15 120.524 0.2 . 1 . . . . 40 ASP H . 15936 2 70 . 1 1 40 40 ASP H H 1 8.471 0.02 . 1 . . . . 40 ASP N . 15936 2 71 . 1 1 41 41 VAL N N 15 121.179 0.2 . 1 . . . . 41 VAL H . 15936 2 72 . 1 1 41 41 VAL H H 1 8.150 0.02 . 1 . . . . 41 VAL N . 15936 2 73 . 1 1 42 42 LEU N N 15 124.569 0.2 . 1 . . . . 42 LEU H . 15936 2 74 . 1 1 42 42 LEU H H 1 8.186 0.02 . 1 . . . . 42 LEU N . 15936 2 75 . 1 1 43 43 ALA N N 15 124.234 0.2 . 1 . . . . 43 ALA H . 15936 2 76 . 1 1 43 43 ALA H H 1 8.080 0.02 . 1 . . . . 43 ALA N . 15936 2 77 . 1 1 44 44 GLY N N 15 107.590 0.2 . 1 . . . . 44 GLY H . 15936 2 78 . 1 1 44 44 GLY H H 1 8.263 0.02 . 1 . . . . 44 GLY N . 15936 2 79 . 1 1 45 45 LEU N N 15 121.578 0.2 . 1 . . . . 45 LEU H . 15936 2 80 . 1 1 45 45 LEU H H 1 7.967 0.02 . 1 . . . . 45 LEU N . 15936 2 81 . 1 1 46 46 THR N N 15 113.796 0.2 . 1 . . . . 46 THR H . 15936 2 82 . 1 1 46 46 THR H H 1 8.028 0.02 . 1 . . . . 46 THR N . 15936 2 83 . 1 1 47 47 ALA N N 15 124.949 0.2 . 1 . . . . 47 ALA H . 15936 2 84 . 1 1 47 47 ALA H H 1 8.336 0.02 . 1 . . . . 47 ALA N . 15936 2 85 . 1 1 48 48 ARG N N 15 118.667 0.2 . 1 . . . . 48 ARG H . 15936 2 86 . 1 1 48 48 ARG H H 1 8.184 0.02 . 1 . . . . 48 ARG N . 15936 2 87 . 1 1 49 49 GLU N N 15 119.635 0.2 . 1 . . . . 49 GLU H . 15936 2 88 . 1 1 49 49 GLU H H 1 7.991 0.02 . 1 . . . . 49 GLU N . 15936 2 89 . 1 1 50 50 ALA N N 15 123.382 0.2 . 1 . . . . 50 ALA H . 15936 2 90 . 1 1 50 50 ALA H H 1 8.306 0.02 . 1 . . . . 50 ALA N . 15936 2 91 . 1 1 51 51 LYS N N 15 119.300 0.2 . 1 . . . . 51 LYS H . 15936 2 92 . 1 1 51 51 LYS H H 1 7.961 0.02 . 1 . . . . 51 LYS N . 15936 2 93 . 1 1 52 52 VAL N N 15 120.145 0.2 . 1 . . . . 52 VAL H . 15936 2 94 . 1 1 52 52 VAL H H 1 7.839 0.02 . 1 . . . . 52 VAL N . 15936 2 95 . 1 1 53 53 LEU N N 15 123.496 0.2 . 1 . . . . 53 LEU H . 15936 2 96 . 1 1 53 53 LEU H H 1 8.085 0.02 . 1 . . . . 53 LEU N . 15936 2 97 . 1 1 54 54 ARG N N 15 119.740 0.2 . 1 . . . . 54 ARG H . 15936 2 98 . 1 1 54 54 ARG H H 1 8.112 0.02 . 1 . . . . 54 ARG N . 15936 2 99 . 1 1 55 55 MET N N 15 120.668 0.2 . 1 . . . . 55 MET H . 15936 2 100 . 1 1 55 55 MET H H 1 8.135 0.02 . 1 . . . . 55 MET N . 15936 2 101 . 1 1 56 56 ARG N N 15 120.905 0.2 . 1 . . . . 56 ARG H . 15936 2 102 . 1 1 56 56 ARG H H 1 8.048 0.02 . 1 . . . . 56 ARG N . 15936 2 103 . 1 1 57 57 PHE N N 15 120.118 0.2 . 1 . . . . 57 PHE H . 15936 2 104 . 1 1 57 57 PHE H H 1 8.152 0.02 . 1 . . . . 57 PHE N . 15936 2 105 . 1 1 58 58 GLY N N 15 109.991 0.2 . 1 . . . . 58 GLY H . 15936 2 106 . 1 1 58 58 GLY H H 1 8.164 0.02 . 1 . . . . 58 GLY N . 15936 2 107 . 1 1 59 59 ILE N N 15 119.195 0.2 . 1 . . . . 59 ILE H . 15936 2 108 . 1 1 59 59 ILE H H 1 7.879 0.02 . 1 . . . . 59 ILE N . 15936 2 109 . 1 1 60 60 ASP N N 15 122.090 0.2 . 1 . . . . 60 ASP H . 15936 2 110 . 1 1 60 60 ASP H H 1 8.515 0.02 . 1 . . . . 60 ASP N . 15936 2 111 . 1 1 61 61 MET N N 15 120.850 0.2 . 1 . . . . 61 MET H . 15936 2 112 . 1 1 61 61 MET H H 1 8.294 0.02 . 1 . . . . 61 MET N . 15936 2 113 . 1 1 62 62 ASN N N 15 119.127 0.2 . 1 . . . . 62 ASN H . 15936 2 114 . 1 1 62 62 ASN H H 1 8.346 0.02 . 1 . . . . 62 ASN N . 15936 2 115 . 1 1 63 63 THR N N 15 113.863 0.2 . 1 . . . . 63 THR H . 15936 2 116 . 1 1 63 63 THR H H 1 8.014 0.02 . 1 . . . . 63 THR N . 15936 2 117 . 1 1 64 64 ASP N N 15 120.850 0.2 . 1 . . . . 64 ASP H . 15936 2 118 . 1 1 64 64 ASP H H 1 8.336 0.02 . 1 . . . . 64 ASP N . 15936 2 119 . 1 1 65 65 TYR N N 15 120.679 0.2 . 1 . . . . 65 TYR H . 15936 2 120 . 1 1 65 65 TYR H H 1 8.024 0.02 . 1 . . . . 65 TYR N . 15936 2 121 . 1 1 66 66 THR N N 15 114.871 0.2 . 1 . . . . 66 THR H . 15936 2 122 . 1 1 66 66 THR H H 1 7.956 0.02 . 1 . . . . 66 THR N . 15936 2 123 . 1 1 67 67 LEU N N 15 123.055 0.2 . 1 . . . . 67 LEU H . 15936 2 124 . 1 1 67 67 LEU H H 1 8.008 0.02 . 1 . . . . 67 LEU N . 15936 2 125 . 1 1 68 68 GLU N N 15 120.412 0.2 . 1 . . . . 68 GLU H . 15936 2 126 . 1 1 68 68 GLU H H 1 8.108 0.02 . 1 . . . . 68 GLU N . 15936 2 127 . 1 1 69 69 GLU N N 15 120.533 0.2 . 1 . . . . 69 GLU H . 15936 2 128 . 1 1 69 69 GLU H H 1 8.125 0.02 . 1 . . . . 69 GLU N . 15936 2 129 . 1 1 70 70 VAL N N 15 120.338 0.2 . 1 . . . . 70 VAL H . 15936 2 130 . 1 1 70 70 VAL H H 1 8.023 0.02 . 1 . . . . 70 VAL N . 15936 2 131 . 1 1 71 71 GLY N N 15 111.470 0.2 . 1 . . . . 71 GLY H . 15936 2 132 . 1 1 71 71 GLY H H 1 8.378 0.02 . 1 . . . . 71 GLY N . 15936 2 133 . 1 1 72 72 LYS N N 15 120.799 0.2 . 1 . . . . 72 LYS H . 15936 2 134 . 1 1 72 72 LYS H H 1 8.105 0.02 . 1 . . . . 72 LYS N . 15936 2 135 . 1 1 73 73 GLN N N 15 119.964 0.2 . 1 . . . . 73 GLN H . 15936 2 136 . 1 1 73 73 GLN H H 1 8.330 0.02 . 1 . . . . 73 GLN N . 15936 2 137 . 1 1 75 75 ASP N N 15 120.642 0.2 . 1 . . . . 75 ASP H . 15936 2 138 . 1 1 75 75 ASP H H 1 8.265 0.02 . 1 . . . . 75 ASP N . 15936 2 139 . 1 1 76 76 VAL N N 15 120.663 0.2 . 1 . . . . 76 VAL H . 15936 2 140 . 1 1 76 76 VAL H H 1 8.089 0.02 . 1 . . . . 76 VAL N . 15936 2 141 . 1 1 77 77 THR N N 15 117.012 0.2 . 1 . . . . 77 THR H . 15936 2 142 . 1 1 77 77 THR H H 1 8.090 0.02 . 1 . . . . 77 THR N . 15936 2 143 . 1 1 78 78 ARG N N 15 122.117 0.2 . 1 . . . . 78 ARG H . 15936 2 144 . 1 1 78 78 ARG H H 1 8.143 0.02 . 1 . . . . 78 ARG N . 15936 2 145 . 1 1 79 79 GLU N N 15 119.481 0.2 . 1 . . . . 79 GLU H . 15936 2 146 . 1 1 79 79 GLU H H 1 8.134 0.02 . 1 . . . . 79 GLU N . 15936 2 147 . 1 1 80 80 ARG N N 15 121.569 0.2 . 1 . . . . 80 ARG H . 15936 2 148 . 1 1 80 80 ARG H H 1 8.227 0.02 . 1 . . . . 80 ARG N . 15936 2 149 . 1 1 81 81 ILE N N 15 121.129 0.2 . 1 . . . . 81 ILE H . 15936 2 150 . 1 1 81 81 ILE H H 1 8.034 0.02 . 1 . . . . 81 ILE N . 15936 2 151 . 1 1 82 82 ARG N N 15 123.535 0.2 . 1 . . . . 82 ARG H . 15936 2 152 . 1 1 82 82 ARG H H 1 8.216 0.02 . 1 . . . . 82 ARG N . 15936 2 153 . 1 1 83 83 GLN N N 15 121.261 0.2 . 1 . . . . 83 GLN H . 15936 2 154 . 1 1 83 83 GLN H H 1 8.242 0.02 . 1 . . . . 83 GLN N . 15936 2 155 . 1 1 84 84 ILE N N 15 122.378 0.2 . 1 . . . . 84 ILE H . 15936 2 156 . 1 1 84 84 ILE H H 1 8.188 0.02 . 1 . . . . 84 ILE N . 15936 2 157 . 1 1 85 85 GLU N N 15 123.167 0.2 . 1 . . . . 85 GLU H . 15936 2 158 . 1 1 85 85 GLU H H 1 8.357 0.02 . 1 . . . . 85 GLU N . 15936 2 159 . 1 1 86 86 ALA N N 15 124.473 0.2 . 1 . . . . 86 ALA H . 15936 2 160 . 1 1 86 86 ALA H H 1 8.234 0.02 . 1 . . . . 86 ALA N . 15936 2 161 . 1 1 87 87 LYS N N 15 119.687 0.2 . 1 . . . . 87 LYS H . 15936 2 162 . 1 1 87 87 LYS H H 1 8.080 0.02 . 1 . . . . 87 LYS N . 15936 2 163 . 1 1 88 88 ALA N N 15 123.769 0.2 . 1 . . . . 88 ALA H . 15936 2 164 . 1 1 88 88 ALA H H 1 8.043 0.02 . 1 . . . . 88 ALA N . 15936 2 165 . 1 1 89 89 LEU N N 15 120.988 0.2 . 1 . . . . 89 LEU H . 15936 2 166 . 1 1 89 89 LEU H H 1 8.014 0.02 . 1 . . . . 89 LEU N . 15936 2 167 . 1 1 90 90 ARG N N 15 121.068 0.2 . 1 . . . . 90 ARG H . 15936 2 168 . 1 1 90 90 ARG H H 1 8.134 0.02 . 1 . . . . 90 ARG N . 15936 2 169 . 1 1 91 91 LYS N N 15 121.824 0.2 . 1 . . . . 91 LYS H . 15936 2 170 . 1 1 91 91 LYS H H 1 8.109 0.02 . 1 . . . . 91 LYS N . 15936 2 171 . 1 1 92 92 LEU N N 15 123.072 0.2 . 1 . . . . 92 LEU H . 15936 2 172 . 1 1 92 92 LEU H H 1 8.073 0.02 . 1 . . . . 92 LEU N . 15936 2 173 . 1 1 93 93 ARG N N 15 121.376 0.2 . 1 . . . . 93 ARG H . 15936 2 174 . 1 1 93 93 ARG H H 1 8.247 0.02 . 1 . . . . 93 ARG N . 15936 2 175 . 1 1 94 94 HIS N N 15 119.805 0.2 . 1 . . . . 94 HIS H . 15936 2 176 . 1 1 94 94 HIS H H 1 8.483 0.02 . 1 . . . . 94 HIS N . 15936 2 177 . 1 1 96 96 SER N N 15 116.960 0.2 . 1 . . . . 96 SER H . 15936 2 178 . 1 1 96 96 SER H H 1 8.486 0.02 . 1 . . . . 96 SER N . 15936 2 179 . 1 1 97 97 ARG N N 15 122.927 0.2 . 1 . . . . 97 ARG H . 15936 2 180 . 1 1 97 97 ARG H H 1 8.492 0.02 . 1 . . . . 97 ARG N . 15936 2 181 . 1 1 98 98 SER N N 15 116.315 0.2 . 1 . . . . 98 SER H . 15936 2 182 . 1 1 98 98 SER H H 1 8.331 0.02 . 1 . . . . 98 SER N . 15936 2 183 . 1 1 99 99 GLU N N 15 122.434 0.2 . 1 . . . . 99 GLU H . 15936 2 184 . 1 1 99 99 GLU H H 1 8.275 0.02 . 1 . . . . 99 GLU N . 15936 2 185 . 1 1 100 100 VAL N N 15 121.306 0.2 . 1 . . . . 100 VAL H . 15936 2 186 . 1 1 100 100 VAL H H 1 8.091 0.02 . 1 . . . . 100 VAL N . 15936 2 187 . 1 1 101 101 LEU N N 15 125.517 0.2 . 1 . . . . 101 LEU H . 15936 2 188 . 1 1 101 101 LEU H H 1 8.223 0.02 . 1 . . . . 101 LEU N . 15936 2 189 . 1 1 102 102 ARG N N 15 121.622 0.2 . 1 . . . . 102 ARG H . 15936 2 190 . 1 1 102 102 ARG H H 1 8.215 0.02 . 1 . . . . 102 ARG N . 15936 2 191 . 1 1 103 103 SER N N 15 116.132 0.2 . 1 . . . . 103 SER H . 15936 2 192 . 1 1 103 103 SER H H 1 8.119 0.02 . 1 . . . . 103 SER N . 15936 2 193 . 1 1 104 104 PHE N N 15 121.743 0.2 . 1 . . . . 104 PHE H . 15936 2 194 . 1 1 104 104 PHE H H 1 8.146 0.02 . 1 . . . . 104 PHE N . 15936 2 195 . 1 1 105 105 LEU N N 15 122.194 0.2 . 1 . . . . 105 LEU H . 15936 2 196 . 1 1 105 105 LEU H H 1 7.994 0.02 . 1 . . . . 105 LEU N . 15936 2 197 . 1 1 106 106 ASP N N 15 119.131 0.2 . 1 . . . . 106 ASP H . 15936 2 198 . 1 1 106 106 ASP H H 1 8.235 0.02 . 1 . . . . 106 ASP N . 15936 2 199 . 1 1 107 107 ASP N N 15 122.619 0.2 . 1 . . . . 107 ASP H . 15936 2 200 . 1 1 107 107 ASP H H 1 7.931 0.02 . 1 . . . . 107 ASP N . 15936 2 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chem_shift_list_3 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chem_shift_list_3 _Assigned_chem_shift_list.Entry_ID 15936 _Assigned_chem_shift_list.ID 3 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_all _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err 0.02 _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err 0.2 _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details 'M1 is deleted in the expression system.' _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 3 '2D 1H-15N HSQC' . . . 15936 3 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 SER N N 15 115.087 0.2 . 1 . . . . 3 SER H . 15936 3 2 . 1 1 3 3 SER H H 1 8.336 0.02 . 1 . . . . 3 SER N . 15936 3 3 . 1 1 4 4 SER N N 15 116.884 0.2 . 1 . . . . 4 SER H . 15936 3 4 . 1 1 4 4 SER H H 1 8.293 0.02 . 1 . . . . 4 SER N . 15936 3 5 . 1 1 6 6 HIS N N 15 119.913 0.2 . 1 . . . . 6 HIS H . 15936 3 6 . 1 1 6 6 HIS H H 1 8.517 0.02 . 1 . . . . 6 HIS N . 15936 3 7 . 1 1 7 7 HIS N N 15 118.071 0.2 . 1 . . . . 7 HIS H . 15936 3 8 . 1 1 7 7 HIS H H 1 8.322 0.02 . 1 . . . . 7 HIS N . 15936 3 9 . 1 1 8 8 HIS N N 15 119.923 0.2 . 1 . . . . 8 HIS H . 15936 3 10 . 1 1 8 8 HIS H H 1 8.655 0.02 . 1 . . . . 8 HIS N . 15936 3 11 . 1 1 9 9 HIS N N 15 121.024 0.2 . 1 . . . . 9 HIS H . 15936 3 12 . 1 1 9 9 HIS H H 1 8.728 0.02 . 1 . . . . 9 HIS N . 15936 3 13 . 1 1 10 10 HIS N N 15 121.721 0.2 . 1 . . . . 10 HIS H . 15936 3 14 . 1 1 10 10 HIS H H 1 8.700 0.02 . 1 . . . . 10 HIS N . 15936 3 15 . 1 1 11 11 SER N N 15 118.908 0.2 . 1 . . . . 11 SER H . 15936 3 16 . 1 1 11 11 SER H H 1 8.508 0.02 . 1 . . . . 11 SER N . 15936 3 17 . 1 1 12 12 SER N N 15 118.384 0.2 . 1 . . . . 12 SER H . 15936 3 18 . 1 1 12 12 SER H H 1 8.535 0.02 . 1 . . . . 12 SER N . 15936 3 19 . 1 1 13 13 GLY N N 15 110.543 0.2 . 1 . . . . 13 GLY H . 15936 3 20 . 1 1 13 13 GLY H H 1 8.381 0.02 . 1 . . . . 13 GLY N . 15936 3 21 . 1 1 14 14 LEU N N 15 121.919 0.2 . 1 . . . . 14 LEU H . 15936 3 22 . 1 1 14 14 LEU H H 1 8.114 0.02 . 1 . . . . 14 LEU N . 15936 3 23 . 1 1 15 15 VAL N N 15 123.531 0.2 . 1 . . . . 15 VAL H . 15936 3 24 . 1 1 15 15 VAL H H 1 8.188 0.02 . 1 . . . . 15 VAL N . 15936 3 25 . 1 1 17 17 ARG N N 15 121.964 0.2 . 1 . . . . 17 ARG H . 15936 3 26 . 1 1 17 17 ARG H H 1 8.447 0.02 . 1 . . . . 17 ARG N . 15936 3 27 . 1 1 18 18 GLY N N 15 110.230 0.2 . 1 . . . . 18 GLY H . 15936 3 28 . 1 1 18 18 GLY H H 1 8.427 0.02 . 1 . . . . 18 GLY N . 15936 3 29 . 1 1 19 19 SER N N 15 115.268 0.2 . 1 . . . . 19 SER H . 15936 3 30 . 1 1 19 19 SER H H 1 8.164 0.02 . 1 . . . . 19 SER N . 15936 3 31 . 1 1 20 20 HIS N N 15 120.138 0.2 . 1 . . . . 20 HIS H . 15936 3 32 . 1 1 20 20 HIS H H 1 8.574 0.02 . 1 . . . . 20 HIS N . 15936 3 33 . 1 1 21 21 MET N N 15 121.316 0.2 . 1 . . . . 21 MET H . 15936 3 34 . 1 1 21 21 MET H H 1 8.324 0.02 . 1 . . . . 21 MET N . 15936 3 35 . 1 1 22 22 LEU N N 15 123.606 0.2 . 1 . . . . 22 LEU H . 15936 3 36 . 1 1 22 22 LEU H H 1 8.261 0.02 . 1 . . . . 22 LEU N . 15936 3 37 . 1 1 23 23 GLU N N 15 121.580 0.2 . 1 . . . . 23 GLU H . 15936 3 38 . 1 1 23 23 GLU H H 1 8.252 0.02 . 1 . . . . 23 GLU N . 15936 3 39 . 1 1 24 24 LEU N N 15 125.024 0.2 . 1 . . . . 24 LEU H . 15936 3 40 . 1 1 24 24 LEU H H 1 8.214 0.02 . 1 . . . . 24 LEU N . 15936 3 41 . 1 1 26 26 LEU N N 15 122.160 0.2 . 1 . . . . 26 LEU H . 15936 3 42 . 1 1 26 26 LEU H H 1 8.279 0.02 . 1 . . . . 26 LEU N . 15936 3 43 . 1 1 27 27 ASP N N 15 119.436 0.2 . 1 . . . . 27 ASP H . 15936 3 44 . 1 1 27 27 ASP H H 1 8.416 0.02 . 1 . . . . 27 ASP N . 15936 3 45 . 1 1 28 28 SER N N 15 116.402 0.2 . 1 . . . . 28 SER H . 15936 3 46 . 1 1 28 28 SER H H 1 8.215 0.02 . 1 . . . . 28 SER N . 15936 3 47 . 1 1 29 29 ALA N N 15 125.428 0.2 . 1 . . . . 29 ALA H . 15936 3 48 . 1 1 29 29 ALA H H 1 8.288 0.02 . 1 . . . . 29 ALA N . 15936 3 49 . 1 1 30 30 THR N N 15 112.579 0.2 . 1 . . . . 30 THR H . 15936 3 50 . 1 1 30 30 THR H H 1 8.075 0.02 . 1 . . . . 30 THR N . 15936 3 51 . 1 1 31 31 THR N N 15 115.986 0.2 . 1 . . . . 31 THR H . 15936 3 52 . 1 1 31 31 THR H H 1 8.049 0.02 . 1 . . . . 31 THR N . 15936 3 53 . 1 1 32 32 GLU N N 15 122.053 0.2 . 1 . . . . 32 GLU H . 15936 3 54 . 1 1 32 32 GLU H H 1 8.304 0.02 . 1 . . . . 32 GLU N . 15936 3 55 . 1 1 33 33 SER N N 15 116.547 0.2 . 1 . . . . 33 SER H . 15936 3 56 . 1 1 33 33 SER H H 1 8.234 0.02 . 1 . . . . 33 SER N . 15936 3 57 . 1 1 34 34 LEU N N 15 123.757 0.2 . 1 . . . . 34 LEU H . 15936 3 58 . 1 1 34 34 LEU H H 1 8.106 0.02 . 1 . . . . 34 LEU N . 15936 3 59 . 1 1 35 35 ARG N N 15 121.114 0.2 . 1 . . . . 35 ARG H . 15936 3 60 . 1 1 35 35 ARG H H 1 8.067 0.02 . 1 . . . . 35 ARG N . 15936 3 61 . 1 1 36 36 ALA N N 15 124.239 0.2 . 1 . . . . 36 ALA H . 15936 3 62 . 1 1 36 36 ALA H H 1 8.106 0.02 . 1 . . . . 36 ALA N . 15936 3 63 . 1 1 37 37 ALA N N 15 122.595 0.2 . 1 . . . . 37 ALA H . 15936 3 64 . 1 1 37 37 ALA H H 1 8.144 0.02 . 1 . . . . 37 ALA N . 15936 3 65 . 1 1 38 38 THR N N 15 112.143 0.2 . 1 . . . . 38 THR H . 15936 3 66 . 1 1 38 38 THR H H 1 7.935 0.02 . 1 . . . . 38 THR N . 15936 3 67 . 1 1 39 39 HIS N N 15 119.822 0.2 . 1 . . . . 39 HIS H . 15936 3 68 . 1 1 39 39 HIS H H 1 8.385 0.02 . 1 . . . . 39 HIS N . 15936 3 69 . 1 1 40 40 ASP N N 15 120.345 0.2 . 1 . . . . 40 ASP H . 15936 3 70 . 1 1 40 40 ASP H H 1 8.451 0.02 . 1 . . . . 40 ASP N . 15936 3 71 . 1 1 41 41 VAL N N 15 121.179 0.2 . 1 . . . . 41 VAL H . 15936 3 72 . 1 1 41 41 VAL H H 1 8.150 0.02 . 1 . . . . 41 VAL N . 15936 3 73 . 1 1 42 42 LEU N N 15 124.159 0.2 . 1 . . . . 42 LEU H . 15936 3 74 . 1 1 42 42 LEU H H 1 8.154 0.02 . 1 . . . . 42 LEU N . 15936 3 75 . 1 1 43 43 ALA N N 15 124.015 0.2 . 1 . . . . 43 ALA H . 15936 3 76 . 1 1 43 43 ALA H H 1 8.048 0.02 . 1 . . . . 43 ALA N . 15936 3 77 . 1 1 44 44 GLY N N 15 107.463 0.2 . 1 . . . . 44 GLY H . 15936 3 78 . 1 1 44 44 GLY H H 1 8.242 0.02 . 1 . . . . 44 GLY N . 15936 3 79 . 1 1 45 45 LEU N N 15 121.561 0.2 . 1 . . . . 45 LEU H . 15936 3 80 . 1 1 45 45 LEU H H 1 7.931 0.02 . 1 . . . . 45 LEU N . 15936 3 81 . 1 1 46 46 THR N N 15 113.646 0.2 . 1 . . . . 46 THR H . 15936 3 82 . 1 1 46 46 THR H H 1 8.013 0.02 . 1 . . . . 46 THR N . 15936 3 83 . 1 1 47 47 ALA N N 15 124.725 0.2 . 1 . . . . 47 ALA H . 15936 3 84 . 1 1 47 47 ALA H H 1 8.356 0.02 . 1 . . . . 47 ALA N . 15936 3 85 . 1 1 48 48 ARG N N 15 118.476 0.2 . 1 . . . . 48 ARG H . 15936 3 86 . 