############################## # Heteronuclear NOE values # ############################## save_noe_apo_C-CaM _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode noe_apo_C-CaM _Heteronucl_NOE_list.Entry_ID 17881 _Heteronucl_NOE_list.ID 1 _Heteronucl_NOE_list.Sample_condition_list_ID 1 _Heteronucl_NOE_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_NOE_list.Spectrometer_frequency_1H 600.13 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'relative intensities' _Heteronucl_NOE_list.NOE_ref_val 1 _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details ; NOE values were measured from spectra with and without proton saturation recorded in an interleaved manner. Proton saturation was acquired with the use of 120o 1H pulse applied by every 5.0 s. In the case of the NONOE spectra, a net relaxation delay of 5.0 s was employed, while a relaxation delay of 2.0 s prior to a 3.0 s proton presaturation period was employed for the NOE spectra. ; _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 3 NOE . . . 17881 1 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 1 1 ASP N N 15 . 1 1 1 1 ASP H H 1 -0.0123 -0.0130 . . . 78 ASP N . 78 ASP H 17881 1 2 . 1 1 2 2 THR N N 15 . 1 1 2 2 THR H H 1 0.2181 0.0129 . . . 79 THR N . 79 THR H 17881 1 3 . 1 1 3 3 ASP N N 15 . 1 1 3 3 ASP H H 1 0.3210 0.0153 . . . 80 ASP N . 80 ASP H 17881 1 4 . 1 1 4 4 SER N N 15 . 1 1 4 4 SER H H 1 0.5244 0.0156 . . . 81 SER N . 81 SER H 17881 1 5 . 1 1 5 5 GLU N N 15 . 1 1 5 5 GLU H H 1 0.6796 0.0172 . . . 82 GLU N . 82 GLU H 17881 1 6 . 1 1 6 6 GLU N N 15 . 1 1 6 6 GLU H H 1 0.7140 0.0186 . . . 83 GLU N . 83 GLU H 17881 1 7 . 1 1 7 7 GLU N N 15 . 1 1 7 7 GLU H H 1 0.6804 0.0187 . . . 84 GLU N . 84 GLU H 17881 1 8 . 1 1 8 8 ILE N N 15 . 1 1 8 8 ILE H H 1 0.6896 0.0197 . . . 85 ILE N . 85 ILE H 17881 1 9 . 1 1 10 10 GLU N N 15 . 1 1 10 10 GLU H H 1 0.7301 0.0220 . . . 87 GLU N . 87 GLU H 17881 1 10 . 1 1 11 11 ALA N N 15 . 1 1 11 11 ALA H H 1 0.7421 0.0250 . . . 88 ALA N . 88 ALA H 17881 1 11 . 1 1 12 12 PHE N N 15 . 1 1 12 12 PHE H H 1 0.7433 0.0345 . . . 89 PHE N . 89 PHE H 17881 1 12 . 1 1 13 13 ARG N N 15 . 1 1 13 13 ARG H H 1 0.7616 0.0259 . . . 90 ARG N . 90 ARG H 17881 1 13 . 1 1 14 14 VAL N N 15 . 1 1 14 14 VAL H H 1 0.7670 0.0269 . . . 91 VAL N . 91 VAL H 17881 1 14 . 1 1 15 15 PHE N N 15 . 1 1 15 15 PHE H H 1 0.8185 0.0514 . . . 92 PHE N . 92 PHE H 17881 1 15 . 1 1 16 16 ASP N N 15 . 1 1 16 16 ASP H H 1 0.7855 0.0283 . . . 93 ASP N . 93 ASP H 17881 1 16 . 1 1 17 17 LYS N N 15 . 