######################################## # Heteronuclear T2 relaxation values # ######################################## save_T2_pH7.4 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode T2_pH7.4 _Heteronucl_T2_list.Entry_ID 16907 _Heteronucl_T2_list.ID 1 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $pH_7.4 _Heteronucl_T2_list.Temp_calibration_method thermocouple _Heteronucl_T2_list.Temp_control_method 'temperature compensation block' _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nz _Heteronucl_T2_list.T2_val_units s _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '2D 1H-15N HSQC' . . . 16907 1 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 PHE N N 15 0.100 0.001 . . . . . . . 16907 1 2 . 1 1 4 4 GLY N N 15 0.091 0.001 . . . . . . . 16907 1 3 . 1 1 5 5 ALA N N 15 0.085 0.002 . . . . . . . 16907 1 4 . 1 1 6 6 ILE N N 15 0.094 0.002 . . . . . . . 16907 1 5 . 1 1 7 7 ALA N N 15 0.093 0.001 . . . . . . . 16907 1 6 . 1 1 8 8 GLY N N 15 0.091 0.000 . . . . . . . 16907 1 7 . 1 1 9 9 PHE N N 15 0.089 0.002 . . . . . . . 16907 1 8 . 1 1 10 10 ILE N N 15 0.092 0.002 . . . . . . . 16907 1 9 . 1 1 11 11 GLU N N 15 0.089 0.001 . . . . . . . 16907 1 10 . 1 1 12 12 GLY N N 15 0.098 0.001 . . . . . . . 16907 1 11 . 1 1 13 13 GLY N N 15 0.090 0.002 . . . . . . . 16907 1 12 . 1 1 14 14 TRP N N 15 0.095 0.002 . . . . . . . 16907 1 13 . 1 1 15 15 THR N N 15 0.095 0.001 . . . . . . . 16907 1 14 . 1 1 16 16 GLY N N 15 0.092 0.001 . . . . . . . 16907 1 15 . 1 1 17 17 MET N N 15 0.082 0.001 . . . . . . . 16907 1 16 . 1 1 18 18 ILE N N 15 0.093 0.000 . . . . . . . 16907 1 17 . 1 1 19 19 ASP N N 15 0.094 0.001 . . . . . . . 16907 1 18 . 1 1 20 20 GLY N N 15 0.095 0.002 . . . . . . . 16907 1 19 . 1 1 21 21 TRP N N 15 0.089 0.001 . . . . . . . 16907 1 20 . 1 1 22 22 TYR N N 15 0.090 0.001 . . . . . . . 16907 1 21 . 1 1 23 23 GLY N N 15 0.106 0.001 . . . . . . . 16907 1 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_T2_pH4.0 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode T2_pH4.0 _Heteronucl_T2_list.Entry_ID 16907 _Heteronucl_T2_list.ID 2 _Heteronucl_T2_list.Sample_condition_list_ID 2 _Heteronucl_T2_list.Sample_condition_list_label $pH_4.0 _Heteronucl_T2_list.Temp_calibration_method thermocouple _Heteronucl_T2_list.Temp_control_method 'temperature compensation block' _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nz _Heteronucl_T2_list.T2_val_units s _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 8 '2D 1H-15N HSQC' . . . 16907 2 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 2 2 LEU N N 15 0.071 0.002 . . . . . . . 16907 2 2 . 1 1 3 3 PHE N N 15 0.086 0.004 . . . . . . . 16907 2 3 . 1 1 4 4 GLY N N 15 0.090 0.002 . . . . . . . 16907 2 4 . 1 1 5 5 ALA N N 15 0.077 0.002 . . . . . . . 16907 2 5 . 1 1 6 6 ILE N N 15 0.094 0.002 . . . . . . . 16907 2 6 . 1 1 7 7 ALA N N 15 0.082 0.001 . . . . . . . 16907 2 7 . 1 1 8 8 GLY N N 15 0.087 0.002 . . . . . . . 16907 2 8 . 1 1 9 9 PHE N N 15 0.084 0.001 . . . . . . . 16907 2 9 . 1 1 10 10 ILE N N 15 0.085 0.002 . . . . . . . 16907 2 10 . 1 1 11 11 GLU N N 15 0.064 0.001 . . . . . . . 16907 2 11 . 1 1 12 12 GLY N N 15 0.088 0.000 . . . . . . . 16907 2 12 . 1 1 13 13 GLY N N 15 0.071 0.002 . . . . . . . 16907 2 13 . 1 1 14 14 TRP N N 15 0.068 0.002 . . . . . . . 16907 2 14 . 1 1 15 15 THR N N 15 0.090 0.001 . . . . . . . 16907 2 15 . 1 1 16 16 GLY N N 15 0.086 0.001 . . . . . . . 16907 2 16 . 1 1 17 17 MET N N 15 0.063 0.002 . . . . . . . 16907 2 17 . 1 1 18 18 ILE N N 15 0.083 0.001 . . . . . . . 16907 2 18 . 1 1 19 19 ASP N N 15 0.088 0.001 . . . . . . . 16907 2 19 . 1 1 20 20 GLY N N 15 0.090 0.001 . . . . . . . 16907 2 20 . 1 1 21 21 TRP N N 15 0.081 0.002 . . . . . . . 16907 2 21 . 1 1 22 22 TYR N N 15 0.071 0.001 . . . . . . . 16907 2 22 . 1 1 23 23 GLY N N 15 0.110 0.002 . . . . . . . 16907 2 stop_ save_