1 1 48 48 ARG H H 1 8.176 0.02 . 1 . . . . 48 ARG N . 15936 3 87 . 1 1 49 49 GLU N N 15 119.415 0.2 . 1 . . . . 49 GLU H . 15936 3 88 . 1 1 49 49 GLU H H 1 7.952 0.02 . 1 . . . . 49 GLU N . 15936 3 89 . 1 1 50 50 ALA N N 15 122.954 0.2 . 1 . . . . 50 ALA H . 15936 3 90 . 1 1 50 50 ALA H H 1 8.317 0.02 . 1 . . . . 50 ALA N . 15936 3 91 . 1 1 51 51 LYS N N 15 119.046 0.2 . 1 . . . . 51 LYS H . 15936 3 92 . 1 1 51 51 LYS H H 1 7.914 0.02 . 1 . . . . 51 LYS N . 15936 3 93 . 1 1 52 52 VAL N N 15 119.880 0.2 . 1 . . . . 52 VAL H . 15936 3 94 . 1 1 52 52 VAL H H 1 7.800 0.02 . 1 . . . . 52 VAL N . 15936 3 95 . 1 1 53 53 LEU N N 15 122.889 0.2 . 1 . . . . 53 LEU H . 15936 3 96 . 1 1 53 53 LEU H H 1 8.065 0.02 . 1 . . . . 53 LEU N . 15936 3 97 . 1 1 54 54 ARG N N 15 119.512 0.2 . 1 . . . . 54 ARG H . 15936 3 98 . 1 1 54 54 ARG H H 1 8.100 0.02 . 1 . . . . 54 ARG N . 15936 3 99 . 1 1 55 55 MET N N 15 120.506 0.2 . 1 . . . . 55 MET H . 15936 3 100 . 1 1 55 55 MET H H 1 8.113 0.02 . 1 . . . . 55 MET N . 15936 3 101 . 1 1 56 56 ARG N N 15 120.992 0.2 . 1 . . . . 56 ARG H . 15936 3 102 . 1 1 56 56 ARG H H 1 8.057 0.02 . 1 . . . . 56 ARG N . 15936 3 103 . 1 1 57 57 PHE N N 15 119.852 0.2 . 1 . . . . 57 PHE H . 15936 3 104 . 1 1 57 57 PHE H H 1 8.129 0.02 . 1 . . . . 57 PHE N . 15936 3 105 . 1 1 58 58 GLY N N 15 109.832 0.2 . 1 . . . . 58 GLY H . 15936 3 106 . 1 1 58 58 GLY H H 1 8.122 0.02 . 1 . . . . 58 GLY N . 15936 3 107 . 1 1 59 59 ILE N N 15 119.125 0.2 . 1 . . . . 59 ILE H . 15936 3 108 . 1 1 59 59 ILE H H 1 7.855 0.02 . 1 . . . . 59 ILE N . 15936 3 109 . 1 1 60 60 ASP N N 15 122.035 0.2 . 1 . . . . 60 ASP H . 15936 3 110 . 1 1 60 60 ASP H H 1 8.496 0.02 . 1 . . . . 60 ASP N . 15936 3 111 . 1 1 61 61 MET N N 15 120.752 0.2 . 1 . . . . 61 MET H . 15936 3 112 . 1 1 61 61 MET H H 1 8.280 0.02 . 1 . . . . 61 MET N . 15936 3 113 . 1 1 62 62 ASN N N 15 119.006 0.2 . 1 . . . . 62 ASN H . 15936 3 114 . 1 1 62 62 ASN H H 1 8.326 0.02 . 1 . . . . 62 ASN N . 15936 3 115 . 1 1 63 63 THR N N 15 113.826 0.2 . 1 . . . . 63 THR H . 15936 3 116 . 1 1 63 63 THR H H 1 7.998 0.02 . 1 . . . . 63 THR N . 15936 3 117 . 1 1 64 64 ASP N N 15 120.789 0.2 . 1 . . . . 64 ASP H . 15936 3 118 . 1 1 64 64 ASP H H 1 8.325 0.02 . 1 . . . . 64 ASP N . 15936 3 119 . 1 1 65 65 TYR N N 15 120.864 0.2 . 1 . . . . 65 TYR H . 15936 3 120 . 1 1 65 65 TYR H H 1 8.033 0.02 . 1 . . . . 65 TYR N . 15936 3 121 . 1 1 66 66 THR N N 15 114.672 0.2 . 1 . . . . 66 THR H . 15936 3 122 . 1 1 66 66 THR H H 1 7.936 0.02 . 1 . . . . 66 THR N . 15936 3 123 . 1 1 67 67 LEU N N 15 122.839 0.2 . 1 . . . . 67 LEU H . 15936 3 124 . 1 1 67 67 LEU H H 1 8.005 0.02 . 1 . . . . 67 LEU N . 15936 3 125 . 1 1 68 68 GLU N N 15 119.988 0.2 . 1 . . . . 68 GLU H . 15936 3 126 . 1 1 68 68 GLU H H 1 8.072 0.02 . 1 . . . . 68 GLU N . 15936 3 127 . 1 1 69 69 GLU N N 15 120.296 0.2 . 1 . . . . 69 GLU H . 15936 3 128 . 1 1 69 69 GLU H H 1 8.091 0.02 . 1 . . . . 69 GLU N . 15936 3 129 . 1 1 70 70 VAL N N 15 120.240 0.2 . 1 . . . . 70 VAL H . 15936 3 130 . 1 1 70 70 VAL H H 1 8.003 0.02 . 1 . . . . 70 VAL N . 15936 3 131 . 1 1 71 71 GLY N N 15 111.221 0.2 . 1 . . . . 71 GLY H . 15936 3 132 . 1 1 71 71 GLY H H 1 8.356 0.02 . 1 . . . . 71 GLY N . 15936 3 133 . 1 1 72 72 LYS N N 15 120.799 0.2 . 1 . . . . 72 LYS H . 15936 3 134 . 1 1 72 72 LYS H H 1 8.105 0.02 . 1 . . . . 72 LYS N . 15936 3 135 . 1 1 73 73 GLN N N 15 119.765 0.2 . 1 . . . . 73 GLN H . 15936 3 136 . 1 1 73 73 GLN H H 1 8.313 0.02 . 1 . . . . 73 GLN N . 15936 3 137 . 1 1 75 75 ASP N N 15 120.518 0.2 . 1 . . . . 75 ASP H . 15936 3 138 . 1 1 75 75 ASP H H 1 8.244 0.02 . 1 . . . . 75 ASP N . 15936 3 139 . 1 1 76 76 VAL N N 15 120.625 0.2 . 1 . . . . 76 VAL H . 15936 3 140 . 1 1 76 76 VAL H H 1 8.077 0.02 . 1 . . . . 76 VAL N . 15936 3 141 . 1 1 77 77 THR N N 15 116.876 0.2 . 1 . . . . 77 THR H . 15936 3 142 . 1 1 77 77 THR H H 1 8.057 0.02 . 1 . . . . 77 THR N . 15936 3 143 . 1 1 78 78 ARG N N 15 122.155 0.2 . 1 . . . . 78 ARG H . 15936 3 144 . 1 1 78 78 ARG H H 1 8.144 0.02 . 1 . . . . 78 ARG N . 15936 3 145 . 1 1 79 79 GLU N N 15 118.962 0.2 . 1 . . . . 79 GLU H . 15936 3 146 . 1 1 79 79 GLU H H 1 8.095 0.02 . 1 . . . . 79 GLU N . 15936 3 147 . 1 1 80 80 ARG N N 15 121.352 0.2 . 1 . . . . 80 ARG H . 15936 3 148 . 1 1 80 80 ARG H H 1 8.199 0.02 . 1 . . . . 80 ARG N . 15936 3 149 . 1 1 81 81 ILE N N 15 121.221 0.2 . 1 . . . . 81 ILE H . 15936 3 150 . 1 1 81 81 ILE H H 1 8.039 0.02 . 1 . . . . 81 ILE N . 15936 3 151 . 1 1 82 82 ARG N N 15 122.894 0.2 . 1 . . . . 82 ARG H . 15936 3 152 . 1 1 82 82 ARG H H 1 8.169 0.02 . 1 . . . . 82 ARG N . 15936 3 153 . 1 1 83 83 GLN N N 15 120.865 0.2 . 1 . . . . 83 GLN H . 15936 3 154 . 1 1 83 83 GLN H H 1 8.198 0.02 . 1 . . . . 83 GLN N . 15936 3 155 . 1 1 84 84 ILE N N 15 122.145 0.2 . 1 . . . . 84 ILE H . 15936 3 156 . 1 1 84 84 ILE H H 1 8.162 0.02 . 1 . . . . 84 ILE N . 15936 3 157 . 1 1 85 85 GLU N N 15 122.662 0.2 . 1 . . . . 85 GLU H . 15936 3 158 . 1 1 85 85 GLU H H 1 8.345 0.02 . 1 . . . . 85 GLU N . 15936 3 159 . 1 1 86 86 ALA N N 15 123.985 0.2 . 1 . . . . 86 ALA H . 15936 3 160 . 1 1 86 86 ALA H H 1 8.200 0.02 . 1 . . . . 86 ALA N . 15936 3 161 . 1 1 87 87 LYS N N 15 119.375 0.2 . 1 . . . . 87 LYS H . 15936 3 162 . 1 1 87 87 LYS H H 1 8.029 0.02 . 1 . . . . 87 LYS N . 15936 3 163 . 1 1 88 88 ALA N N 15 123.472 0.2 . 1 . . . . 88 ALA H . 15936 3 164 . 1 1 88 88 ALA H H 1 8.003 0.02 . 1 . . . . 88 ALA N . 15936 3 165 . 1 1 89 89 LEU N N 15 120.962 0.2 . 1 . . . . 89 LEU H . 15936 3 166 . 1 1 89 89 LEU H H 1 8.014 0.02 . 1 . . . . 89 LEU N . 15936 3 167 . 1 1 90 90 ARG N N 15 121.068 0.2 . 1 . . . . 90 ARG H . 15936 3 168 . 1 1 90 90 ARG H H 1 8.134 0.02 . 1 . . . . 90 ARG N . 15936 3 169 . 1 1 91 91 LYS N N 15 121.824 0.2 . 1 . . . . 91 LYS H . 15936 3 170 . 1 1 91 91 LYS H H 1 8.109 0.02 . 1 . . . . 91 LYS N . 15936 3 171 . 1 1 92 92 LEU N N 15 122.726 0.2 . 1 . . . . 92 LEU H . 15936 3 172 . 1 1 92 92 LEU H H 1 8.025 0.02 . 1 . . . . 92 LEU N . 15936 3 173 . 1 1 93 93 ARG N N 15 120.848 0.2 . 1 . . . . 93 ARG H . 15936 3 174 . 1 1 93 93 ARG H H 1 8.187 0.02 . 1 . . . . 93 ARG N . 15936 3 175 . 1 1 94 94 HIS N N 15 119.654 0.2 . 1 . . . . 94 HIS H . 15936 3 176 . 1 1 94 94 HIS H H 1 8.459 0.02 . 1 . . . . 94 HIS N . 15936 3 177 . 1 1 96 96 SER N N 15 116.888 0.2 . 1 . . . . 96 SER H . 15936 3 178 . 1 1 96 96 SER H H 1 8.467 0.02 . 1 . . . . 96 SER N . 15936 3 179 . 1 1 97 97 ARG N N 15 122.856 0.2 . 1 . . . . 97 ARG H . 15936 3 180 . 1 1 97 97 ARG H H 1 8.495 0.02 . 1 . . . . 97 ARG N . 15936 3 181 . 1 1 98 98 SER N N 15 116.119 0.2 . 1 . . . . 98 SER H . 15936 3 182 . 1 1 98 98 SER H H 1 8.319 0.02 . 1 . . . . 98 SER N . 15936 3 183 . 1 1 99 99 GLU N N 15 122.359 0.2 . 1 . . . . 99 GLU H . 15936 3 184 . 1 1 99 99 GLU H H 1 8.245 0.02 . 1 . . . . 99 GLU N . 15936 3 185 . 1 1 100 100 VAL N N 15 121.162 0.2 . 1 . . . . 100 VAL H . 15936 3 186 . 1 1 100 100 VAL H H 1 8.076 0.02 . 1 . . . . 100 VAL N . 15936 3 187 . 1 1 101 101 LEU N N 15 125.243 0.2 . 1 . . . . 101 LEU H . 15936 3 188 . 1 1 101 101 LEU H H 1 8.201 0.02 . 1 . . . . 101 LEU N . 15936 3 189 . 1 1 102 102 ARG N N 15 121.428 0.2 . 1 . . . . 102 ARG H . 15936 3 190 . 1 1 102 102 ARG H H 1 8.183 0.02 . 1 . . . . 102 ARG N . 15936 3 191 . 1 1 103 103 SER N N 15 115.990 0.2 . 1 . . . . 103 SER H . 15936 3 192 . 1 1 103 103 SER H H 1 8.096 0.02 . 1 . . . . 103 SER N . 15936 3 193 . 1 1 104 104 PHE N N 15 121.755 0.2 . 1 . . . . 104 PHE H . 15936 3 194 . 1 1 104 104 PHE H H 1 8.149 0.02 . 1 . . . . 104 PHE N . 15936 3 195 . 1 1 105 105 LEU N N 15 122.018 0.2 . 1 . . . . 105 LEU H . 15936 3 196 . 1 1 105 105 LEU H H 1 7.975 0.02 . 1 . . . . 105 LEU N . 15936 3 197 . 1 1 106 106 ASP N N 15 119.022 0.2 . 1 . . . . 106 ASP H . 15936 3 198 . 1 1 106 106 ASP H H 1 8.212 0.02 . 1 . . . . 106 ASP N . 15936 3 199 . 1 1 107 107 ASP N N 15 122.555 0.2 . 1 . . . . 107 ASP H . 15936 3 200 . 1 1 107 107 ASP H H 1 7.919 0.02 . 1 . . . . 107 ASP N . 15936 3 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chem_shift_list_4 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chem_shift_list_4 _Assigned_chem_shift_list.Entry_ID 15936 _Assigned_chem_shift_list.ID 4 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_all _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err 0.02 _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err 0.2 _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details 'M1 is deleted in the expression system.' _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 4 '2D 1H-15N HSQC' . . . 15936 4 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 SER N N 15 115.058 0.2 . 1 . . . . 3 SER H . 15936 4 2 . 1 1 3 3 SER H H 1 8.328 0.02 . 1 . . . . 3 SER N . 15936 4 3 . 1 1 4 4 SER N N 15 116.850 0.2 . 1 . . . . 4 SER H . 15936 4 4 . 1 1 4 4 SER H H 1 8.288 0.02 . 1 . . . . 4 SER N . 15936 4 5 . 1 1 6 6 HIS N N 15 119.850 0.2 . 1 . . . . 6 HIS H . 15936 4 6 . 1 1 6 6 HIS H H 1 8.509 0.02 . 1 . . . . 6 HIS N . 15936 4 7 . 1 1 7 7 HIS N N 15 117.982 0.2 . 1 . . . . 7 HIS H . 15936 4 8 . 1 1 7 7 HIS H H 1 8.313 0.02 . 1 . . . . 7 HIS N . 15936 4 9 . 1 1 8 8 HIS N N 15 119.814 0.2 . 1 . . . . 8 HIS H . 15936 4 10 . 1 1 8 8 HIS H H 1 8.646 0.02 . 1 . . . . 8 HIS N . 15936 4 11 . 1 1 9 9 HIS N N 15 120.940 0.2 . 1 . . . . 9 HIS H . 15936 4 12 . 1 1 9 9 HIS H H 1 8.720 0.02 . 1 . . . . 9 HIS N . 15936 4 13 . 1 1 10 10 HIS N N 15 121.623 0.2 . 1 . . . . 10 HIS H . 15936 4 14 . 1 1 10 10 HIS H H 1 8.693 0.02 . 1 . . . . 10 HIS N . 15936 4 15 . 1 1 11 11 SER N N 15 118.830 0.2 . 1 . . . . 11 SER H . 15936 4 16 . 1 1 11 11 SER H H 1 8.499 0.02 . 1 . . . . 11 SER N . 15936 4 17 . 1 1 12 12 SER N N 15 118.329 0.2 . 1 . . . . 12 SER H . 15936 4 18 . 1 1 12 12 SER H H 1 8.525 0.02 . 1 . . . . 12 SER N . 15936 4 19 . 1 1 13 13 GLY N N 15 110.497 0.2 . 1 . . . . 13 GLY H . 15936 4 20 . 1 1 13 13 GLY H H 1 8.374 0.02 . 1 . . . . 13 GLY N . 15936 4 21 . 1 1 14 14 LEU N N 15 121.919 0.2 . 1 . . . . 14 LEU H . 15936 4 22 . 1 1 14 14 LEU H H 1 8.114 0.02 . 1 . . . . 14 LEU N . 15936 4 23 . 1 1 15 15 VAL N N 15 123.347 0.2 . 1 . . . . 15 VAL H . 15936 4 24 . 1 1 15 15 VAL H H 1 8.155 0.02 . 1 . . . . 15 VAL N . 15936 4 25 . 1 1 17 17 ARG N N 15 121.901 0.2 . 1 . . . . 17 ARG H . 15936 4 26 . 1 1 17 17 ARG H H 1 8.431 0.02 . 1 . . . . 17 ARG N . 15936 4 27 . 1 1 18 18 GLY N N 15 110.149 0.2 . 1 . . . . 18 GLY H . 15936 4 28 . 1 1 18 18 GLY H H 1 8.418 0.02 . 1 . . . . 18 GLY N . 15936 4 29 . 1 1 19 19 SER N N 15 115.198 0.2 . 1 . . . . 19 SER H . 15936 4 30 . 1 1 19 19 SER H H 1 8.148 0.02 . 1 . . . . 19 SER N . 15936 4 31 . 1 1 20 20 HIS N N 15 120.089 0.2 . 1 . . . . 20 HIS H . 15936 4 32 . 1 1 20 20 HIS H H 1 8.561 0.02 . 1 . . . . 20 HIS N . 15936 4 33 . 1 1 21 21 MET N N 15 121.255 0.2 . 1 . . . . 21 MET H . 15936 4 34 . 1 1 21 21 MET H H 1 8.314 0.02 . 1 . . . . 21 MET N . 15936 4 35 . 1 1 22 22 LEU N N 15 123.494 0.2 . 1 . . . . 22 LEU H . 15936 4 36 . 1 1 22 22 LEU H H 1 8.244 0.02 . 1 . . . . 22 LEU N . 15936 4 37 . 1 1 23 23 GLU N N 15 121.433 0.2 . 1 . . . . 23 GLU H . 15936 4 38 . 1 1 23 23 GLU H H 1 8.227 0.02 . 1 . . . . 23 GLU N . 15936 4 39 . 1 1 24 24 LEU N N 15 124.819 0.2 . 1 . . . . 24 LEU H . 15936 4 40 . 1 1 24 24 LEU H H 1 8.184 0.02 . 1 . . . . 24 LEU N . 15936 4 41 . 1 1 26 26 LEU N N 15 122.048 0.2 . 1 . . . . 26 LEU H . 15936 4 42 . 1 1 26 26 LEU H H 1 8.257 0.02 . 1 . . . . 26 LEU N . 15936 4 43 . 1 1 27 27 ASP N N 15 119.314 0.2 . 1 . . . . 27 ASP H . 15936 4 44 . 1 1 27 27 ASP H H 1 8.393 0.02 . 1 . . . . 27 ASP N . 15936 4 45 . 1 1 28 28 SER N N 15 116.365 0.2 . 1 . . . . 28 SER H . 15936 4 46 . 1 1 28 28 SER H H 1 8.206 0.02 . 1 . . . . 28 SER N . 15936 4 47 . 1 1 29 29 ALA N N 15 125.348 0.2 . 1 . . . . 29 ALA H . 15936 4 48 . 1 1 29 29 ALA H H 1 8.282 0.02 . 1 . . . . 29 ALA N . 15936 4 49 . 1 1 30 30 THR N N 15 112.513 0.2 . 1 . . . . 30 THR H . 15936 4 50 . 1 1 30 30 THR H H 1 8.062 0.02 . 1 . . . . 30 THR N . 15936 4 51 . 1 1 31 31 THR N N 15 115.928 0.2 . 1 . . . . 31 THR H . 15936 4 52 . 1 1 31 31 THR H H 1 8.039 0.02 . 1 . . . . 31 THR N . 15936 4 53 . 1 1 32 32 GLU N N 15 121.886 0.2 . 1 . . . . 32 GLU H . 15936 4 54 . 1 1 32 32 GLU H H 1 8.294 0.02 . 1 . . . . 32 GLU N . 15936 4 55 . 1 1 33 33 SER N N 15 116.397 0.2 . 1 . . . . 33 SER H . 15936 4 56 . 1 1 33 33 SER H H 1 8.211 0.02 . 1 . . . . 33 SER N . 15936 4 57 . 1 1 34 34 LEU N N 15 123.633 0.2 . 1 . . . . 34 LEU H . 15936 4 58 . 1 1 34 34 LEU H H 1 8.088 0.02 . 1 . . . . 34 LEU N . 15936 4 59 . 1 1 35 35 ARG N N 15 121.114 0.2 . 1 . . . . 35 ARG H . 15936 4 60 . 1 1 35 35 ARG H H 1 8.067 0.02 . 1 . . . . 35 ARG N . 15936 4 61 . 1 1 36 36 ALA N N 15 123.906 0.2 . 1 . . . . 36 ALA H . 15936 4 62 . 1 1 36 36 ALA H H 1 8.077 0.02 . 1 . . . . 36 ALA N . 15936 4 63 . 1 1 37 37 ALA N N 15 122.306 0.2 . 1 . . . . 37 ALA H . 15936 4 64 . 1 1 37 37 ALA H H 1 8.114 0.02 . 1 . . . . 37 ALA N . 15936 4 65 . 1 1 38 38 THR N N 15 111.851 0.2 . 1 . . . . 38 THR H . 15936 4 66 . 1 1 38 38 THR H H 1 7.914 0.02 . 1 . . . . 38 THR N . 15936 4 67 . 1 1 39 39 HIS N N 15 119.666 0.2 . 1 . . . . 39 HIS H . 15936 4 68 . 1 1 39 39 HIS H H 1 8.343 0.02 . 1 . . . . 39 HIS N . 15936 4 69 . 1 1 40 40 ASP N N 15 120.008 0.2 . 1 . . . . 40 ASP H . 15936 4 70 . 1 1 40 40 ASP H H 1 8.423 0.02 . 1 . . . . 40 ASP N . 15936 4 71 . 1 1 41 41 VAL N N 15 121.179 0.2 . 1 . . . . 41 VAL H . 15936 4 72 . 1 1 41 41 VAL H H 1 8.150 0.02 . 1 . . . . 41 VAL N . 15936 4 73 . 1 1 42 42 LEU N N 15 123.449 0.2 . 1 . . . . 42 LEU H . 15936 4 74 . 1 1 42 42 LEU H H 1 8.106 0.02 . 1 . . . . 42 LEU N . 15936 4 75 . 1 1 43 43 ALA N N 15 123.639 0.2 . 1 . . . . 43 ALA H . 15936 4 76 . 1 1 43 43 ALA H H 1 8.002 0.02 . 1 . . . . 43 ALA N . 15936 4 77 . 1 1 44 44 GLY N N 15 107.290 0.2 . 1 . . . . 44 GLY H . 15936 4 78 . 1 1 44 44 GLY H H 1 8.206 0.02 . 1 . . . . 44 GLY N . 15936 4 79 . 1 1 45 45 LEU N N 15 121.512 0.2 . 1 . . . . 45 LEU H . 15936 4 80 . 1 1 45 45 LEU H H 1 7.875 0.02 . 1 . . . . 45 LEU N . 15936 4 81 . 1 1 46 46 THR N N 15 113.426 0.2 . 1 . . . . 46 THR H . 15936 4 82 . 1 1 46 46 THR H H 1 7.990 0.02 . 1 . . . . 46 THR N . 15936 4 83 . 1 1 47 47 ALA N N 15 124.392 0.2 . 1 . . . . 47 ALA H . 15936 4 84 . 1 1 47 47 ALA H H 1 8.396 0.02 . 1 . . . . 47 ALA N . 15936 4 85 . 1 1 48 48 ARG N N 15 118.222 0.2 . 1 . . . . 48 ARG H . 15936 4 86 . 1 1 48 48 ARG H H 1 8.165 0.02 . 1 . . . . 48 ARG N . 15936 4 87 . 1 1 49 49 GLU N N 15 119.074 0.2 . 1 . . . . 49 GLU H . 15936 4 88 . 1 1 49 49 GLU H H 1 7.894 0.02 . 1 . . . . 49 GLU N . 15936 4 89 . 1 1 50 50 ALA N N 15 122.319 0.2 . 1 . . . . 50 ALA H . 15936 4 90 . 1 1 50 50 ALA H H 1 8.348 0.02 . 1 . . . . 50 ALA N . 15936 4 91 . 1 1 51 51 LYS N N 15 118.665 0.2 . 1 . . . . 51 LYS H . 15936 4 92 . 1 1 51 51 LYS H H 1 7.849 0.02 . 1 . . . . 51 LYS N . 15936 4 93 . 1 1 52 52 VAL N N 15 119.585 0.2 . 1 . . . . 52 VAL H . 15936 4 94 . 1 1 52 52 VAL H H 1 7.758 0.02 . 1 . . . . 52 VAL N . 15936 4 95 . 1 1 53 53 LEU N N 15 123.565 0.2 . 1 . . . . 53 LEU H . 15936 4 96 . 1 1 53 53 LEU H H 1 8.087 0.02 . 1 . . . . 53 LEU N . 15936 4 97 . 1 1 54 54 ARG N N 15 119.763 0.2 . 1 . . . . 54 ARG H . 15936 4 98 . 1 1 54 54 ARG H H 1 8.112 0.02 . 1 . . . . 54 ARG N . 15936 4 99 . 1 1 55 55 MET N N 15 120.668 0.2 . 1 . . . . 55 MET H . 15936 4 100 . 1 1 55 55 MET H H 1 8.135 0.02 . 1 . . . . 55 MET N . 15936 4 101 . 1 1 56 56 ARG N N 15 120.992 0.2 . 1 . . . . 56 ARG H . 15936 4 102 . 1 1 56 56 ARG H H 1 8.057 0.02 . 1 . . . . 