1 1 17 17 LYS H H 1 0.5787 0.0169 . . . 94 LYS N . 94 LYS H 17881 1 17 . 1 1 18 18 ASP N N 15 . 1 1 18 18 ASP H H 1 0.5665 0.0234 . . . 95 ASP N . 95 ASP H 17881 1 18 . 1 1 19 19 GLY N N 15 . 1 1 19 19 GLY H H 1 0.6816 0.0231 . . . 96 GLY N . 96 GLY H 17881 1 19 . 1 1 20 20 ASN N N 15 . 1 1 20 20 ASN H H 1 0.6542 0.0293 . . . 97 ASN N . 97 ASN H 17881 1 20 . 1 1 21 21 GLY N N 15 . 1 1 21 21 GLY H H 1 0.7596 0.0680 . . . 98 GLY N . 98 GLY H 17881 1 21 . 1 1 22 22 TYR N N 15 . 1 1 22 22 TYR H H 1 0.7768 0.0376 . . . 99 TYR N . 99 TYR H 17881 1 22 . 1 1 23 23 ILE N N 15 . 1 1 23 23 ILE H H 1 0.7160 0.0504 . . . 100 ILE N . 100 ILE H 17881 1 23 . 1 1 24 24 SER N N 15 . 1 1 24 24 SER H H 1 0.7153 0.0320 . . . 101 SER N . 101 SER H 17881 1 24 . 1 1 25 25 ALA N N 15 . 1 1 25 25 ALA H H 1 0.8828 0.0249 . . . 102 ALA N . 102 ALA H 17881 1 25 . 1 1 26 26 ALA N N 15 . 1 1 26 26 ALA H H 1 0.7225 0.0170 . . . 103 ALA N . 103 ALA H 17881 1 26 . 1 1 27 27 GLU N N 15 . 1 1 27 27 GLU H H 1 0.7530 0.0279 . . . 104 GLU N . 104 GLU H 17881 1 27 . 1 1 28 28 LEU N N 15 . 1 1 28 28 LEU H H 1 0.7886 0.0243 . . . 105 LEU N . 105 LEU H 17881 1 28 . 1 1 29 29 ARG N N 15 . 1 1 29 29 ARG H H 1 0.7672 0.0220 . . . 106 ARG N . 106 ARG H 17881 1 29 . 1 1 30 30 HIS N N 15 . 1 1 30 30 HIS H H 1 0.7752 0.0215 . . . 107 HIS N . 107 HIS H 17881 1 30 . 1 1 31 31 VAL N N 15 . 1 1 31 31 VAL H H 1 0.7777 0.0215 . . . 108 VAL N . 108 VAL H 17881 1 31 . 1 1 32 32 MET N N 15 . 1 1 32 32 MET H H 1 0.7391 0.0277 . . . 109 MET N . 109 MET H 17881 1 32 . 1 1 33 33 THR N N 15 . 1 1 33 33 THR H H 1 0.7212 0.0249 . . . 110 THR N . 110 THR H 17881 1 33 . 1 1 34 34 ASN N N 15 . 1 1 34 34 ASN H H 1 0.7044 0.0302 . . . 111 ASN N . 111 ASN H 17881 1 34 . 1 1 35 35 LEU N N 15 . 1 1 35 35 LEU H H 1 0.6899 0.0219 . . . 112 LEU N . 112 LEU H 17881 1 35 . 1 1 36 36 GLY N N 15 . 1 1 36 36 GLY H H 1 0.6666 0.0199 . . . 113 GLY N . 113 GLY H 17881 1 36 . 1 1 37 37 GLU N N 15 . 1 1 37 37 GLU H H 1 0.5925 0.0192 . . . 114 GLU N . 114 GLU H 17881 1 37 . 1 1 38 38 LYS N N 15 . 1 1 38 38 LYS H H 1 0.4195 0.0186 . . . 115 LYS N . 115 LYS H 17881 1 38 . 1 1 39 39 LEU N N 15 . 1 1 39 39 LEU H H 1 0.5653 0.0251 . . . 116 LEU N . 116 LEU H 17881 1 39 . 1 1 40 40 THR N N 15 . 1 1 40 40 THR H H 1 0.6128 0.0294 . . . 117 THR N . 117 THR H 17881 1 40 . 1 1 41 41 ASP N N 15 . 1 1 41 41 ASP H H 1 0.7791 0.0191 . . . 118 ASP N . 118 ASP H 17881 1 41 . 1 1 42 42 GLU N N 15 . 1 1 42 42 GLU H H 1 0.7117 0.0182 . . . 119 GLU N . 