56 ARG N . 15936 4 103 . 1 1 57 57 PHE N N 15 120.164 0.2 . 1 . . . . 57 PHE H . 15936 4 104 . 1 1 57 57 PHE H H 1 8.155 0.02 . 1 . . . . 57 PHE N . 15936 4 105 . 1 1 58 58 GLY N N 15 109.566 0.2 . 1 . . . . 58 GLY H . 15936 4 106 . 1 1 58 58 GLY H H 1 8.056 0.02 . 1 . . . . 58 GLY N . 15936 4 107 . 1 1 59 59 ILE N N 15 118.998 0.2 . 1 . . . . 59 ILE H . 15936 4 108 . 1 1 59 59 ILE H H 1 7.818 0.02 . 1 . . . . 59 ILE N . 15936 4 109 . 1 1 60 60 ASP N N 15 122.001 0.2 . 1 . . . . 60 ASP H . 15936 4 110 . 1 1 60 60 ASP H H 1 8.472 0.02 . 1 . . . . 60 ASP N . 15936 4 111 . 1 1 61 61 MET N N 15 120.604 0.2 . 1 . . . . 61 MET H . 15936 4 112 . 1 1 61 61 MET H H 1 8.263 0.02 . 1 . . . . 61 MET N . 15936 4 113 . 1 1 62 62 ASN N N 15 118.853 0.2 . 1 . . . . 62 ASN H . 15936 4 114 . 1 1 62 62 ASN H H 1 8.305 0.02 . 1 . . . . 62 ASN N . 15936 4 115 . 1 1 63 63 THR N N 15 113.768 0.2 . 1 . . . . 63 THR H . 15936 4 116 . 1 1 63 63 THR H H 1 7.979 0.02 . 1 . . . . 63 THR N . 15936 4 117 . 1 1 64 64 ASP N N 15 120.688 0.2 . 1 . . . . 64 ASP H . 15936 4 118 . 1 1 64 64 ASP H H 1 8.316 0.02 . 1 . . . . 64 ASP N . 15936 4 119 . 1 1 65 65 TYR N N 15 120.864 0.2 . 1 . . . . 65 TYR H . 15936 4 120 . 1 1 65 65 TYR H H 1 8.033 0.02 . 1 . . . . 65 TYR N . 15936 4 121 . 1 1 66 66 THR N N 15 114.372 0.2 . 1 . . . . 66 THR H . 15936 4 122 . 1 1 66 66 THR H H 1 7.913 0.02 . 1 . . . . 66 THR N . 15936 4 123 . 1 1 67 67 LEU N N 15 122.509 0.2 . 1 . . . . 67 LEU H . 15936 4 124 . 1 1 67 67 LEU H H 1 8.011 0.02 . 1 . . . . 67 LEU N . 15936 4 125 . 1 1 68 68 GLU N N 15 120.412 0.2 . 1 . . . . 68 GLU H . 15936 4 126 . 1 1 68 68 GLU H H 1 8.108 0.02 . 1 . . . . 68 GLU N . 15936 4 127 . 1 1 69 69 GLU N N 15 120.533 0.2 . 1 . . . . 69 GLU H . 15936 4 128 . 1 1 69 69 GLU H H 1 8.125 0.02 . 1 . . . . 69 GLU N . 15936 4 129 . 1 1 70 70 VAL N N 15 120.610 0.2 . 1 . . . . 70 VAL H . 15936 4 130 . 1 1 70 70 VAL H H 1 8.014 0.02 . 1 . . . . 70 VAL N . 15936 4 131 . 1 1 71 71 GLY N N 15 110.742 0.2 . 1 . . . . 71 GLY H . 15936 4 132 . 1 1 71 71 GLY H H 1 8.325 0.02 . 1 . . . . 71 GLY N . 15936 4 133 . 1 1 72 72 LYS N N 15 120.799 0.2 . 1 . . . . 72 LYS H . 15936 4 134 . 1 1 72 72 LYS H H 1 8.105 0.02 . 1 . . . . 72 LYS N . 15936 4 135 . 1 1 73 73 GLN N N 15 119.436 0.2 . 1 . . . . 73 GLN H . 15936 4 136 . 1 1 73 73 GLN H H 1 8.283 0.02 . 1 . . . . 73 GLN N . 15936 4 137 . 1 1 75 75 ASP N N 15 120.258 0.2 . 1 . . . . 75 ASP H . 15936 4 138 . 1 1 75 75 ASP H H 1 8.219 0.02 . 1 . . . . 75 ASP N . 15936 4 139 . 1 1 76 76 VAL N N 15 120.576 0.2 . 1 . . . . 76 VAL H . 15936 4 140 . 1 1 76 76 VAL H H 1 8.065 0.02 . 1 . . . . 76 VAL N . 15936 4 141 . 1 1 77 77 THR N N 15 116.723 0.2 . 1 . . . . 77 THR H . 15936 4 142 . 1 1 77 77 THR H H 1 8.005 0.02 . 1 . . . . 77 THR N . 15936 4 143 . 1 1 78 78 ARG N N 15 122.155 0.2 . 1 . . . . 78 ARG H . 15936 4 144 . 1 1 78 78 ARG H H 1 8.144 0.02 . 1 . . . . 78 ARG N . 15936 4 145 . 1 1 79 79 GLU N N 15 118.038 0.2 . 1 . . . . 79 GLU H . 15936 4 146 . 1 1 79 79 GLU H H 1 8.032 0.02 . 1 . . . . 79 GLU N . 15936 4 147 . 1 1 80 80 ARG N N 15 121.609 0.2 . 1 . . . . 80 ARG H . 15936 4 148 . 1 1 80 80 ARG H H 1 8.228 0.02 . 1 . . . . 80 ARG N . 15936 4 149 . 1 1 81 81 ILE N N 15 121.221 0.2 . 1 . . . . 81 ILE H . 15936 4 150 . 1 1 81 81 ILE H H 1 8.039 0.02 . 1 . . . . 81 ILE N . 15936 4 151 . 1 1 82 82 ARG N N 15 122.290 0.2 . 1 . . . . 82 ARG H . 15936 4 152 . 1 1 82 82 ARG H H 1 8.114 0.02 . 1 . . . . 82 ARG N . 15936 4 153 . 1 1 83 83 GLN N N 15 121.261 0.2 . 1 . . . . 83 GLN H . 15936 4 154 . 1 1 83 83 GLN H H 1 8.242 0.02 . 1 . . . . 83 GLN N . 15936 4 155 . 1 1 84 84 ILE N N 15 121.804 0.2 . 1 . . . . 84 ILE H . 15936 4 156 . 1 1 84 84 ILE H H 1 8.134 0.02 . 1 . . . . 84 ILE N . 15936 4 157 . 1 1 85 85 GLU N N 15 121.850 0.2 . 1 . . . . 85 GLU H . 15936 4 158 . 1 1 85 85 GLU H H 1 8.345 0.02 . 1 . . . . 85 GLU N . 15936 4 159 . 1 1 86 86 ALA N N 15 123.330 0.2 . 1 . . . . 86 ALA H . 15936 4 160 . 1 1 86 86 ALA H H 1 8.162 0.02 . 1 . . . . 86 ALA N . 15936 4 161 . 1 1 87 87 LYS N N 15 118.890 0.2 . 1 . . . . 87 LYS H . 15936 4 162 . 1 1 87 87 LYS H H 1 7.948 0.02 . 1 . . . . 87 LYS N . 15936 4 163 . 1 1 88 88 ALA N N 15 123.033 0.2 . 1 . . . . 88 ALA H . 15936 4 164 . 1 1 88 88 ALA H H 1 7.954 0.02 . 1 . . . . 88 ALA N . 15936 4 165 . 1 1 89 89 LEU N N 15 120.962 0.2 . 1 . . . . 89 LEU H . 15936 4 166 . 1 1 89 89 LEU H H 1 8.014 0.02 . 1 . . . . 89 LEU N . 15936 4 167 . 1 1 90 90 ARG N N 15 121.068 0.2 . 1 . . . . 90 ARG H . 15936 4 168 . 1 1 90 90 ARG H H 1 8.134 0.02 . 1 . . . . 90 ARG N . 15936 4 169 . 1 1 91 91 LYS N N 15 121.824 0.2 . 1 . . . . 91 LYS H . 15936 4 170 . 1 1 91 91 LYS H H 1 8.109 0.02 . 1 . . . . 91 LYS N . 15936 4 171 . 1 1 92 92 LEU N N 15 122.200 0.2 . 1 . . . . 92 LEU H . 15936 4 172 . 1 1 92 92 LEU H H 1 7.955 0.02 . 1 . . . . 92 LEU N . 15936 4 173 . 1 1 93 93 ARG N N 15 121.376 0.2 . 1 . . . . 93 ARG H . 15936 4 174 . 1 1 93 93 ARG H H 1 8.247 0.02 . 1 . . . . 93 ARG N . 15936 4 175 . 1 1 94 94 HIS N N 15 119.388 0.2 . 1 . . . . 94 HIS H . 15936 4 176 . 1 1 94 94 HIS H H 1 8.431 0.02 . 1 . . . . 94 HIS N . 15936 4 177 . 1 1 96 96 SER N N 15 116.776 0.2 . 1 . . . . 96 SER H . 15936 4 178 . 1 1 96 96 SER H H 1 8.435 0.02 . 1 . . . . 96 SER N . 15936 4 179 . 1 1 97 97 ARG N N 15 122.777 0.2 . 1 . . . . 97 ARG H . 15936 4 180 . 1 1 97 97 ARG H H 1 8.508 0.02 . 1 . . . . 97 ARG N . 15936 4 181 . 1 1 98 98 SER N N 15 115.752 0.2 . 1 . . . . 98 SER H . 15936 4 182 . 1 1 98 98 SER H H 1 8.305 0.02 . 1 . . . . 98 SER N . 15936 4 183 . 1 1 99 99 GLU N N 15 122.249 0.2 . 1 . . . . 99 GLU H . 15936 4 184 . 1 1 99 99 GLU H H 1 8.201 0.02 . 1 . . . . 99 GLU N . 15936 4 185 . 1 1 100 100 VAL N N 15 120.991 0.2 . 1 . . . . 100 VAL H . 15936 4 186 . 1 1 100 100 VAL H H 1 8.053 0.02 . 1 . . . . 100 VAL N . 15936 4 187 . 1 1 101 101 LEU N N 15 124.726 0.2 . 1 . . . . 101 LEU H . 15936 4 188 . 1 1 101 101 LEU H H 1 8.175 0.02 . 1 . . . . 101 LEU N . 15936 4 189 . 1 1 102 102 ARG N N 15 121.662 0.2 . 1 . . . . 102 ARG H . 15936 4 190 . 1 1 102 102 ARG H H 1 8.216 0.02 . 1 . . . . 102 ARG N . 15936 4 191 . 1 1 103 103 SER N N 15 115.745 0.2 . 1 . . . . 103 SER H . 15936 4 192 . 1 1 103 103 SER H H 1 8.059 0.02 . 1 . . . . 103 SER N . 15936 4 193 . 1 1 104 104 PHE N N 15 121.755 0.2 . 1 . . . . 104 PHE H . 15936 4 194 . 1 1 104 104 PHE H H 1 8.149 0.02 . 1 . . . . 104 PHE N . 15936 4 195 . 1 1 105 105 LEU N N 15 121.689 0.2 . 1 . . . . 105 LEU H . 15936 4 196 . 1 1 105 105 LEU H H 1 7.948 0.02 . 1 . . . . 105 LEU N . 15936 4 197 . 1 1 106 106 ASP N N 15 118.779 0.2 . 1 . . . . 106 ASP H . 15936 4 198 . 1 1 106 106 ASP H H 1 8.177 0.02 . 1 . . . . 106 ASP N . 15936 4 199 . 1 1 107 107 ASP N N 15 122.452 0.2 . 1 . . . . 107 ASP H . 15936 4 200 . 1 1 107 107 ASP H H 1 7.903 0.02 . 1 . . . . 107 ASP N . 15936 4 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chem_shift_list_5 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chem_shift_list_5 _Assigned_chem_shift_list.Entry_ID 15936 _Assigned_chem_shift_list.ID 5 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_all _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err 0.02 _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err 0.2 _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details 'M1 is deleted in the expression system.' _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 5 '2D 1H-15N HSQC' . . . 15936 5 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 SER N N 15 114.948 0.2 . 1 . . . . 3 SER H . 15936 5 2 . 1 1 3 3 SER H H 1 8.319 0.02 . 1 . . . . 3 SER N . 15936 5 3 . 1 1 4 4 SER N N 15 116.786 0.2 . 1 . . . . 4 SER H . 15936 5 4 . 1 1 4 4 SER H H 1 8.282 0.02 . 1 . . . . 4 SER N . 15936 5 5 . 1 1 6 6 HIS N N 15 119.775 0.2 . 1 . . . . 6 HIS H . 15936 5 6 . 1 1 6 6 HIS H H 1 8.497 0.02 . 1 . . . . 6 HIS N . 15936 5 7 . 1 1 7 7 HIS N N 15 117.884 0.2 . 1 . . . . 7 HIS H . 15936 5 8 . 1 1 7 7 HIS H H 1 8.300 0.02 . 1 . . . . 7 HIS N . 15936 5 9 . 1 1 8 8 HIS N N 15 119.733 0.2 . 1 . . . . 8 HIS H . 15936 5 10 . 1 1 8 8 HIS H H 1 8.637 0.02 . 1 . . . . 8 HIS N . 15936 5 11 . 1 1 9 9 HIS N N 15 120.813 0.2 . 1 . . . . 9 HIS H . 15936 5 12 . 1 1 9 9 HIS H H 1 8.711 0.02 . 1 . . . . 9 HIS N . 15936 5 13 . 1 1 10 10 HIS N N 15 121.496 0.2 . 1 . . . . 10 HIS H . 15936 5 14 . 1 1 10 10 HIS H H 1 8.684 0.02 . 1 . . . . 10 HIS N . 15936 5 15 . 1 1 11 11 SER N N 15 118.720 0.2 . 1 . . . . 11 SER H . 15936 5 16 . 1 1 11 11 SER H H 1 8.487 0.02 . 1 . . . . 11 SER N . 15936 5 17 . 1 1 12 12 SER N N 15 118.265 0.2 . 1 . . . . 12 SER H . 15936 5 18 . 1 1 12 12 SER H H 1 8.511 0.02 . 1 . . . . 12 SER N . 15936 5 19 . 1 1 13 13 GLY N N 15 110.416 0.2 . 1 . . . . 13 GLY H . 15936 5 20 . 1 1 13 13 GLY H H 1 8.366 0.02 . 1 . . . . 13 GLY N . 15936 5 21 . 1 1 14 14 LEU N N 15 121.919 0.2 . 1 . . . . 14 LEU H . 15936 5 22 . 1 1 14 14 LEU H H 1 8.114 0.02 . 1 . . . . 14 LEU N . 15936 5 23 . 1 1 15 15 VAL N N 15 123.139 0.2 . 1 . . . . 15 VAL H . 15936 5 24 . 1 1 15 15 VAL H H 1 8.127 0.02 . 1 . . . . 15 VAL N . 15936 5 25 . 1 1 17 17 ARG N N 15 121.823 0.2 . 1 . . . . 17 ARG H . 15936 5 26 . 1 1 17 17 ARG H H 1 8.409 0.02 . 1 . . . . 17 ARG N . 15936 5 27 . 1 1 18 18 GLY N N 15 110.042 0.2 . 1 . . . . 18 GLY H . 15936 5 28 . 1 1 18 18 GLY H H 1 8.406 0.02 . 1 . . . . 18 GLY N . 15936 5 29 . 1 1 19 19 SER N N 15 115.106 0.2 . 1 . . . . 19 SER H . 15936 5 30 . 1 1 19 19 SER H H 1 8.129 0.02 . 1 . . . . 19 SER N . 15936 5 31 . 1 1 20 20 HIS N N 15 119.996 0.2 . 1 . . . . 20 HIS H . 15936 5 32 . 1 1 20 20 HIS H H 1 8.547 0.02 . 1 . . . . 20 HIS N . 15936 5 33 . 1 1 21 21 MET N N 15 121.085 0.2 . 1 . . . . 21 MET H . 15936 5 34 . 1 1 21 21 MET H H 1 8.299 0.02 . 1 . . . . 21 MET N . 15936 5 35 . 1 1 22 22 LEU N N 15 123.332 0.2 . 1 . . . . 22 LEU H . 15936 5 36 . 1 1 22 22 LEU H H 1 8.218 0.02 . 1 . . . . 22 LEU N . 15936 5 37 . 1 1 23 23 GLU N N 15 121.254 0.2 . 1 . . . . 23 GLU H . 15936 5 38 . 1 1 23 23 GLU H H 1 8.190 0.02 . 1 . . . . 23 GLU N . 15936 5 39 . 1 1 24 24 LEU N N 15 124.585 0.2 . 1 . . . . 24 LEU H . 15936 5 40 . 1 1 24 24 LEU H H 1 8.149 0.02 . 1 . . . . 24 LEU N . 15936 5 41 . 1 1 26 26 LEU N N 15 121.889 0.2 . 1 . . . . 26 LEU H . 15936 5 42 . 1 1 26 26 LEU H H 1 8.215 0.02 . 1 . . . . 26 LEU N . 15936 5 43 . 1 1 27 27 ASP N N 15 119.135 0.2 . 1 . . . . 27 ASP H . 15936 5 44 . 1 1 27 27 ASP H H 1 8.356 0.02 . 1 . . . . 27 ASP N . 15936 5 45 . 1 1 28 28 SER N N 15 116.258 0.2 . 1 . . . . 28 SER H . 15936 5 46 . 1 1 28 28 SER H H 1 8.202 0.02 . 1 . . . . 28 SER N . 15936 5 47 . 1 1 29 29 ALA N N 15 125.230 0.2 . 1 . . . . 29 ALA H . 15936 5 48 . 1 1 29 29 ALA H H 1 8.277 0.02 . 1 . . . . 29 ALA N . 15936 5 49 . 1 1 30 30 THR N N 15 112.513 0.2 . 1 . . . . 30 THR H . 15936 5 50 . 1 1 30 30 THR H H 1 8.051 0.02 . 1 . . . . 30 THR N . 15936 5 51 . 1 1 31 31 THR N N 15 115.836 0.2 . 1 . . . . 31 THR H . 15936 5 52 . 1 1 31 31 THR H H 1 8.033 0.02 . 1 . . . . 31 THR N . 15936 5 53 . 1 1 32 32 GLU N N 15 121.597 0.2 . 1 . . . . 32 GLU H . 15936 5 54 . 1 1 32 32 GLU H H 1 8.280 0.02 . 1 . . . . 32 GLU N . 15936 5 55 . 1 1 33 33 SER N N 15 116.267 0.2 . 1 . . . . 33 SER H . 15936 5 56 . 1 1 33 33 SER H H 1 8.182 0.02 . 1 . . . . 33 SER N . 15936 5 57 . 1 1 34 34 LEU N N 15 123.520 0.2 . 1 . . . . 34 LEU H . 15936 5 58 . 1 1 34 34 LEU H H 1 8.071 0.02 . 1 . . . . 34 LEU N . 15936 5 59 . 1 1 35 35 ARG N N 15 121.114 0.2 . 1 . . . . 35 ARG H . 15936 5 60 . 1 1 35 35 ARG H H 1 8.067 0.02 . 1 . . . . 35 ARG N . 15936 5 61 . 1 1 36 36 ALA N N 15 123.349 0.2 . 1 . . . . 36 ALA H . 15936 5 62 . 1 1 36 36 ALA H H 1 8.039 0.02 . 1 . . . . 36 ALA N . 15936 5 63 . 1 1 37 37 ALA N N 15 121.698 0.2 . 1 . . . . 37 ALA H . 15936 5 64 . 1 1 37 37 ALA H H 1 8.065 0.02 . 1 . . . . 37 ALA N . 15936 5 65 . 1 1 38 38 THR N N 15 111.435 0.2 . 1 . . . . 38 THR H . 15936 5 66 . 1 1 38 38 THR H H 1 7.900 0.02 . 1 . . . . 38 THR N . 15936 5 67 . 1 1 39 39 HIS N N 15 119.412 0.2 . 1 . . . . 39 HIS H . 15936 5 68 . 1 1 39 39 HIS H H 1 8.271 0.02 . 1 . . . . 39 HIS N . 15936 5 69 . 1 1 40 40 ASP N N 15 119.341 0.2 . 1 . . . . 40 ASP H . 15936 5 70 . 1 1 40 40 ASP H H 1 8.376 0.02 . 1 . . . . 40 ASP N . 15936 5 71 . 1 1 41 41 VAL N N 15 121.179 0.2 . 1 . . . . 41 VAL H . 15936 5 72 . 1 1 41 41 VAL H H 1 8.150 0.02 . 1 . . . . 41 VAL N . 15936 5 73 . 1 1 42 42 LEU N N 15 123.449 0.2 . 1 . . . . 42 LEU H . 15936 5 74 . 1 1 42 42 LEU H H 1 8.106 0.02 . 1 . . . . 42 LEU N . 15936 5 75 . 1 1 43 43 ALA N N 15 122.981 0.2 . 1 . . . . 43 ALA H . 15936 5 76 . 1 1 43 43 ALA H H 1 7.949 0.02 . 1 . . . . 43 ALA N . 15936 5 77 . 1 1 44 44 GLY N N 15 106.920 0.2 . 1 . . . . 44 GLY H . 15936 5 78 . 1 1 44 44 GLY H H 1 8.133 0.02 . 1 . . . . 44 GLY N . 15936 5 79 . 1 1 45 45 LEU N N 15 121.532 0.2 . 1 . . . . 45 LEU H . 15936 5 80 . 1 1 45 45 LEU H H 1 7.795 0.02 . 1 . . . . 45 LEU N . 15936 5 81 . 1 1 46 46 THR N N 15 113.282 0.2 . 1 . . . . 46 THR H . 15936 5 82 . 1 1 46 46 THR H H 1 7.965 0.02 . 1 . . . . 46 THR N . 15936 5 83 . 1 1 47 47 ALA N N 15 123.965 0.2 . 1 . . . . 47 ALA H . 15936 5 84 . 1 1 47 47 ALA H H 1 8.451 0.02 . 1 . . . . 47 ALA N . 15936 5 85 . 1 1 48 48 ARG N N 15 117.835 0.2 . 1 . . . . 48 ARG H . 15936 5 86 . 1 1 48 48 ARG H H 1 8.154 0.02 . 1 . . . . 48 ARG N . 15936 5 87 . 1 1 49 49 GLU N N 15 118.595 0.2 . 1 . . . . 49 GLU H . 15936 5 88 . 1 1 49 49 GLU H H 1 7.826 0.02 . 1 . . . . 49 GLU N . 15936 5 89 . 1 1 50 50 ALA N N 15 121.407 0.2 . 1 . . . . 50 ALA H . 15936 5 90 . 1 1 50 50 ALA H H 1 8.398 0.02 . 1 . . . . 50 ALA N . 15936 5 91 . 1 1 51 51 LYS N N 15 118.206 0.2 . 1 . . . . 51 LYS H . 15936 5 92 . 1 1 51 51 LYS H H 1 7.772 0.02 . 1 . . . . 51 LYS N . 15936 5 93 . 1 1 52 52 VAL N N 15 119.331 0.2 . 1 . . . . 52 VAL H . 15936 5 94 . 1 1 52 52 VAL H H 1 7.724 0.02 . 1 . . . . 52 VAL N . 15936 5 95 . 1 1 53 53 LEU N N 15 123.565 0.2 . 1 . . . . 53 LEU H . 15936 5 96 . 1 1 53 53 LEU H H 1 8.087 0.02 . 1 . . . . 53 LEU N . 15936 5 97 . 1 1 54 54 ARG N N 15 119.763 0.2 . 1 . . . . 54 ARG H . 15936 5 98 . 1 1 54 54 ARG H H 1 8.112 0.02 . 1 . . . . 54 ARG N . 15936 5 99 . 1 1 55 55 MET N N 15 120.668 0.2 . 1 . . . . 55 MET H . 15936 5 100 . 1 1 55 55 MET H H 1 8.135 0.02 . 1 . . . . 55 MET N . 15936 5 101 . 1 1 56 56 ARG N N 15 120.992 0.2 . 1 . . . . 56 ARG H . 15936 5 102 . 1 1 56 56 ARG H H 1 8.057 0.02 . 1 . . . . 56 ARG N . 15936 5 103 . 1 1 57 57 PHE N N 15 120.164 0.2 . 1 . . . . 57 PHE H . 15936 5 104 . 1 1 57 57 PHE H H 1 8.155 0.02 . 1 . . . . 57 PHE N . 15936 5 105 . 1 1 58 58 GLY N N 15 109.136 0.2 . 1 . . . . 58 GLY H . 15936 5 106 . 1 1 58 58 GLY H H 1 7.957 0.02 . 1 . . . . 58 GLY N . 15936 5 107 . 1 1 59 59 ILE N N 15 118.894 0.2 . 1 . . . . 59 ILE H . 15936 5 108 . 1 1 59 59 ILE H H 1 7.766 0.02 . 1 . . . . 59 ILE N . 15936 5 109 . 1 1 60 60 ASP N N 15 122.018 0.2 . 1 . . . . 60 ASP H . 15936 5 110 . 1 1 60 60 ASP H H 1 8.435 0.02 . 1 . . . . 60 ASP N . 15936 5 111 . 1 1 61 61 MET N N 15 120.442 0.2 . 1 . . . . 61 MET H . 15936 5 112 . 1 1 61 61 MET H H 1 8.245 0.02 . 1 . . . . 61 MET N . 15936 5 113 . 1 1 62 62 ASN N N 15 118.587 0.2 . 1 . . . . 62 ASN H . 15936 5 114 . 1 1 62 62 ASN H H 1 8.266 0.02 . 1 . . . . 62 ASN N . 15936 5 115 . 1 1 63 63 THR N N 15 113.762 0.2 . 1 . . . . 63 THR H . 15936 5 116 . 1 1 63 63 THR H H 1 7.962 0.02 . 1 . . . . 63 THR N . 15936 5 117 . 1 1 64 64 ASP N N 15 120.526 0.2 . 1 . . . . 64 ASP H . 15936 5 118 . 1 1 64 64 ASP H H 1 8.311 0.02 . 1 . . . . 64 ASP N . 15936 5 119 . 1 1 65 65 TYR N N 15 120.864 0.2 . 1 . . . . 65 TYR H . 15936 5 120 . 1 1 65 65 TYR H H 1 8.033 0.02 . 1 . . . . 65 TYR N . 15936 5 121 . 1 1 66 66 THR N N 15 113.945 0.2 . 1 . . . . 66 THR H . 15936 5 122 . 1 1 66 66 THR H H 1 7.879 0.02 . 1 . . . . 66 THR N . 15936 5 123 . 1 1 67 67 LEU N N 15 122.163 0.2 . 1 . . . . 67 LEU H . 15936 5 124 . 1 1 67 67 LEU H H 1 8.026 0.02 . 1 . . . . 67 LEU N . 15936 5 125 . 1 1 68 68 GLU N N 15 120.412 0.2 . 1 . . . . 68 GLU H . 15936 5 126 . 1 1 68 68 GLU H H 1 8.108 0.02 . 1 . . . . 68 GLU N . 15936 5 127 . 1 1 69 69 GLU N N 15 120.533 0.2 . 1 . . . . 69 GLU H . 15936 5 128 . 1 1 69 69 GLU H H 1 8.125 0.02 . 1 . . . . 69 GLU N . 15936 5 129 . 1 1 70 70 VAL N N 15 120.367 0.2 . 1 . . . . 70 VAL H . 15936 5 130 . 1 1 70 70 VAL H H 1 8.024 0.02 . 1 . . . . 70 VAL N . 15936 5 131 . 1 1 71 71 GLY N N 15 109.812 0.2 . 1 . . . . 71 GLY H . 15936 5 132 . 1 1 71 71 GLY H H 1 8.287 0.02 . 1 . . . . 71 GLY N . 15936 5 133 . 1 1 72 72 LYS N N 15 120.799 0.2 . 1 . . . . 72 LYS H . 15936 5 134 . 1 1 72 72 LYS H H 1 8.105 0.02 . 1 . . . . 72 LYS N . 15936 5 135 . 1 1 73 73 GLN N N 15 118.893 0.2 . 1 . . . . 73 GLN H . 15936 5 136 . 1 1 73 73 GLN H H 1 8.231 0.02 . 1 . . . . 73 GLN N . 15936 5 137 . 1 1 75 75 ASP N N 15 119.845 0.2 . 1 . . . . 75 ASP H . 15936 5 138 . 1 1 75 75 ASP H H 1 8.188 0.02 . 1 . . . . 75 ASP N . 15936 5 139 . 1 1 76 76 VAL N N 15 120.663 0.2 . 1 . . . . 76 VAL H . 15936 5 140 . 1 1 76 76 VAL H H 1 8.089 0.02 . 1 . . . . 76 VAL N . 15936 5 141 . 1 1 77 77 THR N N 15 116.665 0.2 . 1 . . . . 77 THR H . 15936 5 142 . 1 1 77 77 THR H H 1 7.935 0.02 . 1 . . . . 77 THR N . 15936 5 143 . 1 1 78 78 ARG N N 15 122.155 0.2 . 1 . . . . 78 ARG H . 15936 5 144 . 1 1 78 78 ARG H H 1 8.144 0.02 . 1 . . . . 78 ARG N . 15936 5 145 . 1 1 79 79 GLU N N 15 116.687 0.2 . 1 . . . . 79 GLU H . 15936 5 146 . 1 1 79 79 GLU H H 1 7.959 0.02 . 1 . . . . 79 GLU N . 15936 5 147 . 1 1 80 80 ARG N N 15 121.609 0.2 . 1 . . . . 80 ARG H . 15936 5 148 . 1 1 80 80 ARG H H 1 8.228 0.02 . 1 . . . . 80 ARG N . 15936 5 149 . 1 1 81 81 ILE N N 15 121.085 0.2 . 1 . . . . 81 ILE H . 15936 5 150 . 1 1 81 81 ILE H H 1 8.032 0.02 . 1 . . . . 81 ILE N . 15936 5 151 . 1 1 82 82 ARG N N 15 121.072 0.2 . 1 . . . . 82 ARG H . 15936 5 152 . 1 1 82 82 ARG H H 1 7.999 0.02 . 1 . . . . 82 ARG N . 15936 5 153 . 1 1 83 83 GLN N N 15 121.261 0.2 . 1 . . . . 83 GLN H . 15936 5 154 . 1 1 83 83 GLN H H 1 8.242 0.02 . 1 . . . . 83 GLN N . 15936 5 155 . 1 1 84 84 ILE N N 15 121.417 0.2 . 1 . . . . 84 ILE H . 15936 5 156 . 1 1 84 84 ILE H H 1 8.107 0.02 . 1 . . . . 84 ILE N . 15936 5 157 . 1 1 85 85 GLU N N 15 120.649 0.2 . 1 . . . . 85 GLU H . 15936 5 158 . 1 1 85 85 GLU H H 1 8.382 0.02 . 1 . . . . 85 GLU N . 15936 5 159 . 1 1 86 86 ALA N N 15 122.085 0.2 . 1 . . . . 86 ALA H . 15936 5 160 . 1 1 86 86 ALA H H 1 8.110 0.02 . 1 . . . . 86 ALA N . 15936 5 161 . 1 1 87 87 LYS N N 15 118.157 0.2 . 1 . . . . 87 LYS H . 15936 5 162 . 1 1 87 87 LYS H H 1 7.833 0.02 . 1 . . . . 87 LYS N . 15936 5 163 . 1 1 88 88 ALA N N 15 122.450 0.2 . 1 . . . . 88 ALA H . 15936 5 164 . 1 1 88 88 ALA H H 1 7.926 0.02 . 1 . . . . 88 ALA N . 15936 5 165 . 1 1 89 89 LEU N N 15 120.962 0.2 . 1 . . . . 89 LEU H . 15936 5 166 . 1 1 89 89 LEU H H 1 8.014 0.02 . 1 . . . . 89 LEU N . 15936 5 167 . 1 1 90 90 ARG N N 15 121.068 0.2 . 1 . . . . 90 ARG H . 15936 5 168 . 1 1 90 90 ARG H H 1 8.134 0.02 . 1 . . . . 90 ARG N . 15936 5 169 . 1 1 91 91 LYS N N 15 121.824 0.2 . 1 . . . . 91 LYS H . 15936 5 170 . 1 1 91 91 LYS H H 1 8.109 0.02 . 1 . . . . 91 LYS N . 15936 5 171 . 1 1 92 92 LEU N N 15 121.256 0.2 . 1 . . . . 92 LEU H . 15936 5 172 . 1 1 92 92 LEU H H 1 7.853 0.02 . 1 . . . . 92 LEU N . 15936 5 173 . 1 1 93 93 ARG N N 15 121.376 0.2 . 1 . . . . 93 ARG H . 15936 5 174 . 1 1 93 93 ARG H H 1 8.247 0.02 . 1 . . . . 93 ARG N . 15936 5 175 . 1 1 94 94 HIS N N 15 118.892 0.2 . 1 . . . . 94 HIS H . 15936 5 176 . 1 1 94 94 HIS H H 1 8.383 0.02 . 1 . . . . 94 HIS N . 15936 5 177 . 1 1 96 96 SER N N 15 116.522 0.2 . 1 . . . . 96 SER H . 15936 5 178 . 1 1 96 96 SER H H 1 8.373 0.02 . 1 . . . . 96 SER N . 15936 5 179 . 1 1 97 97 ARG N N 15 122.659 0.2 . 1 . . . . 97 ARG H . 15936 5 180 . 1 1 97 97 ARG H H 1 8.542 0.02 . 1 . . . . 97 ARG N . 15936 5 181 . 1 1 98 98 SER N N 15 115.111 0.2 . 1 . . . . 98 SER H . 15936 5 182 . 1 1 98 98 SER H H 1 8.288 0.02 . 1 . . . . 98 SER N . 15936 5 183 . 1 1 99 99 GLU N N 15 122.090 0.2 . 1 . . . . 99 GLU H . 15936 5 184 . 1 1 99 99 GLU H H 1 8.110 0.02 . 1 . . . . 99 GLU N . 15936 5 185 . 1 1 100 100 VAL N N 15 120.662 0.2 . 1 . . . . 100 VAL H . 15936 5 186 . 1 1 100 100 VAL H H 1 8.026 0.02 . 1 . . . . 100 VAL N . 15936 5 187 . 1 1 101 101 LEU N N 15 123.767 0.2 . 1 . . . . 101 LEU H . 15936 5 188 . 1 1 101 101 LEU H H 1 8.142 0.02 . 1 . . . . 101 LEU N . 15936 5 189 . 1 1 102 102 ARG N N 15 121.662 0.2 . 1 . . . . 102 ARG H . 15936 5 190 . 1 1 102 102 ARG H H 1 8.216 0.02 . 1 . . . . 102 ARG N . 15936 5 191 . 1 1 103 103 SER N N 15 115.320 0.2 . 1 . . . . 103 SER H . 15936 5 192 . 1 1 103 103 SER H H 1 7.997 0.02 . 1 . . . . 103 SER N . 15936 5 193 . 1 1 104 104 PHE N N 15 121.755 0.2 . 1 . . . . 104 PHE H . 15936 5 194 . 1 1 104 104 PHE H H 1 8.149 0.02 . 1 . . . . 104 PHE N . 15936 5 195 . 1 1 105 105 LEU N N 15 120.984 0.2 . 1 . . . . 105 LEU H . 15936 5 196 . 1 1 105 105 LEU H H 1 7.913 0.02 . 1 . . . . 105 LEU N . 15936 5 197 . 1 1 106 106 ASP N N 15 118.372 0.2 . 1 . . . . 106 ASP H . 15936 5 198 . 1 1 106 106 ASP H H 1 8.118 0.02 . 1 . . . . 106 ASP N . 15936 5 199 . 1 1 107 107 ASP N N 15 122.296 0.2 . 1 . . . . 107 ASP H . 15936 5 200 . 1 1 107 107 ASP H H 1 7.883 0.02 . 1 . . . . 107 ASP N . 15936 5 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chem_shift_list_6 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chem_shift_list_6 _Assigned_chem_shift_list.Entry_ID 15936 _Assigned_chem_shift_list.ID 6 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_all _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err 0.02 _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err 0.2 _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details 'M1 is deleted in the expression system.' _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 6 '2D 1H-15N HSQC' . . . 15936 6 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 SER N N 15 114.966 0.2 . 1 . . . . 3 SER H . 15936 6 2 . 1 1 3 3 SER H H 1 8.307 0.02 . 1 . . . . 3 SER N . 15936 6 3 . 1 1 4 4 SER N N 15 116.760 0.2 . 1 . . . . 4 SER H . 15936 6 4 . 1 1 4 4 SER H H 1 8.274 0.02 . 1 . . . . 4 SER N . 15936 6 5 . 1 1 6 6 HIS N N 15 119.703 0.2 . 1 . . . . 6 HIS H . 15936 6 6 . 1 1 6 6 HIS H H 1 8.486 0.02 . 1 . . . . 6 HIS N . 15936 6 7 . 1 1 7 7 HIS N N 15 117.739 0.2 . 1 . . . . 7 HIS H . 15936 6 8 . 1 1 7 7 HIS H H 1 8.291 0.02 . 1 . . . . 7 HIS N . 15936 6 9 . 1 1 8 8 HIS N N 15 119.618 0.2 . 1 . . . . 8 HIS H . 15936 6 10 . 1 1 8 8 HIS H H 1 8.621 0.02 . 1 . . . . 8 HIS N . 15936 6 11 . 1 1 9 9 HIS N N 15 120.674 0.2 . 1 . . . . 9 HIS H . 15936 6 12 . 1 1 9 9 HIS H H 1 8.697 0.02 . 1 . . . . 9 HIS N . 15936 6 13 . 1 1 10 10 HIS N N 15 121.386 0.2 . 1 . . . . 10 HIS H . 15936 6 14 . 1 1 10 10 HIS H H 1 8.672 0.02 . 1 . . . . 10 HIS N . 15936 6 15 . 1 1 11 11 SER N N 15 118.616 0.2 . 1 . . . . 11 SER H . 15936 6 16 . 1 1 11 11 SER H H 1 8.474 0.02 . 1 . . . . 11 SER N . 15936 6 17 . 1 1 12 12 SER N N 15 118.197 0.2 . 1 . . . . 12 SER H . 15936 6 18 . 1 1 12 12 SER H H 1 8.498 0.02 . 1 . . . . 12 SER N . 15936 6 19 . 1 1 13 13 GLY N N 15 110.347 0.2 . 1 . . . . 13 GLY H . 15936 6 20 . 1 1 13 13 GLY H H 1 8.354 0.02 . 1 . . . . 13 GLY N . 15936 6 21 . 1 1 14 14 LEU N N 15 121.919 0.2 . 1 . . . . 14 LEU H . 15936 6 22 . 1 1 14 14 LEU H H 1 8.114 0.02 . 1 . . . . 14 LEU N . 15936 6 23 . 1 1 15 15 VAL N N 15 123.670 0.2 . 1 . . . . 15 VAL H . 15936 6 24 . 1 1 15 15 VAL H H 1 8.207 0.02 . 1 . . . . 15 VAL N . 15936 6 25 . 1 1 17 17 ARG N N 15 121.745 0.2 . 1 . . . . 17 ARG H . 15936 6 26 . 1 1 17 17 ARG H H 1 8.385 0.02 . 1 . . . . 17 ARG N . 15936 6 27 . 1 1 18 18 GLY N N 15 109.941 0.2 . 1 . . . . 18 GLY H . 15936 6 28 . 1 1 18 18 GLY H H 1 8.393 0.02 . 1 . . . . 18 GLY N . 15936 6 29 . 1 1 19 19 SER N N 15 115.013 0.2 . 1 . . . . 19 SER H . 15936 6 30 . 1 1 19 19 SER H H 1 8.108 0.02 . 1 . . . . 19 SER N . 15936 6 31 . 1 1 20 20 HIS N N 15 119.910 0.2 . 1 . . . . 20 HIS H . 15936 6 32 . 1 1 20 20 HIS H H 1 8.527 0.02 . 1 . . . . 20 HIS N . 15936 6 33 . 1 1 21 21 MET N N 15 120.920 0.2 . 1 . . . . 21 MET H . 15936 6 34 . 1 1 21 21 MET H H 1 8.281 0.02 . 1 . . . . 21 MET N . 15936 6 35 . 1 1 22 22 LEU N N 15 123.110 0.2 . 1 . . . . 22 LEU H . 15936 6 36 . 1 1 22 22 LEU H H 1 8.184 0.02 . 1 . . . . 22 LEU N . 15936 6 37 . 1 1 23 23 GLU N N 15 121.063 0.2 . 1 . . . . 23 GLU H . 15936 6 38 . 1 1 23 23 GLU H H 1 8.149 0.02 . 1 . . . . 23 GLU N . 15936 6 39 . 1 1 24 24 LEU N N 15 124.288 0.2 . 1 . . . . 24 LEU H . 15936 6 40 . 1 1 24 24 LEU H H 1 8.106 0.02 . 1 . . . . 24 LEU N . 15936 6 41 . 1 1 26 26 LEU N N 15 121.704 0.2 . 1 . . . . 26 LEU H . 15936 6 42 . 1 1 26 26 LEU H H 1 8.161 0.02 . 1 . . . . 26 LEU N . 15936 6 43 . 1 1 27 27 ASP N N 15 118.976 0.2 . 1 . . . . 27 ASP H . 15936 6 44 . 1 1 27 27 ASP H H 1 8.318 0.02 . 1 . . . . 27 ASP N . 15936 6 45 . 1 1 28 28 SER N N 15 116.200 0.2 . 1 . . . . 28 SER H . 15936 6 46 . 1 1 28 28 SER H H 1 8.206 0.02 . 1 . . . . 28 SER N . 15936 6 47 . 1 1 29 29 ALA N N 15 125.126 0.2 . 1 . . . . 29 ALA H . 15936 6 48 . 1 1 29 29 ALA H H 1 8.272 0.02 . 1 . . . . 29 ALA N . 15936 6 49 . 1 1 30 30 THR N N 15 112.628 0.2 . 1 . . . . 30 THR H . 15936 6 50 . 1 1 30 30 THR H H 1 8.046 0.02 . 1 . . . . 30 THR N . 15936 6 51 . 1 1 31 31 THR N N 15 115.781 0.2 . 1 . . . . 31 THR H . 15936 6 52 . 1 1 31 31 THR H H 1 8.035 0.02 . 1 . . . . 31 THR N . 15936 6 53 . 1 1 32 32 GLU N N 15 121.303 0.2 . 1 . . . . 32 GLU H . 15936 6 54 . 1 1 32 32 GLU H H 1 8.269 0.02 . 1 . . . . 32 GLU N . 15936 6 55 . 1 1 33 33 SER N N 15 116.157 0.2 . 1 . . . . 33 SER H . 15936 6 56 . 1 1 33 33 SER H H 1 8.149 0.02 . 1 . . . . 33 SER N . 15936 6 57 . 1 1 34 34 LEU N N 15 123.422 0.2 . 1 . . . . 34 LEU H . 15936 6 58 . 1 1 34 34 LEU H H 1 8.061 0.02 . 1 . . . . 34 LEU N . 15936 6 59 . 1 1 35 35 ARG N N 15 121.114 0.2 . 1 . . . . 35 ARG H . 15936 6 60 . 1 1 35 35 ARG H H 1 8.067 0.02 . 1 . . . . 35 ARG N . 15936 6 61 . 1 1 36 36 ALA N N 15 122.849 0.2 . 1 . . . . 36 ALA H . 15936 6 62 . 1 1 36 36 ALA H H 1 8.018 0.02 . 1 . . . . 36 ALA N . 15936 6 63 . 1 1 37 37 ALA N N 15 122.806 0.2 . 1 . . . . 37 ALA H . 15936 6 64 . 1 1 37 37 ALA H H 1 8.170 0.02 . 1 . . . . 37 ALA N . 15936 6 65 . 1 1 38 38 THR N N 15 111.164 0.2 . 1 . . . . 38 THR H . 15936 6 66 . 1 1 38 38 THR H H 1 7.914 0.02 . 1 . . . . 38 THR N . 15936 6 67 . 1 1 39 39 HIS N N 15 119.218 0.2 . 1 . . . . 39 HIS H . 15936 6 68 . 1 1 39 39 HIS H H 1 8.200 0.02 . 1 . . . . 39 HIS N . 15936 6 69 . 1 1 40 40 ASP N N 15 118.729 0.2 . 1 . . . . 40 ASP H . 15936 6 70 . 1 1 40 40 ASP H H 1 8.330 0.02 . 1 . . . . 40 ASP N . 15936 6 71 . 1 1 41 41 VAL N N 15 121.179 0.2 . 1 . . . . 41 VAL H . 15936 6 72 . 1 1 41 41 VAL H H 1 8.150 0.02 . 1 . . . . 41 VAL N . 15936 6 73 . 1 1 42 42 LEU N N 15 123.449 0.2 . 1 . . . . 42 LEU H . 15936 6 74 . 1 1 42 42 LEU H H 1 8.106 0.02 . 1 . . . . 42 LEU N . 15936 6 75 . 1 1 43 43 ALA N N 15 122.415 0.2 . 1 . . . . 43 ALA H . 15936 6 76 . 1 1 43 43 ALA H H 1 7.952 0.02 . 1 . . . . 43 ALA N . 15936 6 77 . 1 1 44 44 GLY N N 15 106.551 0.2 . 1 . . . . 44 GLY H . 15936 6 78 . 1 1 44 44 GLY H H 1 8.043 0.02 . 1 . . . . 44 GLY N . 15936 6 79 . 1 1 45 45 LEU N N 15 121.708 0.2 . 1 . . . . 45 LEU H . 15936 6 80 . 1 1 45 45 LEU H H 1 7.776 0.02 . 1 . . . . 45 LEU N . 15936 6 81 . 1 1 46 46 THR N N 15 113.256 0.2 . 1 . . . . 46 THR H . 15936 6 82 . 1 1 46 46 THR H H 1 7.955 0.02 . 1 . . . . 46 THR N . 15936 6 83 . 1 1 47 47 ALA N N 15 123.641 0.2 . 1 . . . . 47 ALA H . 15936 6 84 . 1 1 47 47 ALA H H 1 8.433 0.02 . 1 . . . . 47 ALA N . 15936 6 85 . 1 1 48 48 ARG N N 15 117.642 0.2 . 1 . . . . 48 ARG H . 15936 6 86 . 1 1 48 48 ARG H H 1 8.110 0.02 . 1 . . . . 48 ARG N . 15936 6 87 . 1 1 49 49 GLU N N 15 118.323 0.2 . 1 . . . . 49 GLU H . 15936 6 88 . 1 1 49 49 GLU H H 1 7.813 0.02 . 1 . . . . 49 GLU N . 15936 6 89 . 1 1 50 50 ALA N N 15 120.780 0.2 . 1 . . . . 50 ALA H . 15936 6 90 . 1 1 50 50 ALA H H 1 8.414 0.02 . 1 . . . . 50 ALA N . 15936 6 91 . 1 1 51 51 LYS N N 15 117.897 0.2 . 1 . . . . 51 LYS H . 15936 6 92 . 1 1 51 51 LYS H H 1 7.723 0.02 . 1 . . . . 51 LYS N . 15936 6 93 . 1 1 52 52 VAL N N 15 119.307 0.2 . 1 . . . . 52 VAL H . 15936 6 94 . 1 1 52 52 VAL H H 1 7.729 0.02 . 1 . . . . 52 VAL N . 15936 6 95 . 1 1 53 53 LEU N N 15 123.565 0.2 . 1 . . . . 53 LEU H . 15936 6 96 . 1 1 53 53 LEU H H 1 8.087 0.02 . 1 . . . . 53 LEU N . 15936 6 97 . 1 1 54 54 ARG N N 15 119.763 0.2 . 1 . . . . 54 ARG H . 15936 6 98 . 1 1 54 54 ARG H H 1 8.112 0.02 . 1 . . . . 54 ARG N . 15936 6 99 . 1 1 55 55 MET N N 15 120.668 0.2 . 1 . . . . 55 MET H . 15936 6 100 . 1 1 55 55 MET H H 1 8.135 0.02 . 1 . . . . 55 MET N . 15936 6 101 . 1 1 56 56 ARG N N 15 120.992 0.2 . 1 . . . . 56 ARG H . 15936 6 102 . 1 1 56 56 ARG H H 1 8.057 0.02 . 1 . . . . 56 ARG N . 15936 6 103 . 1 1 57 57 PHE N N 15 120.164 0.2 . 1 . . . . 57 PHE H . 15936 6 104 . 1 1 57 57 PHE H H 1 8.155 0.02 . 1 . . . . 57 PHE N . 15936 6 105 . 1 1 58 58 GLY N N 15 108.827 0.2 . 1 . . . . 58 GLY H . 15936 6 106 . 1 1 58 58 GLY H H 1 7.902 0.02 . 1 . . . . 58 GLY N . 15936 6 107 . 1 1 59 59 ILE N N 15 118.868 0.2 . 1 . . . . 59 ILE H . 15936 6 108 . 1 1 59 59 ILE H H 1 7.744 0.02 . 1 . . . . 59 ILE N . 15936 6 109 . 1 1 60 60 ASP N N 15 121.963 0.2 . 1 . . . . 60 ASP H . 15936 6 110 . 1 1 60 60 ASP H H 1 8.405 0.02 . 1 . . . . 60 ASP N . 15936 6 111 . 1 1 61 61 MET N N 15 120.324 0.2 . 1 . . . . 61 MET H . 15936 6 112 . 1 1 61 61 MET H H 1 8.228 0.02 . 1 . . . . 61 MET N . 15936 6 113 . 1 1 62 62 ASN N N 15 118.400 0.2 . 1 . . . . 62 ASN H . 15936 6 114 . 1 1 62 62 ASN H H 1 8.234 0.02 . 1 . . . . 62 ASN N . 15936 6 115 . 1 1 63 63 THR N N 15 113.964 0.2 . 1 . . . . 63 THR H . 15936 6 116 . 1 1 63 63 THR H H 1 7.962 0.02 . 1 . . . . 63 THR N . 15936 6 117 . 1 1 64 64 ASP N N 15 120.393 0.2 . 1 . . . . 64 ASP H . 15936 6 118 . 1 1 64 64 ASP H H 1 8.306 0.02 . 1 . . . . 64 ASP N . 15936 6 119 . 1 1 65 65 TYR N N 15 120.864 0.2 . 1 . . . . 65 TYR H . 15936 6 120 . 1 1 65 65 TYR H H 1 8.033 0.02 . 1 . . . . 65 TYR N . 15936 6 121 . 1 1 66 66 THR N N 15 113.795 0.2 . 1 . . . . 66 THR H . 15936 6 122 . 1 1 66 66 THR H H 1 7.856 0.02 . 1 . . . . 66 THR N . 15936 6 123 . 1 1 67 67 LEU N N 15 123.084 0.2 . 1 . . . . 67 LEU H . 15936 6 124 . 1 1 67 67 LEU H H 1 8.008 0.02 . 1 . . . . 67 LEU N . 15936 6 125 . 1 1 68 68 GLU N N 15 120.412 0.2 . 1 . . . . 68 GLU H . 15936 6 126 . 1 1 68 68 GLU H H 1 8.108 0.02 . 1 . . . . 68 GLU N . 15936 6 127 . 1 1 69 69 GLU N N 15 120.533 0.2 . 1 . . . . 69 GLU H . 15936 6 128 . 1 1 69 69 GLU H H 1 8.125 0.02 . 1 . . . . 69 GLU N . 15936 6 129 . 1 1 70 70 VAL N N 15 120.367 0.2 . 1 . . . . 70 VAL H . 15936 6 130 . 1 1 70 70 VAL H H 1 8.024 0.02 . 1 . . . . 70 VAL N . 15936 6 131 . 1 1 71 71 GLY N N 15 108.834 0.2 . 1 . . . . 71 GLY H . 15936 6 132 . 1 1 71 71 GLY H H 1 8.258 0.02 . 1 . . . . 71 GLY N . 15936 6 133 . 1 1 72 72 LYS N N 15 120.799 0.2 . 1 . . . . 72 LYS H . 15936 6 134 . 1 1 72 72 LYS H H 1 8.105 0.02 . 1 . . . . 72 LYS N . 15936 6 135 . 1 1 73 73 GLN N N 15 118.307 0.2 . 1 . . . . 73 GLN H . 15936 6 136 . 1 1 73 73 GLN H H 1 8.197 0.02 . 1 . . . . 73 GLN N . 15936 6 137 . 1 1 75 75 ASP N N 15 119.496 0.2 . 1 . . . . 75 ASP H . 15936 6 138 . 1 1 75 75 ASP H H 1 8.177 0.02 . 1 . . . . 75 ASP N . 15936 6 139 . 1 1 76 76 VAL N N 15 120.663 0.2 . 1 . . . . 76 VAL H . 15936 6 140 . 1 1 76 76 VAL H H 1 8.089 0.02 . 1 . . . . 76 VAL N . 15936 6 141 . 1 1 77 77 THR N N 15 116.804 0.2 . 1 . . . . 77 THR H . 15936 6 142 . 1 1 77 77 THR H H 1 7.895 0.02 . 1 . . . . 77 THR N . 15936 6 143 . 1 1 78 78 ARG N N 15 122.155 0.2 . 1 . . . . 78 ARG H . 15936 6 144 . 1 1 78 78 ARG H H 1 8.144 0.02 . 1 . . . . 78 ARG N . 15936 6 145 . 1 1 79 79 GLU N N 15 115.982 0.2 . 1 . . . . 79 GLU H . 15936 6 146 . 1 1 79 79 GLU H H 1 7.937 0.02 . 1 . . . . 79 GLU N . 15936 6 147 . 1 1 80 80 ARG N N 15 121.609 0.2 . 1 . . . . 80 ARG H . 15936 6 148 . 1 1 80 80 ARG H H 1 8.228 0.02 . 1 . . . . 80 ARG N . 15936 6 149 . 1 1 81 81 ILE N N 15 121.221 0.2 . 1 . . . . 81 ILE H . 15936 6 150 . 1 1 81 81 ILE H H 1 8.039 0.02 . 1 . . . . 81 ILE N . 15936 6 151 . 1 1 82 82 ARG N N 15 123.581 0.2 . 1 . . . . 82 ARG H . 15936 6 152 . 1 1 82 82 ARG H H 1 8.219 0.02 . 1 . . . . 82 ARG N . 15936 6 153 . 1 1 83 83 GLN N N 15 121.261 0.2 . 1 . . . . 83 GLN H . 15936 6 154 . 1 1 83 83 GLN H H 1 8.242 0.02 . 1 . . . . 83 GLN N . 15936 6 155 . 1 1 84 84 ILE N N 15 121.238 0.2 . 1 . . . . 84 ILE H . 15936 6 156 . 1 1 84 84 ILE H H 1 8.076 0.02 . 1 . . . . 84 ILE N . 15936 6 157 . 1 1 85 85 GLU N N 15 119.910 0.2 . 1 . . . . 85 GLU H . 15936 6 158 . 1 1 85 85 GLU H H 1 8.444 0.02 . 1 . . . . 85 GLU N . 15936 6 159 . 1 1 86 86 ALA N N 15 122.920 0.2 . 1 . . . . 86 ALA H . 15936 6 160 . 1 1 86 86 ALA H H 1 8.091 0.02 . 1 . . . . 86 ALA N . 15936 6 161 . 1 1 87 87 LYS N N 15 117.683 0.2 . 1 . . . . 87 LYS H . 15936 6 162 . 1 1 87 87 LYS H H 1 7.759 0.02 . 1 . . . . 87 LYS N . 15936 6 163 . 1 1 88 88 ALA N N 15 122.161 0.2 . 1 . . . . 88 ALA H . 15936 6 164 . 1 1 88 88 ALA H H 1 7.954 0.02 . 1 . . . . 88 ALA N . 15936 6 165 . 1 1 89 89 LEU N N 15 120.962 0.2 . 1 . . . . 89 LEU H . 15936 6 166 . 1 1 89 89 LEU H H 1 8.014 0.02 . 1 . . . . 89 LEU N . 15936 6 167 . 1 1 90 90 ARG N N 15 121.068 0.2 . 1 . . . . 90 ARG H . 15936 6 168 . 1 1 90 90 ARG H H 1 8.134 0.02 . 1 . . . . 90 ARG N . 15936 6 169 . 1 1 91 91 LYS N N 15 121.824 0.2 . 1 . . . . 91 LYS H . 15936 6 170 . 1 1 91 91 LYS H H 1 8.109 0.02 . 1 . . . . 91 LYS N . 15936 6 171 . 1 1 92 92 LEU N N 15 120.460 0.2 . 1 . . . . 92 LEU H . 15936 6 172 . 1 1 92 92 LEU H H 1 7.781 0.02 . 1 . . . . 92 LEU N . 15936 6 173 . 1 1 93 93 ARG N N 15 121.376 0.2 . 1 . . . . 93 ARG H . 15936 6 174 . 1 1 93 93 ARG H H 1 8.247 0.02 . 1 . . . . 93 ARG N . 15936 6 175 . 1 1 94 94 HIS N N 15 118.409 0.2 . 1 . . . . 94 HIS H . 15936 6 176 . 1 1 94 94 HIS H H 1 8.338 0.02 . 1 . . . . 94 HIS N . 15936 6 177 . 1 1 96 96 SER N N 15 116.256 0.2 . 1 . . . . 96 SER H . 15936 6 178 . 1 1 96 96 SER H H 1 8.305 0.02 . 1 . . . . 96 SER N . 15936 6 179 . 1 1 97 97 ARG N N 15 122.589 0.2 . 1 . . . . 97 ARG H . 15936 6 180 . 1 1 97 97 ARG H H 1 8.574 0.02 . 1 . . . . 97 ARG N . 15936 6 181 . 1 1 98 98 SER N N 15 114.470 0.2 . 1 . . . . 98 SER H . 15936 6 182 . 1 1 98 98 SER H H 1 8.271 0.02 . 1 . . . . 98 SER N . 15936 6 183 . 1 1 99 99 GLU N N 15 121.908 0.2 . 1 . . . . 99 GLU H . 15936 6 184 . 1 1 99 99 GLU H H 1 8.025 0.02 . 1 . . . . 99 GLU N . 15936 6 185 . 1 1 100 100 VAL N N 15 120.535 0.2 . 1 . . . . 100 VAL H . 15936 6 186 . 1 1 100 100 VAL H H 1 7.992 0.02 . 1 . . . . 100 VAL N . 15936 6 187 . 1 1 101 101 LEU N N 15 124.281 0.2 . 1 . . . . 101 LEU H . 15936 6 188 . 1 1 101 101 LEU H H 1 8.106 0.02 . 1 . . . . 101 LEU N . 15936 6 189 . 1 1 102 102 ARG N N 15 121.662 0.2 . 1 . . . . 102 ARG H . 15936 6 190 . 1 1 102 102 ARG H H 1 8.216 0.02 . 1 . . . . 102 ARG N . 15936 6 191 . 1 1 103 103 SER N N 15 114.928 0.2 . 1 . . . . 103 SER H . 15936 6 192 . 1 1 103 103 SER H H 1 7.936 0.02 . 1 . . . . 103 SER N . 15936 6 193 . 1 1 104 104 PHE N N 15 121.755 0.2 . 1 . . . . 104 PHE H . 15936 6 194 . 1 1 104 104 PHE H H 1 8.149 0.02 . 1 . . . . 104 PHE N . 15936 6 195 . 1 1 105 105 LEU N N 15 120.337 0.2 . 1 . . . . 105 LEU H . 15936 6 196 . 1 1 105 105 LEU H H 1 7.883 0.02 . 1 . . . . 105 LEU N . 15936 6 197 . 1 1 106 106 ASP N N 15 117.976 0.2 . 1 . . . . 106 ASP H . 15936 6 198 . 1 1 106 106 ASP H H 1 8.059 0.02 . 1 . . . . 106 ASP N . 15936 6 199 . 1 1 107 107 ASP N N 15 122.157 0.2 . 1 . . . . 107 ASP H . 15936 6 200 . 1 1 107 107 ASP H H 1 7.867 0.02 . 1 . . . . 107 ASP N . 15936 6 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chem_shift_list_7 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chem_shift_list_7 _Assigned_chem_shift_list.Entry_ID 15936 _Assigned_chem_shift_list.ID 7 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_all _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err 0.02 _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err 0.2 _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details 'M1 is deleted in the expression system.' _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 7 '2D 1H-15N HSQC' . . . 15936 7 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 SER N N 15 114.943 0.2 . 1 . . . . 3 SER H . 15936 7 2 . 1 1 3 3 SER H H 1 8.303 0.02 . 1 . . . . 3 SER N . 15936 7 3 . 1 1 4 4 SER N N 15 116.697 0.2 . 1 . . . . 4 SER H . 15936 7 4 . 1 1 4 4 SER H H 1 8.272 0.02 . 1 . . . . 4 SER N . 15936 7 5 . 1 1 6 6 HIS N N 15 119.619 0.2 . 1 . . . . 6 HIS H . 15936 7 6 . 1 1 6 6 HIS H H 1 8.484 0.02 . 1 . . . . 6 HIS N . 15936 7 7 . 1 1 7 7 HIS N N 15 117.670 0.2 . 1 . . . . 7 HIS H . 15936 7 8 . 1 1 7 7 HIS H H 1 8.281 0.02 . 1 . . . . 7 HIS N . 15936 7 9 . 1 1 8 8 HIS N N 15 119.525 0.2 . 1 . . . . 8 HIS H . 15936 7 10 . 1 1 8 8 HIS H H 1 8.614 0.02 . 1 . . . . 8 HIS N . 15936 7 11 . 1 1 9 9 HIS N N 15 120.559 0.2 . 1 . . . . 9 HIS H . 15936 7 12 . 1 1 9 9 HIS H H 1 8.693 0.02 . 1 . . . . 9 HIS N . 15936 7 13 . 1 1 10 10 HIS N N 15 121.276 0.2 . 1 . . . . 10 HIS H . 15936 7 14 . 1 1 10 10 HIS H H 1 8.667 0.02 . 1 . . . . 10 HIS N . 15936 7 15 . 1 1 11 11 SER N N 15 118.501 0.2 . 1 . . . . 11 SER H . 15936 7 16 . 1 1 11 11 SER H H 1 8.468 0.02 . 1 . . . . 11 SER N . 15936 7 17 . 1 1 12 12 SER N N 15 118.135 0.2 . 1 . . . . 12 SER H . 15936 7 18 . 1 1 12 12 SER H H 1 8.487 0.02 . 1 . . . . 12 SER N . 15936 7 19 . 1 1 13 13 GLY N N 15 110.278 0.2 . 1 . . . . 13 GLY H . 15936 7 20 . 1 1 13 13 GLY H H 1 8.347 0.02 . 1 . . . . 13 GLY N . 15936 7 21 . 1 1 14 14 LEU N N 15 121.919 0.2 . 1 . . . . 14 LEU H . 15936 7 22 . 1 1 14 14 LEU H H 1 8.114 0.02 . 1 . . . . 14 LEU N . 15936 7 23 . 1 1 15 15 VAL N N 15 123.670 0.2 . 1 . . . . 15 VAL H . 15936 7 24 . 1 1 15 15 VAL H H 1 8.207 0.02 . 1 . . . . 15 VAL N . 15936 7 25 . 1 1 17 17 ARG N N 15 121.664 0.2 . 1 . . . . 17 ARG H . 15936 7 26 . 1 1 17 17 ARG H H 1 8.364 0.02 . 1 . . . . 17 ARG N . 15936 7 27 . 1 1 18 18 GLY N N 15 109.837 0.2 . 1 . . . . 18 GLY H . 15936 7 28 . 1 1 18 18 GLY H H 1 8.385 0.02 . 1 . . . . 18 GLY N . 15936 7 29 . 1 1 19 19 SER N N 15 114.927 0.2 . 1 . . . . 19 SER H . 15936 7 30 . 1 1 19 19 SER H H 1 8.093 0.02 . 1 . . . . 19 SER N . 15936 7 31 . 1 1 20 20 HIS N N 15 119.823 0.2 . 1 . . . . 20 HIS H . 15936 7 32 . 1 1 20 20 HIS H H 1 8.514 0.02 . 1 . . . . 20 HIS N . 15936 7 33 . 1 1 21 21 MET N N 15 120.732 0.2 . 1 . . . . 21 MET H . 15936 7 34 . 1 1 21 21 MET H H 1 8.264 0.02 . 1 . . . . 21 MET N . 15936 7 35 . 1 1 22 22 LEU N N 15 122.864 0.2 . 1 . . . . 22 LEU H . 15936 7 36 . 1 1 22 22 LEU H H 1 8.147 0.02 . 1 . . . . 22 LEU N . 15936 7 37 . 1 1 23 23 GLU N N 15 120.861 0.2 . 1 . . . . 23 GLU H . 15936 7 38 . 1 1 23 23 GLU H H 1 8.109 0.02 . 1 . . . . 23 GLU N . 15936 7 39 . 1 1 24 24 LEU N N 15 123.947 0.2 . 1 . . . . 24 LEU H . 15936 7 40 . 1 1 24 24 LEU H H 1 8.058 0.02 . 1 . . . . 24 LEU N . 15936 7 41 . 1 1 26 26 LEU N N 15 121.476 0.2 . 1 . . . . 26 LEU H . 15936 7 42 . 1 1 26 26 LEU H H 1 8.099 0.02 . 1 . . . . 26 LEU N . 15936 7 43 . 1 1 27 27 ASP N N 15 118.817 0.2 . 1 . . . . 27 ASP H . 15936 7 44 . 1 1 27 27 ASP H H 1 8.287 0.02 . 1 . . . . 27 ASP N . 15936 7 45 . 1 1 28 28 SER N N 15 116.166 0.2 . 1 . . . . 28 SER H . 15936 7 46 . 1 1 28 28 SER H H 1 8.216 0.02 . 1 . . . . 28 SER N . 15936 7 47 . 1 1 29 29 ALA N N 15 124.999 0.2 . 1 . . . . 29 ALA H . 15936 7 48 . 1 1 29 29 ALA H H 1 8.263 0.02 . 1 . . . . 29 ALA N . 15936 7 49 . 1 1 30 30 THR N N 15 112.747 0.2 . 1 . . . . 30 THR H . 15936 7 50 . 1 1 30 30 THR H H 1 8.052 0.02 . 1 . . . . 30 THR N . 15936 7 51 . 1 1 31 31 THR N N 15 115.714 0.2 . 1 . . . . 31 THR H . 15936 7 52 . 1 1 31 31 THR H H 1 8.041 0.02 . 1 . . . . 31 THR N . 15936 7 53 . 1 1 32 32 GLU N N 15 121.092 0.2 . 1 . . . . 32 GLU H . 15936 7 54 . 1 1 32 32 GLU H H 1 8.266 0.02 . 1 . . . . 32 GLU N . 15936 7 55 . 1 1 33 33 SER N N 15 116.082 0.2 . 1 . . . . 33 SER H . 15936 7 56 . 1 1 33 33 SER H H 1 8.131 0.02 . 1 . . . . 33 SER N . 15936 7 57 . 1 1 34 34 LEU N N 15 123.358 0.2 . 1 . . . . 34 LEU H . 15936 7 58 . 1 1 34 34 LEU H H 1 8.066 0.02 . 1 . . . . 34 LEU N . 15936 7 59 . 1 1 35 35 ARG N N 15 121.114 0.2 . 1 . . . . 35 ARG H . 15936 7 60 . 1 1 35 35 ARG H H 1 8.067 0.02 . 1 . . . . 35 ARG N . 15936 7 61 . 1 1 36 36 ALA N N 15 122.491 0.2 . 1 . . . . 36 ALA H . 15936 7 62 . 1 1 36 36 ALA H H 1 8.018 0.02 . 1 . . . . 36 ALA N . 15936 7 63 . 1 1 37 37 ALA N N 15 122.806 0.2 . 1 . . . . 37 ALA H . 15936 7 64 . 1 1 37 37 ALA H H 1 8.170 0.02 . 1 . . . . 37 ALA N . 15936 7 65 . 1 1 38 38 THR N N 15 111.066 0.2 . 1 . . . . 38 THR H . 15936 7 66 . 1 1 38 38 THR H H 1 7.951 0.02 . 1 . . . . 38 THR N . 15936 7 67 . 1 1 39 39 HIS N N 15 119.311 0.2 . 1 . . . . 39 HIS H . 15936 7 68 . 1 1 39 39 HIS H H 1 8.196 0.02 . 1 . . . . 39 HIS N . 15936 7 69 . 1 1 40 40 ASP N N 15 118.304 0.2 . 1 . . . . 40 ASP H . 15936 7 70 . 1 1 40 40 ASP H H 1 8.223 0.02 . 1 . . . . 40 ASP N . 15936 7 71 . 1 1 41 41 VAL N N 15 121.179 0.2 . 1 . . . . 41 VAL H . 15936 7 72 . 1 1 41 41 VAL H H 1 8.150 0.02 . 1 . . . . 41 VAL N . 15936 7 73 . 1 1 42 42 LEU N N 15 123.449 0.2 . 1 . . . . 42 LEU H . 15936 7 74 . 1 1 42 42 LEU H H 1 8.106 0.02 . 1 . . . . 42 LEU N . 15936 7 75 . 1 1 43 43 ALA N N 15 123.639 0.2 . 1 . . . . 43 ALA H . 15936 7 76 . 1 1 43 43 ALA H H 1 8.002 0.02 . 1 . . . . 43 ALA N . 15936 7 77 . 1 1 44 44 GLY N N 15 106.320 0.2 . 1 . . . . 44 GLY H . 15936 7 78 . 1 1 44 44 GLY H H 1 7.989 0.02 . 1 . . . . 44 GLY N . 15936 7 79 . 1 1 45 45 LEU N N 15 122.020 0.2 . 1 . . . . 45 LEU H . 15936 7 80 . 1 1 45 45 LEU H H 1 7.854 0.02 . 1 . . . . 45 LEU N . 15936 7 81 . 1 1 46 46 THR N N 15 113.368 0.2 . 1 . . . . 46 THR H . 15936 7 82 . 1 1 46 46 THR H H 1 7.973 0.02 . 1 . . . . 46 THR N . 15936 7 83 . 1 1 47 47 ALA N N 15 123.480 0.2 . 1 . . . . 47 ALA H . 15936 7 84 . 1 1 47 47 ALA H H 1 8.341 0.02 . 1 . . . . 47 ALA N . 15936 7 85 . 1 1 48 48 ARG N N 15 118.222 0.2 . 1 . . . . 48 ARG H . 15936 7 86 . 1 1 48 48 ARG H H 1 8.165 0.02 . 1 . . . . 48 ARG N . 15936 7 87 . 1 1 49 49 GLU N N 15 117.919 0.2 . 1 . . . . 49 GLU H . 15936 7 88 . 1 1 49 49 GLU H H 1 7.658 0.02 . 1 . . . . 49 GLU N . 15936 7 89 . 1 1 50 50 ALA N N 15 120.494 0.2 . 1 . . . . 50 ALA H . 15936 7 90 . 1 1 50 50 ALA H H 1 8.391 0.02 . 1 . . . . 50 ALA N . 15936 7 91 . 1 1 51 51 LYS N N 15 117.712 0.2 . 1 . . . . 51 LYS H . 15936 7 92 . 1 1 51 51 LYS H H 1 7.699 0.02 . 1 . . . . 51 LYS N . 15936 7 93 . 1 1 52 52 VAL N N 15 119.340 0.2 . 1 . . . . 52 VAL H . 15936 7 94 . 1 1 52 52 VAL H H 1 7.765 0.02 . 1 . . . . 52 VAL N . 15936 7 95 . 1 1 53 53 LEU N N 15 123.565 0.2 . 1 . . . . 53 LEU H . 15936 7 96 . 1 1 53 53 LEU H H 1 8.087 0.02 . 1 . . . . 53 LEU N . 15936 7 97 . 1 1 54 54 ARG N N 15 119.763 0.2 . 1 . . . . 54 ARG H . 15936 7 98 . 1 1 54 54 ARG H H 1 8.112 0.02 . 1 . . . . 54 ARG N . 15936 7 99 . 1 1 55 55 MET N N 15 120.668 0.2 . 1 . . . . 55 MET H . 15936 7 100 . 1 1 55 55 MET H H 1 8.135 0.02 . 1 . . . . 55 MET N . 15936 7 101 . 1 1 56 56 ARG N N 15 120.992 0.2 . 1 . . . . 56 ARG H . 15936 7 102 . 1 1 56 56 ARG H H 1 8.057 0.02 . 1 . . . . 56 ARG N . 15936 7 103 . 1 1 57 57 PHE N N 15 120.164 0.2 . 1 . . . . 57 PHE H . 15936 7 104 . 1 1 57 57 PHE H H 1 8.155 0.02 . 1 . . . . 57 PHE N . 15936 7 105 . 1 1 58 58 GLY N N 15 108.622 0.2 . 1 . . . . 58 GLY H . 15936 7 106 . 1 1 58 58 GLY H H 1 7.904 0.02 . 1 . . . . 58 GLY N . 15936 7 107 . 1 1 59 59 ILE N N 15 118.369 0.2 . 1 . . . . 59 ILE H . 15936 7 108 . 1 1 59 59 ILE H H 1 7.700 0.02 . 1 . . . . 59 ILE N . 15936 7 109 . 1 1 60 60 ASP N N 15 121.864 0.2 . 1 . . . . 60 ASP H . 15936 7 110 . 1 1 60 60 ASP H H 1 8.385 0.02 . 1 . . . . 60 ASP N . 15936 7 111 . 1 1 61 61 MET N N 15 120.185 0.2 . 1 . . . . 61 MET H . 15936 7 112 . 1 1 61 61 MET H H 1 8.227 0.02 . 1 . . . . 61 MET N . 15936 7 113 . 1 1 62 62 ASN N N 15 118.192 0.2 . 1 . . . . 62 ASN H . 15936 7 114 . 1 1 62 62 ASN H H 1 8.235 0.02 . 1 . . . . 62 ASN N . 15936 7 115 . 1 1 63 63 THR N N 15 114.392 0.2 . 1 . . . . 63 THR H . 15936 7 116 . 1 1 63 63 THR H H 1 7.999 0.02 . 1 . . . . 63 THR N . 15936 7 117 . 1 1 64 64 ASP N N 15 120.304 0.2 . 1 . . . . 64 ASP H . 15936 7 118 . 1 1 64 64 ASP H H 1 8.306 0.02 . 1 . . . . 64 ASP N . 15936 7 119 . 1 1 65 65 TYR N N 15 120.864 0.2 . 1 . . . . 65 TYR H . 15936 7 120 . 1 1 65 65 TYR H H 1 8.033 0.02 . 1 . . . . 65 TYR N . 15936 7 121 . 1 1 66 66 THR N N 15 113.996 0.2 . 1 . . . . 66 THR H . 15936 7 122 . 1 1 66 66 THR H H 1 7.862 0.02 . 1 . . . . 66 THR N . 15936 7 123 . 1 1 67 67 LEU N N 15 123.084 0.2 . 1 . . . . 67 LEU H . 15936 7 124 . 1 1 67 67 LEU H H 1 8.008 0.02 . 1 . . . . 67 LEU N . 15936 7 125 . 1 1 68 68 GLU N N 15 120.412 0.2 . 1 . . . . 68 GLU H . 15936 7 126 . 1 1 68 68 GLU H H 1 8.108 0.02 . 1 . . . . 68 GLU N . 15936 7 127 . 1 1 69 69 GLU N N 15 120.533 0.2 . 1 . . . . 69 GLU H . 15936 7 128 . 1 1 69 69 GLU H H 1 8.125 0.02 . 1 . . . . 69 GLU N . 15936 7 129 . 1 1 70 70 VAL N N 15 120.367 0.2 . 1 . . . . 70 VAL H . 15936 7 130 . 1 1 70 70 VAL H H 1 8.024 0.02 . 1 . . . . 70 VAL N . 15936 7 131 . 1 1 71 71 GLY N N 15 108.143 0.2 . 1 . . . . 71 GLY H . 15936 7 132 . 1 1 71 71 GLY H H 1 8.244 0.02 . 1 . . . . 71 GLY N . 15936 7 133 . 1 1 72 72 LYS N N 15 120.799 0.2 . 1 . . . . 72 LYS H . 15936 7 134 . 1 1 72 72 LYS H H 1 8.105 0.02 . 1 . . . . 72 LYS N . 15936 7 135 . 1 1 73 73 GLN N N 15 117.935 0.2 . 1 . . . . 73 GLN H . 15936 7 136 . 1 1 73 73 GLN H H 1 8.059 0.02 . 1 . . . . 73 GLN N . 15936 7 137 . 1 1 75 75 ASP N N 15 119.086 0.2 . 1 . . . . 75 ASP H . 15936 7 138 . 1 1 75 75 ASP H H 1 8.165 0.02 . 1 . . . . 75 ASP N . 15936 7 139 . 1 1 76 76 VAL N N 15 120.663 0.2 . 1 . . . . 76 VAL H . 15936 7 140 . 1 1 76 76 VAL H H 1 8.089 0.02 . 1 . . . . 76 VAL N . 15936 7 141 . 1 1 77 77 THR N N 15 116.986 0.2 . 1 . . . . 77 THR H . 15936 7 142 . 1 1 77 77 THR H H 1 7.909 0.02 . 1 . . . . 77 THR N . 15936 7 143 . 1 1 78 78 ARG N N 15 122.155 0.2 . 1 . . . . 78 ARG H . 15936 7 144 . 1 1 78 78 ARG H H 1 8.144 0.02 . 1 . . . . 78 ARG N . 15936 7 145 . 1 1 79 79 GLU N N 15 115.942 0.2 . 1 . . . . 79 GLU H . 15936 7 146 . 1 1 79 79 GLU H H 1 7.970 0.02 . 1 . . . . 79 GLU N . 15936 7 147 . 1 1 80 80 ARG N N 15 121.609 0.2 . 1 . . . . 80 ARG H . 15936 7 148 . 1 1 80 80 ARG H H 1 8.228 0.02 . 1 . . . . 80 ARG N . 15936 7 149 . 1 1 81 81 ILE N N 15 121.221 0.2 . 1 . . . . 81 ILE H . 15936 7 150 . 1 1 81 81 ILE H H 1 8.039 0.02 . 1 . . . . 81 ILE N . 15936 7 151 . 1 1 82 82 ARG N N 15 123.581 0.2 . 1 . . . . 82 ARG H . 15936 7 152 . 1 1 82 82 ARG H H 1 8.219 0.02 . 1 . . . . 82 ARG N . 15936 7 153 . 1 1 83 83 GLN N N 15 121.261 0.2 . 1 . . . . 83 GLN H . 15936 7 154 . 1 1 83 83 GLN H H 1 8.242 0.02 . 1 . . . . 83 GLN N . 15936 7 155 . 1 1 84 84 ILE N N 15 122.410 0.2 . 1 . . . . 84 ILE H . 15936 7 156 . 1 1 84 84 ILE H H 1 8.191 0.02 . 1 . . . . 84 ILE N . 15936 7 157 . 1 1 85 85 GLU N N 15 119.540 0.2 . 1 . . . . 85 GLU H . 15936 7 158 . 1 1 85 85 GLU H H 1 8.494 0.02 . 1 . . . . 85 GLU N . 15936 7 159 . 1 1 86 86 ALA N N 15 122.628 0.2 . 1 . . . . 86 ALA H . 15936 7 160 . 1 1 86 86 ALA H H 1 8.055 0.02 . 1 . . . . 86 ALA N . 15936 7 161 . 1 1 87 87 LYS N N 15 117.487 0.2 . 1 . . . . 87 LYS H . 15936 7 162 . 1 1 87 87 LYS H H 1 7.734 0.02 . 1 . . . . 87 LYS N . 15936 7 163 . 1 1 88 88 ALA N N 15 122.115 0.2 . 1 . . . . 88 ALA H . 15936 7 164 . 1 1 88 88 ALA H H 1 8.025 0.02 . 1 . . . . 88 ALA N . 15936 7 165 . 1 1 89 89 LEU N N 15 120.962 0.2 . 1 . . . . 89 LEU H . 15936 7 166 . 1 1 89 89 LEU H H 1 8.014 0.02 . 1 . . . . 89 LEU N . 15936 7 167 . 1 1 90 90 ARG N N 15 121.068 0.2 . 1 . . . . 90 ARG H . 15936 7 168 . 1 1 90 90 ARG H H 1 8.134 0.02 . 1 . . . . 90 ARG N . 15936 7 169 . 1 1 91 91 LYS N N 15 121.824 0.2 . 1 . . . . 91 LYS H . 15936 7 170 . 1 1 91 91 LYS H H 1 8.109 0.02 . 1 . . . . 91 LYS N . 15936 7 171 . 1 1 92 92 LEU N N 15 119.977 0.2 . 1 . . . . 92 LEU H . 15936 7 172 . 1 1 92 92 LEU H H 1 7.753 0.02 . 1 . . . . 92 LEU N . 15936 7 173 . 1 1 93 93 ARG N N 15 121.376 0.2 . 1 . . . . 93 ARG H . 15936 7 174 . 1 1 93 93 ARG H H 1 8.247 0.02 . 1 . . . . 93 ARG N . 15936 7 175 . 1 1 94 94 HIS N N 15 118.216 0.2 . 1 . . . . 94 HIS H . 15936 7 176 . 1 1 94 94 HIS H H 1 8.302 0.02 . 1 . . . . 94 HIS N . 15936 7 177 . 1 1 96 96 SER N N 15 116.071 0.2 . 1 . . . . 96 SER H . 15936 7 178 . 1 1 96 96 SER H H 1 8.263 0.02 . 1 . . . . 96 SER N . 15936 7 179 . 1 1 97 97 ARG N N 15 122.563 0.2 . 1 . . . . 97 ARG H . 15936 7 180 . 1 1 97 97 ARG H H 1 8.596 0.02 . 1 . . . . 97 ARG N . 15936 7 181 . 1 1 98 98 SER N N 15 113.996 0.2 . 1 . . . . 98 SER H . 15936 7 182 . 1 1 98 98 SER H H 1 8.260 0.02 . 1 . . . . 98 SER N . 15936 7 183 . 1 1 99 99 GLU N N 15 121.770 0.2 . 1 . . . . 99 GLU H . 15936 7 184 . 1 1 99 99 GLU H H 1 7.971 0.02 . 1 . . . . 99 GLU N . 15936 7 185 . 1 1 100 100 VAL N N 15 120.394 0.2 . 1 . . . . 100 VAL H . 15936 7 186 . 1 1 100 100 VAL H H 1 7.968 0.02 . 1 . . . . 100 VAL N . 15936 7 187 . 1 1 101 101 LEU N N 15 123.944 0.2 . 1 . . . . 101 LEU H . 15936 7 188 . 1 1 101 101 LEU H H 1 8.058 0.02 . 1 . . . . 101 LEU N . 15936 7 189 . 1 1 102 102 ARG N N 15 121.662 0.2 . 1 . . . . 102 ARG H . 15936 7 190 . 1 1 102 102 ARG H H 1 8.216 0.02 . 1 . . . . 102 ARG N . 15936 7 191 . 1 1 103 103 SER N N 15 114.668 0.2 . 1 . . . . 103 SER H . 15936 7 192 . 1 1 103 103 SER H H 1 7.899 0.02 . 1 . . . . 103 SER N . 15936 7 193 . 1 1 104 104 PHE N N 15 121.755 0.2 . 1 . . . . 104 PHE H . 15936 7 194 . 1 1 104 104 PHE H H 1 8.149 0.02 . 1 . . . . 104 PHE N . 15936 7 195 . 1 1 105 105 LEU N N 15 119.933 0.2 . 1 . . . . 105 LEU H . 15936 7 196 . 1 1 105 105 LEU H H 1 7.879 0.02 . 1 . . . . 105 LEU N . 15936 7 197 . 1 1 106 106 ASP N N 15 117.705 0.2 . 1 . . . . 106 ASP H . 15936 7 198 . 1 1 106 106 ASP H H 1 8.035 0.02 . 1 . . . . 106 ASP N . 15936 7 199 . 1 1 107 107 ASP N N 15 122.028 0.2 . 1 . . . . 107 ASP H . 15936 7 200 . 1 1 107 107 ASP H H 1 7.858 0.02 . 1 . . . . 107 ASP N . 15936 7 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chem_shift_list_8 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chem_shift_list_8 _Assigned_chem_shift_list.Entry_ID 15936 _Assigned_chem_shift_list.ID 8 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_all _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err 0.02 _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err 0.2 _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 8 '2D 1H-15N HSQC' . . . 15936 8 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 SER N N 15 114.885 0.2 . 1 . . . . 3 SER H . 15936 8 2 . 1 1 3 3 SER H H 1 8.296 0.02 . 1 . . . . 3 SER N . 15936 8 3 . 1 1 4 4 SER N N 15 116.642 0.2 . 1 . . . . 4 SER H . 15936 8 4 . 1 1 4 4 SER H H 1 8.267 0.02 . 1 . . . . 4 SER N . 15936 8 5 . 1 1 6 6 HIS N N 15 119.541 0.2 . 1 . . . . 6 HIS H . 15936 8 6 . 1 1 6 6 HIS H H 1 8.471 0.02 . 1 . . . . 6 HIS N . 15936 8 7 . 1 1 7 7 HIS N N 15 117.552 0.2 . 1 . . . . 7 HIS H . 15936 8 8 . 1 1 7 7 HIS H H 1 8.275 0.02 . 1 . . . . 7 HIS N . 15936 8 9 . 1 1 8 8 HIS N N 15 119.415 0.2 . 1 . . . . 8 HIS H . 15936 8 10 . 1 1 8 8 HIS H H 1 8.606 0.02 . 1 . . . . 8 HIS N . 15936 8 11 . 1 1 9 9 HIS N N 15 120.363 0.2 . 1 . . . . 9 HIS H . 15936 8 12 . 1 1 9 9 HIS H H 1 8.677 0.02 . 1 . . . . 9 HIS N . 15936 8 13 . 1 1 10 10 HIS N N 15 121.123 0.2 . 1 . . . . 10 HIS H . 15936 8 14 . 1 1 10 10 HIS H H 1 8.660 0.02 . 1 . . . . 10 HIS N . 15936 8 15 . 1 1 11 11 SER N N 15 118.362 0.2 . 1 . . . . 11 SER H . 15936 8 16 . 1 1 11 11 SER H H 1 8.456 0.02 . 1 . . . . 11 SER N . 15936 8 17 . 1 1 12 12 SER N N 15 118.043 0.2 . 1 . . . . 12 SER H . 15936 8 18 . 1 1 12 12 SER H H 1 8.471 0.02 . 1 . . . . 12 SER N . 15936 8 19 . 1 1 13 13 GLY N N 15 110.157 0.2 . 1 . . . . 13 GLY H . 15936 8 20 . 1 1 13 13 GLY H H 1 8.334 0.02 . 1 . . . . 13 GLY N . 15936 8 21 . 1 1 14 14 LEU N N 15 121.919 0.2 . 1 . . . . 14 LEU H . 15936 8 22 . 1 1 14 14 LEU H H 1 8.114 0.02 . 1 . . . . 14 LEU N . 15936 8 23 . 1 1 15 15 VAL N N 15 123.670 0.2 . 1 . . . . 15 VAL H . 15936 8 24 . 1 1 15 15 VAL H H 1 8.207 0.02 . 1 . . . . 15 VAL N . 15936 8 25 . 1 1 17 17 ARG N N 15 121.531 0.2 . 1 . . . . 17 ARG H . 15936 8 26 . 1 1 17 17 ARG H H 1 8.326 0.02 . 1 . . . . 17 ARG N . 15936 8 27 . 1 1 18 18 GLY N N 15 109.699 0.2 . 1 . . . . 18 GLY H . 15936 8 28 . 1 1 18 18 GLY H H 1 8.372 0.02 . 1 . . . . 18 GLY N . 15936 8 29 . 1 1 19 19 SER N N 15 114.840 0.2 . 1 . . . . 19 SER H . 15936 8 30 . 1 1 19 19 SER H H 1 8.069 0.02 . 1 . . . . 19 SER N . 15936 8 31 . 1 1 20 20 HIS N N 15 119.650 0.2 . 1 . . . . 20 HIS H . 15936 8 32 . 1 1 20 20 HIS H H 1 8.487 0.02 . 1 . . . . 20 HIS N . 15936 8 33 . 1 1 21 21 MET N N 15 120.438 0.2 . 1 . . . . 21 MET H . 15936 8 34 . 1 1 21 21 MET H H 1 8.237 0.02 . 1 . . . . 21 MET N . 15936 8 35 . 1 1 22 22 LEU N N 15 122.466 0.2 . 1 . . . . 22 LEU H . 15936 8 36 . 1 1 22 22 LEU H H 1 8.083 0.02 . 1 . . . . 22 LEU N . 15936 8 37 . 1 1 23 23 GLU N N 15 120.535 0.2 . 1 . . . . 23 GLU H . 15936 8 38 . 1 1 23 23 GLU H H 1 8.056 0.02 . 1 . . . . 23 GLU N . 15936 8 39 . 1 1 24 24 LEU N N 15 123.468 0.2 . 1 . . . . 24 LEU H . 15936 8 40 . 1 1 24 24 LEU H H 1 7.984 0.02 . 1 . . . . 24 LEU N . 15936 8 41 . 1 1 26 26 LEU N N 15 121.115 0.2 . 1 . . . . 26 LEU H . 15936 8 42 . 1 1 26 26 LEU H H 1 8.001 0.02 . 1 . . . . 26 LEU N . 15936 8 43 . 1 1 27 27 ASP N N 15 118.650 0.2 . 1 . . . . 27 ASP H . 15936 8 44 . 1 1 27 27 ASP H H 1 8.257 0.02 . 1 . . . . 27 ASP N . 15936 8 45 . 1 1 28 28 SER N N 15 116.137 0.2 . 1 . . . . 28 SER H . 15936 8 46 . 1 1 28 28 SER H H 1 8.232 0.02 . 1 . . . . 28 SER N . 15936 8 47 . 1 1 29 29 ALA N N 15 124.849 0.2 . 1 . . . . 29 ALA H . 15936 8 48 . 1 1 29 29 ALA H H 1 8.251 0.02 . 1 . . . . 29 ALA N . 15936 8 49 . 1 1 30 30 THR N N 15 112.923 0.2 . 1 . . . . 30 THR H . 15936 8 50 . 1 1 30 30 THR H H 1 8.061 0.02 . 1 . . . . 30 THR N . 15936 8 51 . 1 1 31 31 THR N N 15 115.587 0.2 . 1 . . . . 31 THR H . 15936 8 52 . 1 1 31 31 THR H H 1 8.035 0.02 . 1 . . . . 31 THR N . 15936 8 53 . 1 1 32 32 GLU N N 15 120.832 0.2 . 1 . . . . 32 GLU H . 15936 8 54 . 1 1 32 32 GLU H H 1 8.262 0.02 . 1 . . . . 32 GLU N . 15936 8 55 . 1 1 33 33 SER N N 15 115.984 0.2 . 1 . . . . 33 SER H . 15936 8 56 . 1 1 33 33 SER H H 1 8.115 0.02 . 1 . . . . 33 SER N . 15936 8 57 . 1 1 34 34 LEU N N 15 123.327 0.2 . 1 . . . . 34 LEU H . 15936 8 58 . 1 1 34 34 LEU H H 1 8.075 0.02 . 1 . . . . 34 LEU N . 15936 8 59 . 1 1 35 35 ARG N N 15 121.114 0.2 . 1 . . . . 35 ARG H . 15936 8 60 . 1 1 35 35 ARG H H 1 8.067 0.02 . 1 . . . . 35 ARG N . 15936 8 61 . 1 1 36 36 ALA N N 15 122.430 0.2 . 1 . . . . 36 ALA H . 15936 8 62 . 1 1 36 36 ALA H H 1 8.032 0.02 . 1 . . . . 36 ALA N . 15936 8 63 . 1 1 37 37 ALA N N 15 122.806 0.2 . 1 . . . . 37 ALA H . 15936 8 64 . 1 1 37 37 ALA H H 1 8.170 0.02 . 1 . . . . 37 ALA N . 15936 8 65 . 1 1 38 38 THR N N 15 111.193 0.2 . 1 . . . . 38 THR H . 15936 8 66 . 1 1 38 38 THR H H 1 8.019 0.02 . 1 . . . . 38 THR N . 15936 8 67 . 1 1 39 39 HIS N N 15 118.979 0.2 . 1 . . . . 39 HIS H . 15936 8 68 . 1 1 39 39 HIS H H 1 8.148 0.02 . 1 . . . . 39 HIS N . 15936 8 69 . 1 1 40 40 ASP N N 15 117.600 0.2 . 1 . . . . 40 ASP H . 15936 8 70 . 1 1 40 40 ASP H H 1 8.148 0.02 . 1 . . . . 40 ASP N . 15936 8 71 . 1 1 41 41 VAL N N 15 121.179 0.2 . 1 . . . . 41 VAL H . 15936 8 72 . 1 1 41 41 VAL H H 1 8.150 0.02 . 1 . . . . 41 VAL N . 15936 8 73 . 1 1 42 42 LEU N N 15 123.449 0.2 . 1 . . . . 42 LEU H . 15936 8 74 . 1 1 42 42 LEU H H 1 8.106 0.02 . 1 . . . . 42 LEU N . 15936 8 75 . 1 1 43 43 ALA N N 15 123.639 0.2 . 1 . . . . 43 ALA H . 15936 8 76 . 1 1 43 43 ALA H H 1 8.002 0.02 . 1 . . . . 43 ALA N . 15936 8 77 . 1 1 44 44 GLY N N 15 106.274 0.2 . 1 . . . . 44 GLY H . 15936 8 78 . 1 1 44 44 GLY H H 1 7.954 0.02 . 1 . . . . 44 GLY N . 15936 8 79 . 1 1 45 45 LEU N N 15 122.199 0.2 . 1 . . . . 45 LEU H . 15936 8 80 . 1 1 45 45 LEU H H 1 7.999 0.02 . 1 . . . . 45 LEU N . 15936 8 81 . 1 1 46 46 THR N N 15 113.640 0.2 . 1 . . . . 46 THR H . 15936 8 82 . 1 1 46 46 THR H H 1 8.054 0.02 . 1 . . . . 46 THR N . 15936 8 83 . 1 1 47 47 ALA N N 15 123.370 0.2 . 1 . . . . 47 ALA H . 15936 8 84 . 1 1 47 47 ALA H H 1 8.149 0.02 . 1 . . . . 47 ALA N . 15936 8 85 . 1 1 48 48 ARG N N 15 118.222 0.2 . 1 . . . . 48 ARG H . 15936 8 86 . 1 1 48 48 ARG H H 1 8.165 0.02 . 1 . . . . 48 ARG N . 15936 8 87 . 1 1 49 49 GLU N N 15 117.573 0.2 . 1 . . . . 49 GLU H . 15936 8 88 . 1 1 49 49 GLU H H 1 7.645 0.02 . 1 . . . . 49 GLU N . 15936 8 89 . 1 1 50 50 ALA N N 15 120.269 0.2 . 1 . . . . 50 ALA H . 15936 8 90 . 1 1 50 50 ALA H H 1 8.342 0.02 . 1 . . . . 50 ALA N . 15936 8 91 . 1 1 51 51 LYS N N 15 117.611 0.2 . 1 . . . . 51 LYS H . 15936 8 92 . 1 1 51 51 LYS H H 1 7.675 0.02 . 1 . . . . 51 LYS N . 15936 8 93 . 1 1 52 52 VAL N N 15 119.573 0.2 . 1 . . . . 52 VAL H . 15936 8 94 . 1 1 52 52 VAL H H 1 7.822 0.02 . 1 . . . . 52 VAL N . 15936 8 95 . 1 1 53 53 LEU N N 15 123.565 0.2 . 1 . . . . 53 LEU H . 15936 8 96 . 1 1 53 53 LEU H H 1 8.087 0.02 . 1 . . . . 53 LEU N . 15936 8 97 . 1 1 54 54 ARG N N 15 119.763 0.2 . 1 . . . . 54 ARG H . 15936 8 98 . 1 1 54 54 ARG H H 1 8.112 0.02 . 1 . . . . 54 ARG N . 15936 8 99 . 1 1 55 55 MET N N 15 120.668 0.2 . 1 . . . . 55 MET H . 15936 8 100 . 1 1 55 55 MET H H 1 8.135 0.02 . 1 . . . . 55 MET N . 15936 8 101 . 1 1 56 56 ARG N N 15 120.992 0.2 . 1 . . . . 56 ARG H . 15936 8 102 . 1 1 56 56 ARG H H 1 8.057 0.02 . 1 . . . . 56 ARG N . 15936 8 103 . 1 1 57 57 PHE N N 15 120.164 0.2 . 1 . . . . 57 PHE H . 15936 8 104 . 1 1 57 57 PHE H H 1 8.155 0.02 . 1 . . . . 57 PHE N . 15936 8 105 . 1 1 58 58 GLY N N 15 108.183 0.2 . 1 . . . . 58 GLY H . 15936 8 106 . 1 1 58 58 GLY H H 1 7.947 0.02 . 1 . . . . 58 GLY N . 15936 8 107 . 1 1 59 59 ILE N N 15 118.103 0.2 . 1 . . . . 59 ILE H . 15936 8 108 . 1 1 59 59 ILE H H 1 7.677 0.02 . 1 . . . . 59 ILE N . 15936 8 109 . 1 1 60 60 ASP N N 15 121.767 0.2 . 1 . . . . 60 ASP H . 15936 8 110 . 1 1 60 60 ASP H H 1 8.374 0.02 . 1 . . . . 60 ASP N . 15936 8 111 . 1 1 61 61 MET N N 15 120.038 0.2 . 1 . . . . 61 MET H . 15936 8 112 . 1 1 61 61 MET H H 1 8.253 0.02 . 1 . . . . 61 MET N . 15936 8 113 . 1 1 62 62 ASN N N 15 118.079 0.2 . 1 . . . . 62 ASN H . 15936 8 114 . 1 1 62 62 ASN H H 1 8.252 0.02 . 1 . . . . 62 ASN N . 15936 8 115 . 1 1 63 63 THR N N 15 115.408 0.2 . 1 . . . . 63 THR H . 15936 8 116 . 1 1 63 63 THR H H 1 8.096 0.02 . 1 . . . . 63 THR N . 15936 8 117 . 1 1 64 64 ASP N N 15 120.223 0.2 . 1 . . . . 64 ASP H . 15936 8 118 . 1 1 64 64 ASP H H 1 8.290 0.02 . 1 . . . . 64 ASP N . 15936 8 119 . 1 1 65 65 TYR N N 15 120.864 0.2 . 1 . . . . 65 TYR H . 15936 8 120 . 1 1 65 65 TYR H H 1 8.033 0.02 . 1 . . . . 65 TYR N . 15936 8 121 . 1 1 66 66 THR N N 15 114.632 0.2 . 1 . . . . 66 THR H . 15936 8 122 . 1 1 66 66 THR H H 1 7.905 0.02 . 1 . . . . 66 THR N . 15936 8 123 . 1 1 67 67 LEU N N 15 123.084 0.2 . 1 . . . . 67 LEU H . 15936 8 124 . 1 1 67 67 LEU H H 1 8.008 0.02 . 1 . . . . 67 LEU N . 15936 8 125 . 1 1 68 68 GLU N N 15 120.412 0.2 . 1 . . . . 68 GLU H . 15936 8 126 . 1 1 68 68 GLU H H 1 8.108 0.02 . 1 . . . . 68 GLU N . 15936 8 127 . 1 1 69 69 GLU N N 15 120.533 0.2 . 1 . . . . 69 GLU H . 15936 8 128 . 1 1 69 69 GLU H H 1 8.125 0.02 . 1 . . . . 69 GLU N . 15936 8 129 . 1 1 70 70 VAL N N 15 120.367 0.2 . 1 . . . . 70 VAL H . 15936 8 130 . 1 1 70 70 VAL H H 1 8.024 0.02 . 1 . . . . 70 VAL N . 15936 8 131 . 1 1 71 71 GLY N N 15 107.508 0.2 . 1 . . . . 71 GLY H . 15936 8 132 . 1 1 71 71 GLY H H 1 8.223 0.02 . 1 . . . . 71 GLY N . 15936 8 133 . 1 1 72 72 LYS N N 15 120.799 0.2 . 1 . . . . 72 LYS H . 15936 8 134 . 1 1 72 72 LYS H H 1 8.105 0.02 . 1 . . . . 72 LYS N . 15936 8 135 . 1 1 73 73 GLN N N 15 119.410 0.2 . 1 . . . . 73 GLN H . 15936 8 136 . 1 1 73 73 GLN H H 1 8.284 0.02 . 1 . . . . 73 GLN N . 15936 8 137 . 1 1 75 75 ASP N N 15 120.258 0.2 . 1 . . . . 75 ASP H . 15936 8 138 . 1 1 75 75 ASP H H 1 8.219 0.02 . 1 . . . . 75 ASP N . 15936 8 139 . 1 1 76 76 VAL N N 15 120.663 0.2 . 1 . . . . 76 VAL H . 15936 8 140 . 1 1 76 76 VAL H H 1 8.089 0.02 . 1 . . . . 76 VAL N . 15936 8 141 . 1 1 77 77 THR N N 15 117.142 0.2 . 1 . . . . 77 THR H . 15936 8 142 . 1 1 77 77 THR H H 1 7.964 0.02 . 1 . . . . 77 THR N . 15936 8 143 . 1 1 78 78 ARG N N 15 122.155 0.2 . 1 . . . . 78 ARG H . 15936 8 144 . 1 1 78 78 ARG H H 1 8.144 0.02 . 1 . . . . 78 ARG N . 15936 8 145 . 1 1 79 79 GLU N N 15 118.038 0.2 . 1 . . . . 79 GLU H . 15936 8 146 . 1 1 79 79 GLU H H 1 8.032 0.02 . 1 . . . . 79 GLU N . 15936 8 147 . 1 1 80 80 ARG N N 15 121.609 0.2 . 1 . . . . 80 ARG H . 15936 8 148 . 1 1 80 80 ARG H H 1 8.228 0.02 . 1 . . . . 80 ARG N . 15936 8 149 . 1 1 81 81 ILE N N 15 121.221 0.2 . 1 . . . . 81 ILE H . 15936 8 150 . 1 1 81 81 ILE H H 1 8.039 0.02 . 1 . . . . 81 ILE N . 15936 8 151 . 1 1 82 82 ARG N N 15 123.581 0.2 . 1 . . . . 82 ARG H . 15936 8 152 . 1 1 82 82 ARG H H 1 8.219 0.02 . 1 . . . . 82 ARG N . 15936 8 153 . 1 1 83 83 GLN N N 15 121.261 0.2 . 1 . . . . 83 GLN H . 15936 8 154 . 1 1 83 83 GLN H H 1 8.242 0.02 . 1 . . . . 83 GLN N . 15936 8 155 . 1 1 84 84 ILE N N 15 122.410 0.2 . 1 . . . . 84 ILE H . 15936 8 156 . 1 1 84 84 ILE H H 1 8.191 0.02 . 1 . . . . 84 ILE N . 15936 8 157 . 1 1 85 85 GLU N N 15 119.355 0.2 . 1 . . . . 85 GLU H . 15936 8 158 . 1 1 85 85 GLU H H 1 8.558 0.02 . 1 . . . . 85 GLU N . 15936 8 159 . 1 1 86 86 ALA N N 15 123.370 0.2 . 1 . . . . 86 ALA H . 15936 8 160 . 1 1 86 86 ALA H H 1 8.168 0.02 . 1 . . . . 86 ALA N . 15936 8 161 . 1 1 87 87 LYS N N 15 117.409 0.2 . 1 . . . . 87 LYS H . 15936 8 162 . 1 1 87 87 LYS H H 1 7.727 0.02 . 1 . . . . 87 LYS N . 15936 8 163 . 1 1 88 88 ALA N N 15 122.193 0.2 . 1 . . . . 88 ALA H . 15936 8 164 . 1 1 88 88 ALA H H 1 7.999 0.02 . 1 . . . . 88 ALA N . 15936 8 165 . 1 1 89 89 LEU N N 15 120.962 0.2 . 1 . . . . 89 LEU H . 15936 8 166 . 1 1 89 89 LEU H H 1 8.014 0.02 . 1 . . . . 89 LEU N . 15936 8 167 . 1 1 90 90 ARG N N 15 121.068 0.2 . 1 . . . . 90 ARG H . 15936 8 168 . 1 1 90 90 ARG H H 1 8.134 0.02 . 1 . . . . 90 ARG N . 15936 8 169 . 1 1 91 91 LYS N N 15 121.824 0.2 . 1 . . . . 91 LYS H . 15936 8 170 . 1 1 91 91 LYS H H 1 8.109 0.02 . 1 . . . . 91 LYS N . 15936 8 171 . 1 1 92 92 LEU N N 15 119.607 0.2 . 1 . . . . 92 LEU H . 15936 8 172 . 1 1 92 92 LEU H H 1 7.749 0.02 . 1 . . . . 92 LEU N . 15936 8 173 . 1 1 93 93 ARG N N 15 121.376 0.2 . 1 . . . . 93 ARG H . 15936 8 174 . 1 1 93 93 ARG H H 1 8.247 0.02 . 1 . . . . 93 ARG N . 15936 8 175 . 1 1 94 94 HIS N N 15 118.095 0.2 . 1 . . . . 94 HIS H . 15936 8 176 . 1 1 94 94 HIS H H 1 8.275 0.02 . 1 . . . . 94 HIS N . 15936 8 177 . 1 1 96 96 SER N N 15 115.933 0.2 . 1 . . . . 96 SER H . 15936 8 178 . 1 1 96 96 SER H H 1 8.225 0.02 . 1 . . . . 96 SER N . 15936 8 179 . 1 1 97 97 ARG N N 15 122.517 0.2 . 1 . . . . 97 ARG H . 15936 8 180 . 1 1 97 97 ARG H H 1 8.629 0.02 . 1 . . . . 97 ARG N . 15936 8 181 . 1 1 98 98 SER N N 15 113.442 0.2 . 1 . . . . 98 SER H . 15936 8 182 . 1 1 98 98 SER H H 1 8.246 0.02 . 1 . . . . 98 SER N . 15936 8 183 . 1 1 99 99 GLU N N 15 121.576 0.2 . 1 . . . . 99 GLU H . 15936 8 184 . 1 1 99 99 GLU H H 1 7.890 0.02 . 1 . . . . 99 GLU N . 15936 8 185 . 1 1 100 100 VAL N N 15 120.316 0.2 . 1 . . . . 100 VAL H . 15936 8 186 . 1 1 100 100 VAL H H 1 7.943 0.02 . 1 . . . . 100 VAL N . 15936 8 187 . 1 1 101 101 LEU N N 15 123.470 0.2 . 1 . . . . 101 LEU H . 15936 8 188 . 1 1 101 101 LEU H H 1 7.984 0.02 . 1 . . . . 101 LEU N . 15936 8 189 . 1 1 102 102 ARG N N 15 121.662 0.2 . 1 . . . . 102 ARG H . 15936 8 190 . 1 1 102 102 ARG H H 1 8.216 0.02 . 1 . . . . 102 ARG N . 15936 8 191 . 1 1 103 103 SER N N 15 114.425 0.2 . 1 . . . . 103 SER H . 15936 8 192 . 1 1 103 103 SER H H 1 7.859 0.02 . 1 . . . . 103 SER N . 15936 8 193 . 1 1 104 104 PHE N N 15 121.755 0.2 . 1 . . . . 104 PHE H . 15936 8 194 . 1 1 104 104 PHE H H 1 8.149 0.02 . 1 . . . . 104 PHE N . 15936 8 195 . 1 1 105 105 LEU N N 15 119.552 0.2 . 1 . . . . 105 LEU H . 15936 8 196 . 1 1 105 105 LEU H H 1 7.881 0.02 . 1 . . . . 105 LEU N . 15936 8 197 . 1 1 106 106 ASP N N 15 117.405 0.2 . 1 . . . . 106 ASP H . 15936 8 198 . 1 1 106 106 ASP H H 1 8.007 0.02 . 1 . . . . 106 ASP N . 15936 8 199 . 1 1 107 107 ASP N N 15 121.924 0.2 . 1 . . . . 107 ASP H . 15936 8 200 . 1 1 107 107 ASP H H 1 7.836 0.02 . 1 . . . . 107 ASP N . 15936 8 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chem_shift_list_9 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chem_shift_list_9 _Assigned_chem_shift_list.Entry_ID 15936 _Assigned_chem_shift_list.ID 9 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_all _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err 0.02 _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err 0.2 _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details 'M1 is deleted in the expression system.' _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 9 '2D 1H-15N HSQC' . . . 15936 9 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 SER N N 15 114.839 0.2 . 1 . . . . 3 SER H . 15936 9 2 . 1 1 3 3 SER H H 1 8.293 0.02 . 1 . . . . 3 SER N . 15936 9 3 . 1 1 4 4 SER N N 15 116.593 0.2 . 1 . . . . 4 SER H . 15936 9 4 . 1 1 4 4 SER H H 1 8.266 0.02 . 1 . . . . 4 SER N . 15936 9 5 . 1 1 6 6 HIS N N 15 119.307 0.2 . 1 . . . . 6 HIS H . 15936 9 6 . 1 1 6 6 HIS H H 1 8.438 0.02 . 1 . . . . 6 HIS N . 15936 9 7 . 1 1 7 7 HIS N N 15 117.413 0.2 . 1 . . . . 7 HIS H . 15936 9 8 . 1 1 7 7 HIS H H 1 8.268 0.02 . 1 . . . . 7 HIS N . 15936 9 9 . 1 1 8 8 HIS N N 15 119.392 0.2 . 1 . . . . 8 HIS H . 15936 9 10 . 1 1 8 8 HIS H H 1 8.598 0.02 . 1 . . . . 8 HIS N . 15936 9 11 . 1 1 9 9 HIS N N 15 120.120 0.2 . 1 . . . . 9 HIS H . 15936 9 12 . 1 1 9 9 HIS H H 1 8.674 0.02 . 1 . . . . 9 HIS N . 15936 9 13 . 1 1 10 10 HIS N N 15 120.956 0.2 . 1 . . . . 10 HIS H . 15936 9 14 . 1 1 10 10 HIS H H 1 8.655 0.02 . 1 . . . . 10 HIS N . 15936 9 15 . 1 1 11 11 SER N N 15 118.247 0.2 . 1 . . . . 11 SER H . 15936 9 16 . 1 1 11 11 SER H H 1 8.445 0.02 . 1 . . . . 11 SER N . 15936 9 17 . 1 1 12 12 SER N N 15 117.930 0.2 . 1 . . . . 12 SER H . 15936 9 18 . 1 1 12 12 SER H H 1 8.454 0.02 . 1 . . . . 12 SER N . 15936 9 19 . 1 1 13 13 GLY N N 15 110.021 0.2 . 1 . . . . 13 GLY H . 15936 9 20 . 1 1 13 13 GLY H H 1 8.319 0.02 . 1 . . . . 13 GLY N . 15936 9 21 . 1 1 14 14 LEU N N 15 121.919 0.2 . 1 . . . . 14 LEU H . 15936 9 22 . 1 1 14 14 LEU H H 1 8.114 0.02 . 1 . . . . 14 LEU N . 15936 9 23 . 1 1 15 15 VAL N N 15 123.670 0.2 . 1 . . . . 15 VAL H . 15936 9 24 . 1 1 15 15 VAL H H 1 8.207 0.02 . 1 . . . . 15 VAL N . 15936 9 25 . 1 1 17 17 ARG N N 15 121.361 0.2 . 1 . . . . 17 ARG H . 15936 9 26 . 1 1 17 17 ARG H H 1 8.280 0.02 . 1 . . . . 17 ARG N . 15936 9 27 . 1 1 18 18 GLY N N 15 109.522 0.2 . 1 . . . . 18 GLY H . 15936 9 28 . 1 1 18 18 GLY H H 1 8.357 0.02 . 1 . . . . 18 GLY N . 15936 9 29 . 1 1 19 19 SER N N 15 114.730 0.2 . 1 . . . . 19 SER H . 15936 9 30 . 1 1 19 19 SER H H 1 8.048 0.02 . 1 . . . . 19 SER N . 15936 9 31 . 1 1 20 20 HIS N N 15 119.500 0.2 . 1 . . . . 20 HIS H . 15936 9 32 . 1 1 20 20 HIS H H 1 8.463 0.02 . 1 . . . . 20 HIS N . 15936 9 33 . 1 1 21 21 MET N N 15 120.083 0.2 . 1 . . . . 21 MET H . 15936 9 34 . 1 1 21 21 MET H H 1 8.208 0.02 . 1 . . . . 21 MET N . 15936 9 35 . 1 1 22 22 LEU N N 15 121.986 0.2 . 1 . . . . 22 LEU H . 15936 9 36 . 1 1 22 22 LEU H H 1 8.013 0.02 . 1 . . . . 22 LEU N . 15936 9 37 . 1 1 23 23 GLU N N 15 120.145 0.2 . 1 . . . . 23 GLU H . 15936 9 38 . 1 1 23 23 GLU H H 1 7.998 0.02 . 1 . . . . 23 GLU N . 15936 9 39 . 1 1 24 24 LEU N N 15 124.857 0.2 . 1 . . . . 24 LEU H . 15936 9 40 . 1 1 24 24 LEU H H 1 8.190 0.02 . 1 . . . . 24 LEU N . 15936 9 41 . 1 1 26 26 LEU N N 15 120.850 0.2 . 1 . . . . 26 LEU H . 15936 9 42 . 1 1 26 26 LEU H H 1 8.143 0.02 . 1 . . . . 26 LEU N . 15936 9 43 . 1 1 27 27 ASP N N 15 118.589 0.2 . 1 . . . . 27 ASP H . 15936 9 44 . 1 1 27 27 ASP H H 1 8.242 0.02 . 1 . . . . 27 ASP N . 15936 9 45 . 1 1 28 28 SER N N 15 116.224 0.2 . 1 . . . . 28 SER H . 15936 9 46 . 1 1 28 28 SER H H 1 8.265 0.02 . 1 . . . . 28 SER N . 15936 9 47 . 1 1 29 29 ALA N N 15 124.719 0.2 . 1 . . . . 29 ALA H . 15936 9 48 . 1 1 29 29 ALA H H 1 8.242 0.02 . 1 . . . . 29 ALA N . 15936 9 49 . 1 1 30 30 THR N N 15 113.194 0.2 . 1 . . . . 30 THR H . 15936 9 50 . 1 1 30 30 THR H H 1 8.087 0.02 . 1 . . . . 30 THR N . 15936 9 51 . 1 1 31 31 THR N N 15 115.535 0.2 . 1 . . . . 31 THR H . 15936 9 52 . 1 1 31 31 THR H H 1 8.028 0.02 . 1 . . . . 31 THR N . 15936 9 53 . 1 1 32 32 GLU N N 15 120.699 0.2 . 1 . . . . 32 GLU H . 15936 9 54 . 1 1 32 32 GLU H H 1 8.252 0.02 . 1 . . . . 32 GLU N . 15936 9 55 . 1 1 33 33 SER N N 15 115.917 0.2 . 1 . . . . 33 SER H . 15936 9 56 . 1 1 33 33 SER H H 1 8.103 0.02 . 1 . . . . 33 SER N . 15936 9 57 . 1 1 34 34 LEU N N 15 123.266 0.2 . 1 . . . . 34 LEU H . 15936 9 58 . 1 1 34 34 LEU H H 1 8.099 0.02 . 1 . . . . 34 LEU N . 15936 9 59 . 1 1 35 35 ARG N N 15 121.114 0.2 . 1 . . . . 35 ARG H . 15936 9 60 . 1 1 35 35 ARG H H 1 8.067 0.02 . 1 . . . . 35 ARG N . 15936 9 61 . 1 1 36 36 ALA N N 15 122.246 0.2 . 1 . . . . 36 ALA H . 15936 9 62 . 1 1 36 36 ALA H H 1 8.065 0.02 . 1 . . . . 36 ALA N . 15936 9 63 . 1 1 37 37 ALA N N 15 122.806 0.2 . 1 . . . . 37 ALA H . 15936 9 64 . 1 1 37 37 ALA H H 1 8.170 0.02 . 1 . . . . 37 ALA N . 15936 9 65 . 1 1 38 38 THR N N 15 111.447 0.2 . 1 . . . . 38 THR H . 15936 9 66 . 1 1 38 38 THR H H 1 8.111 0.02 . 1 . . . . 38 THR N . 15936 9 67 . 1 1 39 39 HIS N N 15 118.898 0.2 . 1 . . . . 39 HIS H . 15936 9 68 . 1 1 39 39 HIS H H 1 8.150 0.02 . 1 . . . . 39 HIS N . 15936 9 69 . 1 1 40 40 ASP N N 15 120.008 0.2 . 1 . . . . 40 ASP H . 15936 9 70 . 1 1 40 40 ASP H H 1 8.423 0.02 . 1 . . . . 40 ASP N . 15936 9 71 . 1 1 41 41 VAL N N 15 121.179 0.2 . 1 . . . . 41 VAL H . 15936 9 72 . 1 1 41 41 VAL H H 1 8.150 0.02 . 1 . . . . 41 VAL N . 15936 9 73 . 1 1 42 42 LEU N N 15 123.449 0.2 . 1 . . . . 42 LEU H . 15936 9 74 . 1 1 42 42 LEU H H 1 8.106 0.02 . 1 . . . . 42 LEU N . 15936 9 75 . 1 1 43 43 ALA N N 15 123.639 0.2 . 1 . . . . 43 ALA H . 15936 9 76 . 1 1 43 43 ALA H H 1 8.002 0.02 . 1 . . . . 43 ALA N . 15936 9 77 . 1 1 44 44 GLY N N 15 106.389 0.2 . 1 . . . . 44 GLY H . 15936 9 78 . 1 1 44 44 GLY H H 1 7.967 0.02 . 1 . . . . 44 GLY N . 15936 9 79 . 1 1 45 45 LEU N N 15 121.708 0.2 . 1 . . . . 45 LEU H . 15936 9 80 . 1 1 45 45 LEU H H 1 7.935 0.02 . 1 . . . . 45 LEU N . 15936 9 81 . 1 1 46 46 THR N N 15 114.067 0.2 . 1 . . . . 46 THR H . 15936 9 82 . 1 1 46 46 THR H H 1 8.182 0.02 . 1 . . . . 46 THR N . 15936 9 83 . 1 1 47 47 ALA N N 15 123.248 0.2 . 1 . . . . 47 ALA H . 15936 9 84 . 1 1 47 47 ALA H H 1 7.957 0.02 . 1 . . . . 47 ALA N . 15936 9 85 . 1 1 48 48 ARG N N 15 118.222 0.2 . 1 . . . . 48 ARG H . 15936 9 86 . 1 1 48 48 ARG H H 1 8.165 0.02 . 1 . . . . 48 ARG N . 15936 9 87 . 1 1 49 49 GLU N N 15 117.399 0.2 . 1 . . . . 49 GLU H . 15936 9 88 . 1 1 49 49 GLU H H 1 7.649 0.02 . 1 . . . . 49 GLU N . 15936 9 89 . 1 1 50 50 ALA N N 15 120.148 0.2 . 1 . . . . 50 ALA H . 15936 9 90 . 1 1 50 50 ALA H H 1 8.297 0.02 . 1 . . . . 50 ALA N . 15936 9 91 . 1 1 51 51 LYS N N 15 117.510 0.2 . 1 . . . . 51 LYS H . 15936 9 92 . 1 1 51 51 LYS H H 1 7.660 0.02 . 1 . . . . 51 LYS N . 15936 9 93 . 1 1 52 52 VAL N N 15 119.695 0.2 . 1 . . . . 52 VAL H . 15936 9 94 . 1 1 52 52 VAL H H 1 7.898 0.02 . 1 . . . . 52 VAL N . 15936 9 95 . 1 1 53 53 LEU N N 15 123.565 0.2 . 1 . . . . 53 LEU H . 15936 9 96 . 1 1 53 53 LEU H H 1 8.087 0.02 . 1 . . . . 53 LEU N . 15936 9 97 . 1 1 54 54 ARG N N 15 119.763 0.2 . 1 . . . . 54 ARG H . 15936 9 98 . 1 1 54 54 ARG H H 1 8.112 0.02 . 1 . . . . 54 ARG N . 15936 9 99 . 1 1 55 55 MET N N 15 120.668 0.2 . 1 . . . . 55 MET H . 15936 9 100 . 1 1 55 55 MET H H 1 8.135 0.02 . 1 . . . . 55 MET N . 15936 9 101 . 1 1 56 56 ARG N N 15 120.992 0.2 . 1 . . . . 56 ARG H . 15936 9 102 . 1 1 56 56 ARG H H 1 8.057 0.02 . 1 . . . . 56 ARG N . 15936 9 103 . 1 1 57 57 PHE N N 15 120.164 0.2 . 1 . . . . 57 PHE H . 15936 9 104 . 1 1 57 57 PHE H H 1 8.155 0.02 . 1 . . . . 57 PHE N . 15936 9 105 . 1 1 58 58 GLY N N 15 107.461 0.2 . 1 . . . . 58 GLY H . 15936 9 106 . 1 1 58 58 GLY H H 1 8.049 0.02 . 1 . . . . 58 GLY N . 15936 9 107 . 1 1 59 59 ILE N N 15 118.039 0.2 . 1 . . . . 59 ILE H . 15936 9 108 . 1 1 59 59 ILE H H 1 7.684 0.02 . 1 . . . . 59 ILE N . 15936 9 109 . 1 1 60 60 ASP N N 15 121.770 0.2 . 1 . . . . 60 ASP H . 15936 9 110 . 1 1 60 60 ASP H H 1 8.398 0.02 . 1 . . . . 60 ASP N . 15936 9 111 . 1 1 61 61 MET N N 15 119.666 0.2 . 1 . . . . 61 MET H . 15936 9 112 . 1 1 61 61 MET H H 1 8.331 0.02 . 1 . . . . 61 MET N . 15936 9 113 . 1 1 62 62 ASN N N 15 118.853 0.2 . 1 . . . . 62 ASN H . 15936 9 114 . 1 1 62 62 ASN H H 1 8.305 0.02 . 1 . . . . 62 ASN N . 15936 9 115 . 1 1 63 63 THR N N 15 116.009 0.2 . 1 . . . . 63 THR H . 15936 9 116 . 1 1 63 63 THR H H 1 8.108 0.02 . 1 . . . . 63 THR N . 15936 9 117 . 1 1 64 64 ASP N N 15 120.445 0.2 . 1 . . . . 64 ASP H . 15936 9 118 . 1 1 64 64 ASP H H 1 8.361 0.02 . 1 . . . . 64 ASP N . 15936 9 119 . 1 1 65 65 TYR N N 15 120.864 0.2 . 1 . . . . 65 TYR H . 15936 9 120 . 1 1 65 65 TYR H H 1 8.033 0.02 . 1 . . . . 65 TYR N . 15936 9 121 . 1 1 66 66 THR N N 15 115.388 0.2 . 1 . . . . 66 THR H . 15936 9 122 . 1 1 66 66 THR H H 1 7.982 0.02 . 1 . . . . 66 THR N . 15936 9 123 . 1 1 67 67 LEU N N 15 123.084 0.2 . 1 . . . . 67 LEU H . 15936 9 124 . 1 1 67 67 LEU H H 1 8.008 0.02 . 1 . . . . 67 LEU N . 15936 9 125 . 1 1 68 68 GLU N N 15 120.412 0.2 . 1 . . . . 68 GLU H . 15936 9 126 . 1 1 68 68 GLU H H 1 8.108 0.02 . 1 . . . . 68 GLU N . 15936 9 127 . 1 1 69 69 GLU N N 15 120.533 0.2 . 1 . . . . 69 GLU H . 15936 9 128 . 1 1 69 69 GLU H H 1 8.125 0.02 . 1 . . . . 69 GLU N . 15936 9 129 . 1 1 70 70 VAL N N 15 120.367 0.2 . 1 . . . . 70 VAL H . 15936 9 130 . 1 1 70 70 VAL H H 1 8.024 0.02 . 1 . . . . 70 VAL N . 15936 9 131 . 1 1 71 71 GLY N N 15 107.061 0.2 . 1 . . . . 71 GLY H . 15936 9 132 . 1 1 71 71 GLY H H 1 8.223 0.02 . 1 . . . . 71 GLY N . 15936 9 133 . 1 1 72 72 LYS N N 15 120.799 0.2 . 1 . . . . 72 LYS H . 15936 9 134 . 1 1 72 72 LYS H H 1 8.105 0.02 . 1 . . . . 72 LYS N . 15936 9 135 . 1 1 73 73 GLN N N 15 119.410 0.2 . 1 . . . . 73 GLN H . 15936 9 136 . 1 1 73 73 GLN H H 1 8.284 0.02 . 1 . . . . 73 GLN N . 15936 9 137 . 1 1 75 75 ASP N N 15 120.258 0.2 . 1 . . . . 75 ASP H . 15936 9 138 . 1 1 75 75 ASP H H 1 8.219 0.02 . 1 . . . . 75 ASP N . 15936 9 139 . 1 1 76 76 VAL N N 15 120.663 0.2 . 1 . . . . 76 VAL H . 15936 9 140 . 1 1 76 76 VAL H H 1 8.089 0.02 . 1 . . . . 76 VAL N . 15936 9 141 . 1 1 77 77 THR N N 15 117.332 0.2 . 1 . . . . 77 THR H . 15936 9 142 . 1 1 77 77 THR H H 1 8.019 0.02 . 1 . . . . 77 THR N . 15936 9 143 . 1 1 78 78 ARG N N 15 122.155 0.2 . 1 . . . . 78 ARG H . 15936 9 144 . 1 1 78 78 ARG H H 1 8.144 0.02 . 1 . . . . 78 ARG N . 15936 9 145 . 1 1 79 79 GLU N N 15 118.038 0.2 . 1 . . . . 79 GLU H . 15936 9 146 . 1 1 79 79 GLU H H 1 8.032 0.02 . 1 . . . . 79 GLU N . 15936 9 147 . 1 1 80 80 ARG N N 15 121.609 0.2 . 1 . . . . 80 ARG H . 15936 9 148 . 1 1 80 80 ARG H H 1 8.228 0.02 . 1 . . . . 80 ARG N . 15936 9 149 . 1 1 81 81 ILE N N 15 121.221 0.2 . 1 . . . . 81 ILE H . 15936 9 150 . 1 1 81 81 ILE H H 1 8.039 0.02 . 1 . . . . 81 ILE N . 15936 9 151 . 1 1 82 82 ARG N N 15 123.581 0.2 . 1 . . . . 82 ARG H . 15936 9 152 . 1 1 82 82 ARG H H 1 8.219 0.02 . 1 . . . . 82 ARG N . 15936 9 153 . 1 1 83 83 GLN N N 15 121.261 0.2 . 1 . . . . 83 GLN H . 15936 9 154 . 1 1 83 83 GLN H H 1 8.242 0.02 . 1 . . . . 83 GLN N . 15936 9 155 . 1 1 84 84 ILE N N 15 122.410 0.2 . 1 . . . . 84 ILE H . 15936 9 156 . 1 1 84 84 ILE H H 1 8.191 0.02 . 1 . . . . 84 ILE N . 15936 9 157 . 1 1 85 85 GLU N N 15 119.223 0.2 . 1 . . . . 85 GLU H . 15936 9 158 . 1 1 85 85 GLU H H 1 8.601 0.02 . 1 . . . . 85 GLU N . 15936 9 159 . 1 1 86 86 ALA N N 15 123.370 0.2 . 1 . . . . 86 ALA H . 15936 9 160 . 1 1 86 86 ALA H H 1 8.168 0.02 . 1 . . . . 86 ALA N . 15936 9 161 . 1 1 87 87 LYS N N 15 117.420 0.2 . 1 . . . . 87 LYS H . 15936 9 162 . 1 1 87 87 LYS H H 1 7.731 0.02 . 1 . . . . 87 LYS N . 15936 9 163 . 1 1 88 88 ALA N N 15 121.976 0.2 . 1 . . . . 88 ALA H . 15936 9 164 . 1 1 88 88 ALA H H 1 8.004 0.02 . 1 . . . . 88 ALA N . 15936 9 165 . 1 1 89 89 LEU N N 15 120.962 0.2 . 1 . . . . 89 LEU H . 15936 9 166 . 1 1 89 89 LEU H H 1 8.014 0.02 . 1 . . . . 89 LEU N . 15936 9 167 . 1 1 90 90 ARG N N 15 121.068 0.2 . 1 . . . . 90 ARG H . 15936 9 168 . 1 1 90 90 ARG H H 1 8.134 0.02 . 1 . . . . 90 ARG N . 15936 9 169 . 1 1 91 91 LYS N N 15 121.824 0.2 . 1 . . . . 91 LYS H . 15936 9 170 . 1 1 91 91 LYS H H 1 8.109 0.02 . 1 . . . . 91 LYS N . 15936 9 171 . 1 1 92 92 LEU N N 15 119.376 0.2 . 1 . . . . 92 LEU H . 15936 9 172 . 1 1 92 92 LEU H H 1 7.775 0.02 . 1 . . . . 92 LEU N . 15936 9 173 . 1 1 93 93 ARG N N 15 121.376 0.2 . 1 . . . . 93 ARG H . 15936 9 174 . 1 1 93 93 ARG H H 1 8.247 0.02 . 1 . . . . 93 ARG N . 15936 9 175 . 1 1 94 94 HIS N N 15 118.193 0.2 . 1 . . . . 94 HIS H . 15936 9 176 . 1 1 94 94 HIS H H 1 8.199 0.02 . 1 . . . . 94 HIS N . 15936 9 177 . 1 1 96 96 SER N N 15 115.887 0.2 . 1 . . . . 96 SER H . 15936 9 178 . 1 1 96 96 SER H H 1 8.208 0.02 . 1 . . . . 96 SER N . 15936 9 179 . 1 1 97 97 ARG N N 15 122.433 0.2 . 1 . . . . 97 ARG H . 15936 9 180 . 1 1 97 97 ARG H H 1 8.676 0.02 . 1 . . . . 97 ARG N . 15936 9 181 . 1 1 98 98 SER N N 15 112.876 0.2 . 1 . . . . 98 SER H . 15936 9 182 . 1 1 98 98 SER H H 1 8.237 0.02 . 1 . . . . 98 SER N . 15936 9 183 . 1 1 99 99 GLU N N 15 121.415 0.2 . 1 . . . . 99 GLU H . 15936 9 184 . 1 1 99 99 GLU H H 1 7.800 0.02 . 1 . . . . 99 GLU N . 15936 9 185 . 1 1 100 100 VAL N N 15 120.350 0.2 . 1 . . . . 100 VAL H . 15936 9 186 . 1 1 100 100 VAL H H 1 7.934 0.02 . 1 . . . . 100 VAL N . 15936 9 187 . 1 1 101 101 LEU N N 15 122.918 0.2 . 1 . . . . 101 LEU H . 15936 9 188 . 1 1 101 101 LEU H H 1 7.908 0.02 . 1 . . . . 101 LEU N . 15936 9 189 . 1 1 102 102 ARG N N 15 121.662 0.2 . 1 . . . . 102 ARG H . 15936 9 190 . 1 1 102 102 ARG H H 1 8.216 0.02 . 1 . . . . 102 ARG N . 15936 9 191 . 1 1 103 103 SER N N 15 114.246 0.2 . 1 . . . . 103 SER H . 15936 9 192 . 1 1 103 103 SER H H 1 7.831 0.02 . 1 . . . . 103 SER N . 15936 9 193 . 1 1 104 104 PHE N N 15 121.755 0.2 . 1 . . . . 104 PHE H . 15936 9 194 . 1 1 104 104 PHE H H 1 8.149 0.02 . 1 . . . . 104 PHE N . 15936 9 195 . 1 1 105 105 LEU N N 15 119.200 0.2 . 1 . . . . 105 LEU H . 15936 9 196 . 1 1 105 105 LEU H H 1 7.896 0.02 . 1 . . . . 105 LEU N . 15936 9 197 . 1 1 106 106 ASP N N 15 117.070 0.2 . 1 . . . . 106 ASP H . 15936 9 198 . 1 1 106 106 ASP H H 1 7.981 0.02 . 1 . . . . 106 ASP N . 15936 9 199 . 1 1 107 107 ASP N N 15 121.846 0.2 . 1 . . . . 107 ASP H . 15936 9 200 . 1 1 107 107 ASP H H 1 7.820 0.02 . 1 . . . . 107 ASP N . 15936 9 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chem_shift_list_10 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chem_shift_list_10 _Assigned_chem_shift_list.Entry_ID 15936 _Assigned_chem_shift_list.ID 10 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_all _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err 0.02 _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err 0.2 _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 10 '2D 1H-15N HSQC' . . . 15936 10 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 SER N N 15 114.832 0.2 . 1 . . . . 3 SER H . 15936 10 2 . 1 1 3 3 SER H H 1 8.289 0.02 . 1 . . . . 3 SER N . 15936 10 3 . 1 1 4 4 SER N N 15 116.581 0.2 . 1 . . . . 4 SER H . 15936 10 4 . 1 1 4 4 SER H H 1 8.268 0.02 . 1 . . . . 4 SER N . 15936 10 5 . 1 1 6 6 HIS N N 15 119.200 0.2 . 1 . . . . 6 HIS H . 15936 10 6 . 1 1 6 6 HIS H H 1 8.421 0.02 . 1 . . . . 6 HIS N . 15936 10 7 . 1 1 7 7 HIS N N 15 117.376 0.2 . 1 . . . . 7 HIS H . 15936 10 8 . 1 1 7 7 HIS H H 1 8.264 0.02 . 1 . . . . 7 HIS N . 15936 10 9 . 1 1 8 8 HIS N N 15 119.399 0.2 . 1 . . . . 8 HIS H . 15936 10 10 . 1 1 8 8 HIS H H 1 8.588 0.02 . 1 . . . . 8 HIS N . 15936 10 11 . 1 1 9 9 HIS N N 15 120.016 0.2 . 1 . . . . 9 HIS H . 15936 10 12 . 1 1 9 9 HIS H H 1 8.668 0.02 . 1 . . . . 9 HIS N . 15936 10 13 . 1 1 10 10 HIS N N 15 120.850 0.2 . 1 . . . . 10 HIS H . 15936 10 14 . 1 1 10 10 HIS H H 1 8.650 0.02 . 1 . . . . 10 HIS N . 15936 10 15 . 1 1 11 11 SER N N 15 118.131 0.2 . 1 . . . . 11 SER H . 15936 10 16 . 1 1 11 11 SER H H 1 8.436 0.02 . 1 . . . . 11 SER N . 15936 10 17 . 1 1 12 12 SER N N 15 117.878 0.2 . 1 . . . . 12 SER H . 15936 10 18 . 1 1 12 12 SER H H 1 8.444 0.02 . 1 . . . . 12 SER N . 15936 10 19 . 1 1 13 13 GLY N N 15 109.931 0.2 . 1 . . . . 13 GLY H . 15936 10 20 . 1 1 13 13 GLY H H 1 8.305 0.02 . 1 . . . . 13 GLY N . 15936 10 21 . 1 1 14 14 LEU N N 15 121.919 0.2 . 1 . . . . 14 LEU H . 15936 10 22 . 1 1 14 14 LEU H H 1 8.114 0.02 . 1 . . . . 14 LEU N . 15936 10 23 . 1 1 15 15 VAL N N 15 123.670 0.2 . 1 . . . . 15 VAL H . 15936 10 24 . 1 1 15 15 VAL H H 1 8.207 0.02 . 1 . . . . 15 VAL N . 15936 10 25 . 1 1 17 17 ARG N N 15 121.214 0.2 . 1 . . . . 17 ARG H . 15936 10 26 . 1 1 17 17 ARG H H 1 8.243 0.02 . 1 . . . . 17 ARG N . 15936 10 27 . 1 1 18 18 GLY N N 15 109.349 0.2 . 1 . . . . 18 GLY H . 15936 10 28 . 1 1 18 18 GLY H H 1 8.341 0.02 . 1 . . . . 18 GLY N . 15936 10 29 . 1 1 19 19 SER N N 15 114.626 0.2 . 1 . . . . 19 SER H . 15936 10 30 . 1 1 19 19 SER H H 1 8.030 0.02 . 1 . . . . 19 SER N . 15936 10 31 . 1 1 20 20 HIS N N 15 119.402 0.2 . 1 . . . . 20 HIS H . 15936 10 32 . 1 1 20 20 HIS H H 1 8.446 0.02 . 1 . . . . 20 HIS N . 15936 10 33 . 1 1 21 21 MET N N 15 119.855 0.2 . 1 . . . . 21 MET H . 15936 10 34 . 1 1 21 21 MET H H 1 8.188 0.02 . 1 . . . . 21 MET N . 15936 10 35 . 1 1 22 22 LEU N N 15 121.571 0.2 . 1 . . . . 22 LEU H . 15936 10 36 . 1 1 22 22 LEU H H 1 7.952 0.02 . 1 . . . . 22 LEU N . 15936 10 37 . 1 1 23 23 GLU N N 15 119.824 0.2 . 1 . . . . 23 GLU H . 15936 10 38 . 1 1 23 23 GLU H H 1 7.952 0.02 . 1 . . . . 23 GLU N . 15936 10 39 . 1 1 24 24 LEU N N 15 124.857 0.2 . 1 . . . . 24 LEU H . 15936 10 40 . 1 1 24 24 LEU H H 1 8.190 0.02 . 1 . . . . 24 LEU N . 15936 10 41 . 1 1 26 26 LEU N N 15 120.521 0.2 . 1 . . . . 26 LEU H . 15936 10 42 . 1 1 26 26 LEU H H 1 8.164 0.02 . 1 . . . . 26 LEU N . 15936 10 43 . 1 1 27 27 ASP N N 15 118.679 0.2 . 1 . . . . 27 ASP H . 15936 10 44 . 1 1 27 27 ASP H H 1 8.261 0.02 . 1 . . . . 27 ASP N . 15936 10 45 . 1 1 28 28 SER N N 15 116.359 0.2 . 1 . . . . 28 SER H . 15936 10 46 . 1 1 28 28 SER H H 1 8.291 0.02 . 1 . . . . 28 SER N . 15936 10 47 . 1 1 29 29 ALA N N 15 124.586 0.2 . 1 . . . . 29 ALA H . 15936 10 48 . 1 1 29 29 ALA H H 1 8.243 0.02 . 1 . . . . 29 ALA N . 15936 10 49 . 1 1 30 30 THR N N 15 113.400 0.2 . 1 . . . . 30 THR H . 15936 10 50 . 1 1 30 30 THR H H 1 8.116 0.02 . 1 . . . . 30 THR N . 15936 10 51 . 1 1 31 31 THR N N 15 115.561 0.2 . 1 . . . . 31 THR H . 15936 10 52 . 1 1 31 31 THR H H 1 8.018 0.02 . 1 . . . . 31 THR N . 15936 10 53 . 1 1 32 32 GLU N N 15 120.399 0.2 . 1 . . . . 32 GLU H . 15936 10 54 . 1 1 32 32 GLU H H 1 8.238 0.02 . 1 . . . . 32 GLU N . 15936 10 55 . 1 1 33 33 SER N N 15 115.888 0.2 . 1 . . . . 33 SER H . 15936 10 56 . 1 1 33 33 SER H H 1 8.104 0.02 . 1 . . . . 33 SER N . 15936 10 57 . 1 1 34 34 LEU N N 15 123.185 0.2 . 1 . . . . 34 LEU H . 15936 10 58 . 1 1 34 34 LEU H H 1 8.110 0.02 . 1 . . . . 34 LEU N . 15936 10 59 . 1 1 35 35 ARG N N 15 121.114 0.2 . 1 . . . . 35 ARG H . 15936 10 60 . 1 1 35 35 ARG H H 1 8.067 0.02 . 1 . . . . 35 ARG N . 15936 10 61 . 1 1 36 36 ALA N N 15 122.269 0.2 . 1 . . . . 36 ALA H . 15936 10 62 . 1 1 36 36 ALA H H 1 8.097 0.02 . 1 . . . . 36 ALA N . 15936 10 63 . 1 1 37 37 ALA N N 15 122.806 0.2 . 1 . . . . 37 ALA H . 15936 10 64 . 1 1 37 37 ALA H H 1 8.170 0.02 . 1 . . . . 37 ALA N . 15936 10 65 . 1 1 38 38 THR N N 15 111.528 0.2 . 1 . . . . 38 THR H . 15936 10 66 . 1 1 38 38 THR H H 1 8.144 0.02 . 1 . . . . 38 THR N . 15936 10 67 . 1 1 39 39 HIS N N 15 118.829 0.2 . 1 . . . . 39 HIS H . 15936 10 68 . 1 1 39 39 HIS H H 1 8.145 0.02 . 1 . . . . 39 HIS N . 15936 10 69 . 1 1 40 40 ASP N N 15 120.008 0.2 . 1 . . . . 40 ASP H . 15936 10 70 . 1 1 40 40 ASP H H 1 8.423 0.02 . 1 . . . . 40 ASP N . 15936 10 71 . 1 1 41 41 VAL N N 15 121.179 0.2 . 1 . . . . 41 VAL H . 15936 10 72 . 1 1 41 41 VAL H H 1 8.150 0.02 . 1 . . . . 41 VAL N . 15936 10 73 . 1 1 42 42 LEU N N 15 123.449 0.2 . 1 . . . . 42 LEU H . 15936 10 74 . 1 1 42 42 LEU H H 1 8.106 0.02 . 1 . . . . 42 LEU N . 15936 10 75 . 1 1 43 43 ALA N N 15 123.639 0.2 . 1 . . . . 43 ALA H . 15936 10 76 . 1 1 43 43 ALA H H 1 8.002 0.02 . 1 . . . . 43 ALA N . 15936 10 77 . 1 1 44 44 GLY N N 15 106.424 0.2 . 1 . . . . 44 GLY H . 15936 10 78 . 1 1 44 44 GLY H H 1 7.985 0.02 . 1 . . . . 44 GLY N . 15936 10 79 . 1 1 45 45 LEU N N 15 121.587 0.2 . 1 . . . . 45 LEU H . 15936 10 80 . 1 1 45 45 LEU H H 1 7.948 0.02 . 1 . . . . 45 LEU N . 15936 10 81 . 1 1 46 46 THR N N 15 114.217 0.2 . 1 . . . . 46 THR H . 15936 10 82 . 1 1 46 46 THR H H 1 8.224 0.02 . 1 . . . . 46 THR N . 15936 10 83 . 1 1 47 47 ALA N N 15 123.277 0.2 . 1 . . . . 47 ALA H . 15936 10 84 . 1 1 47 47 ALA H H 1 7.928 0.02 . 1 . . . . 47 ALA N . 15936 10 85 . 1 1 48 48 ARG N N 15 118.222 0.2 . 1 . . . . 48 ARG H . 15936 10 86 . 1 1 48 48 ARG H H 1 8.165 0.02 . 1 . . . . 48 ARG N . 15936 10 87 . 1 1 49 49 GLU N N 15 117.336 0.2 . 1 . . . . 49 GLU H . 15936 10 88 . 1 1 49 49 GLU H H 1 7.657 0.02 . 1 . . . . 49 GLU N . 15936 10 89 . 1 1 50 50 ALA N N 15 120.252 0.2 . 1 . . . . 50 ALA H . 15936 10 90 . 1 1 50 50 ALA H H 1 8.252 0.02 . 1 . . . . 50 ALA N . 15936 10 91 . 1 1 51 51 LYS N N 15 117.427 0.2 . 1 . . . . 51 LYS H . 15936 10 92 . 1 1 51 51 LYS H H 1 7.665 0.02 . 1 . . . . 51 LYS N . 15936 10 93 . 1 1 52 52 VAL N N 15 120.116 0.2 . 1 . . . . 52 VAL H . 15936 10 94 . 1 1 52 52 VAL H H 1 7.896 0.02 . 1 . . . . 52 VAL N . 15936 10 95 . 1 1 53 53 LEU N N 15 123.565 0.2 . 1 . . . . 53 LEU H . 15936 10 96 . 1 1 53 53 LEU H H 1 8.087 0.02 . 1 . . . . 53 LEU N . 15936 10 97 . 1 1 54 54 ARG N N 15 119.763 0.2 . 1 . . . . 54 ARG H . 15936 10 98 . 1 1 54 54 ARG H H 1 8.112 0.02 . 1 . . . . 54 ARG N . 15936 10 99 . 1 1 55 55 MET N N 15 120.668 0.2 . 1 . . . . 55 MET H . 15936 10 100 . 1 1 55 55 MET H H 1 8.135 0.02 . 1 . . . . 55 MET N . 15936 10 101 . 1 1 56 56 ARG N N 15 120.992 0.2 . 1 . . . . 56 ARG H . 15936 10 102 . 1 1 56 56 ARG H H 1 8.057 0.02 . 1 . . . . 56 ARG N . 15936 10 103 . 1 1 57 57 PHE N N 15 120.164 0.2 . 1 . . . . 57 PHE H . 15936 10 104 . 1 1 57 57 PHE H H 1 8.155 0.02 . 1 . . . . 57 PHE N . 15936 10 105 . 1 1 58 58 GLY N N 15 107.115 0.2 . 1 . . . . 58 GLY H . 15936 10 106 . 1 1 58 58 GLY H H 1 8.118 0.02 . 1 . . . . 58 GLY N . 15936 10 107 . 1 1 59 59 ILE N N 15 118.034 0.2 . 1 . . . . 59 ILE H . 15936 10 108 . 1 1 59 59 ILE H H 1 7.696 0.02 . 1 . . . . 59 ILE N . 15936 10 109 . 1 1 60 60 ASP N N 15 121.923 0.2 . 1 . . . . 60 ASP H . 15936 10 110 . 1 1 60 60 ASP H H 1 8.428 0.02 . 1 . . . . 60 ASP N . 15936 10 111 . 1 1 61 61 MET N N 15 120.604 0.2 . 1 . . . . 61 MET H . 15936 10 112 . 1 1 61 61 MET H H 1 8.263 0.02 . 1 . . . . 61 MET N . 15936 10 113 . 1 1 62 62 ASN N N 15 118.853 0.2 . 1 . . . . 62 ASN H . 15936 10 114 . 1 1 62 62 ASN H H 1 8.305 0.02 . 1 . . . . 62 ASN N . 15936 10 115 . 1 1 63 63 THR N N 15 116.690 0.2 . 1 . . . . 63 THR H . 15936 10 116 . 1 1 63 63 THR H H 1 8.153 0.02 . 1 . . . . 63 THR N . 15936 10 117 . 1 1 64 64 ASP N N 15 120.636 0.2 . 1 . . . . 64 ASP H . 15936 10 118 . 1 1 64 64 ASP H H 1 8.451 0.02 . 1 . . . . 64 ASP N . 15936 10 119 . 1 1 65 65 TYR N N 15 120.864 0.2 . 1 . . . . 65 TYR H . 15936 10 120 . 1 1 65 65 TYR H H 1 8.033 0.02 . 1 . . . . 65 TYR N . 15936 10 121 . 1 1 66 66 THR N N 15 116.093 0.2 . 1 . . . . 66 THR H . 15936 10 122 . 1 1 66 66 THR H H 1 8.017 0.02 . 1 . . . . 66 THR N . 15936 10 123 . 1 1 67 67 LEU N N 15 123.084 0.2 . 1 . . . . 67 LEU H . 15936 10 124 . 1 1 67 67 LEU H H 1 8.008 0.02 . 1 . . . . 67 LEU N . 15936 10 125 . 1 1 68 68 GLU N N 15 120.412 0.2 . 1 . . . . 68 GLU H . 15936 10 126 . 1 1 68 68 GLU H H 1 8.108 0.02 . 1 . . . . 68 GLU N . 15936 10 127 . 1 1 69 69 GLU N N 15 120.533 0.2 . 1 . . . . 69 GLU H . 15936 10 128 . 1 1 69 69 GLU H H 1 8.125 0.02 . 1 . . . . 69 GLU N . 15936 10 129 . 1 1 70 70 VAL N N 15 120.367 0.2 . 1 . . . . 70 VAL H . 15936 10 130 . 1 1 70 70 VAL H H 1 8.024 0.02 . 1 . . . . 70 VAL N . 15936 10 131 . 1 1 71 71 GLY N N 15 106.896 0.2 . 1 . . . . 71 GLY H . 15936 10 132 . 1 1 71 71 GLY H H 1 8.234 0.02 . 1 . . . . 71 GLY N . 15936 10 133 . 1 1 72 72 LYS N N 15 120.799 0.2 . 1 . . . . 72 LYS H . 15936 10 134 . 1 1 72 72 LYS H H 1 8.105 0.02 . 1 . . . . 72 LYS N . 15936 10 135 . 1 1 73 73 GLN N N 15 119.410 0.2 . 1 . . . . 73 GLN H . 15936 10 136 . 1 1 73 73 GLN H H 1 8.284 0.02 . 1 . . . . 73 GLN N . 15936 10 137 . 1 1 75 75 ASP N N 15 120.258 0.2 . 1 . . . . 75 ASP H . 15936 10 138 . 1 1 75 75 ASP H H 1 8.219 0.02 . 1 . . . . 75 ASP N . 15936 10 139 . 1 1 76 76 VAL N N 15 120.663 0.2 . 1 . . . . 76 VAL H . 15936 10 140 . 1 1 76 76 VAL H H 1 8.089 0.02 . 1 . . . . 76 VAL N . 15936 10 141 . 1 1 77 77 THR N N 15 117.220 0.2 . 1 . . . . 77 THR H . 15936 10 142 . 1 1 77 77 THR H H 1 8.072 0.02 . 1 . . . . 77 THR N . 15936 10 143 . 1 1 78 78 ARG N N 15 122.155 0.2 . 1 . . . . 78 ARG H . 15936 10 144 . 1 1 78 78 ARG H H 1 8.144 0.02 . 1 . . . . 78 ARG N . 15936 10 145 . 1 1 79 79 GLU N N 15 118.038 0.2 . 1 . . . . 79 GLU H . 15936 10 146 . 1 1 79 79 GLU H H 1 8.032 0.02 . 1 . . . . 79 GLU N . 15936 10 147 . 1 1 80 80 ARG N N 15 121.609 0.2 . 1 . . . . 80 ARG H . 15936 10 148 . 1 1 80 80 ARG H H 1 8.228 0.02 . 1 . . . . 80 ARG N . 15936 10 149 . 1 1 81 81 ILE N N 15 121.221 0.2 . 1 . . . . 81 ILE H . 15936 10 150 . 1 1 81 81 ILE H H 1 8.039 0.02 . 1 . . . . 81 ILE N . 15936 10 151 . 1 1 82 82 ARG N N 15 123.581 0.2 . 1 . . . . 82 ARG H . 15936 10 152 . 1 1 82 82 ARG H H 1 8.219 0.02 . 1 . . . . 82 ARG N . 15936 10 153 . 1 1 83 83 GLN N N 15 121.261 0.2 . 1 . . . . 83 GLN H . 15936 10 154 . 1 1 83 83 GLN H H 1 8.242 0.02 . 1 . . . . 83 GLN N . 15936 10 155 . 1 1 84 84 ILE N N 15 122.410 0.2 . 1 . . . . 84 ILE H . 15936 10 156 . 1 1 84 84 ILE H H 1 8.191 0.02 . 1 . . . . 84 ILE N . 15936 10 157 . 1 1 85 85 GLU N N 15 119.142 0.2 . 1 . . . . 85 GLU H . 15936 10 158 . 1 1 85 85 GLU H H 1 8.618 0.02 . 1 . . . . 85 GLU N . 15936 10 159 . 1 1 86 86 ALA N N 15 123.370 0.2 . 1 . . . . 86 ALA H . 15936 10 160 . 1 1 86 86 ALA H H 1 8.168 0.02 . 1 . . . . 86 ALA N . 15936 10 161 . 1 1 87 87 LYS N N 15 117.438 0.2 . 1 . . . . 87 LYS H . 15936 10 162 . 1 1 87 87 LYS H H 1 7.743 0.02 . 1 . . . . 87 LYS N . 15936 10 163 . 1 1 88 88 ALA N N 15 121.234 0.2 . 1 . . . . 88 ALA H . 15936 10 164 . 1 1 88 88 ALA H H 1 7.953 0.02 . 1 . . . . 88 ALA N . 15936 10 165 . 1 1 89 89 LEU N N 15 120.962 0.2 . 1 . . . . 89 LEU H . 15936 10 166 . 1 1 89 89 LEU H H 1 8.014 0.02 . 1 . . . . 89 LEU N . 15936 10 167 . 1 1 90 90 ARG N N 15 121.068 0.2 . 1 . . . . 90 ARG H . 15936 10 168 . 1 1 90 90 ARG H H 1 8.134 0.02 . 1 . . . . 90 ARG N . 15936 10 169 . 1 1 91 91 LYS N N 15 121.824 0.2 . 1 . . . . 91 LYS H . 15936 10 170 . 1 1 91 91 LYS H H 1 8.109 0.02 . 1 . . . . 91 LYS N . 15936 10 171 . 1 1 92 92 LEU N N 15 119.249 0.2 . 1 . . . . 92 LEU H . 15936 10 172 . 1 1 92 92 LEU H H 1 7.798 0.02 . 1 . . . . 92 LEU N . 15936 10 173 . 1 1 93 93 ARG N N 15 121.376 0.2 . 1 . . . . 93 ARG H . 15936 10 174 . 1 1 93 93 ARG H H 1 8.247 0.02 . 1 . . . . 93 ARG N . 15936 10 175 . 1 1 94 94 HIS N N 15 118.314 0.2 . 1 . . . . 94 HIS H . 15936 10 176 . 1 1 94 94 HIS H H 1 8.161 0.02 . 1 . . . . 94 HIS N . 15936 10 177 . 1 1 96 96 SER N N 15 115.898 0.2 . 1 . . . . 96 SER H . 15936 10 178 . 1 1 96 96 SER H H 1 8.205 0.02 . 1 . . . . 96 SER N . 15936 10 179 . 1 1 97 97 ARG N N 15 122.402 0.2 . 1 . . . . 97 ARG H . 15936 10 180 . 1 1 97 97 ARG H H 1 8.709 0.02 . 1 . . . . 97 ARG N . 15936 10 181 . 1 1 98 98 SER N N 15 112.547 0.2 . 1 . . . . 98 SER H . 15936 10 182 . 1 1 98 98 SER H H 1 8.230 0.02 . 1 . . . . 98 SER N . 15936 10 183 . 1 1 99 99 GLU N N 15 121.319 0.2 . 1 . . . . 99 GLU H . 15936 10 184 . 1 1 99 99 GLU H H 1 7.745 0.02 . 1 . . . . 99 GLU N . 15936 10 185 . 1 1 100 100 VAL N N 15 120.423 0.2 . 1 . . . . 100 VAL H . 15936 10 186 . 1 1 100 100 VAL H H 1 7.932 0.02 . 1 . . . . 100 VAL N . 15936 10 187 . 1 1 101 101 LEU N N 15 122.491 0.2 . 1 . . . . 101 LEU H . 15936 10 188 . 1 1 101 101 LEU H H 1 7.872 0.02 . 1 . . . . 101 LEU N . 15936 10 189 . 1 1 102 102 ARG N N 15 121.662 0.2 . 1 . . . . 102 ARG H . 15936 10 190 . 1 1 102 102 ARG H H 1 8.216 0.02 . 1 . . . . 102 ARG N . 15936 10 191 . 1 1 103 103 SER N N 15 114.183 0.2 . 1 . . . . 103 SER H . 15936 10 192 . 1 1 103 103 SER H H 1 7.821 0.02 . 1 . . . . 103 SER N . 15936 10 193 . 1 1 104 104 PHE N N 15 121.755 0.2 . 1 . . . . 104 PHE H . 15936 10 194 . 1 1 104 104 PHE H H 1 8.149 0.02 . 1 . . . . 104 PHE N . 15936 10 195 . 1 1 105 105 LEU N N 15 118.957 0.2 . 1 . . . . 105 LEU H . 15936 10 196 . 1 1 105 105 LEU H H 1 7.911 0.02 . 1 . . . . 105 LEU N . 15936 10 197 . 1 1 106 106 ASP N N 15 116.850 0.2 . 1 . . . . 106 ASP H . 15936 10 198 . 1 1 106 106 ASP H H 1 7.968 0.02 . 1 . . . . 106 ASP N . 15936 10 199 . 1 1 107 107 ASP N N 15 121.814 0.2 . 1 . . . . 107 ASP H . 15936 10 200 . 1 1 107 107 ASP H H 1 7.798 0.02 . 1 . . . . 107 ASP N . 15936 10 stop_ save_