119 GLU H 17881 1 42 . 1 1 43 43 GLU N N 15 . 1 1 43 43 GLU H H 1 0.7812 0.0225 . . . 120 GLU N . 120 GLU H 17881 1 43 . 1 1 44 44 VAL N N 15 . 1 1 44 44 VAL H H 1 0.7484 0.0184 . . . 121 VAL N . 121 VAL H 17881 1 44 . 1 1 46 46 GLU N N 15 . 1 1 46 46 GLU H H 1 0.7713 0.0180 . . . 123 GLU N . 123 GLU H 17881 1 45 . 1 1 47 47 MET N N 15 . 1 1 47 47 MET H H 1 0.7130 0.0202 . . . 124 MET N . 124 MET H 17881 1 46 . 1 1 48 48 ILE N N 15 . 1 1 48 48 ILE H H 1 0.7137 0.0221 . . . 125 ILE N . 125 ILE H 17881 1 47 . 1 1 49 49 ARG N N 15 . 1 1 49 49 ARG H H 1 0.6835 0.0204 . . . 126 ARG N . 126 ARG H 17881 1 48 . 1 1 50 50 GLU N N 15 . 1 1 50 50 GLU H H 1 0.6934 0.0292 . . . 127 GLU N . 127 GLU H 17881 1 49 . 1 1 51 51 ALA N N 15 . 1 1 51 51 ALA H H 1 0.7059 0.0208 . . . 128 ALA N . 128 ALA H 17881 1 50 . 1 1 52 52 ASP N N 15 . 1 1 52 52 ASP H H 1 0.6238 0.0247 . . . 129 ASP N . 129 ASP H 17881 1 51 . 1 1 53 53 ILE N N 15 . 1 1 53 53 ILE H H 1 0.6994 0.0265 . . . 130 ILE N . 130 ILE H 17881 1 52 . 1 1 54 54 ASP N N 15 . 1 1 54 54 ASP H H 1 0.5856 0.0301 . . . 131 ASP N . 131 ASP H 17881 1 53 . 1 1 55 55 GLY N N 15 . 1 1 55 55 GLY H H 1 0.6014 0.0251 . . . 132 GLY N . 132 GLY H 17881 1 54 . 1 1 56 56 ASP N N 15 . 1 1 56 56 ASP H H 1 0.6116 0.0241 . . . 133 ASP N . 133 ASP H 17881 1 55 . 1 1 57 57 GLY N N 15 . 1 1 57 57 GLY H H 1 0.6474 0.0434 . . . 134 GLY N . 134 GLY H 17881 1 56 . 1 1 58 58 GLN N N 15 . 1 1 58 58 GLN H H 1 0.5747 0.0259 . . . 135 GLN N . 135 GLN H 17881 1 57 . 1 1 59 59 VAL N N 15 . 1 1 59 59 VAL H H 1 0.6943 0.0471 . . . 136 VAL N . 136 VAL H 17881 1 58 . 1 1 60 60 ASN N N 15 . 1 1 60 60 ASN H H 1 0.7293 0.0249 . . . 137 ASN N . 137 ASN H 17881 1 59 . 1 1 61 61 TYR N N 15 . 1 1 61 61 TYR H H 1 0.7633 0.0447 . . . 138 TYR N . 138 TYR H 17881 1 60 . 1 1 62 62 GLU N N 15 . 1 1 62 62 GLU H H 1 0.7494 0.0374 . . . 139 GLU N . 139 GLU H 17881 1 61 . 1 1 63 63 GLU N N 15 . 1 1 63 63 GLU H H 1 0.7968 0.0281 . . . 140 GLU N . 140 GLU H 17881 1 62 . 1 1 64 64 PHE N N 15 . 1 1 64 64 PHE H H 1 0.7353 0.0373 . . . 141 PHE N . 141 PHE H 17881 1 63 . 1 1 65 65 VAL N N 15 . 1 1 65 65 VAL H H 1 0.8090 0.0242 . . . 142 VAL N . 142 VAL H 17881 1 64 . 1 1 66 66 GLN N N 15 . 1 1 66 66 GLN H H 1 0.7850 0.0260 . . . 143 GLN N . 143 GLN H 17881 1 65 . 1 1 67 67 MET N N 15 . 1 1 67 67 MET H H 1 0.6983 0.0195 . . . 144 MET N . 144 MET H 17881 1 66 . 1 1 68 68 MET N N 15 . 1 1 68 68 MET H H 1 0.6810 0.0215 . . . 145 MET N . 145 MET H 17881 1 67 . 1 1 69 69 THR N N 15 . 1 1 69 69 THR H H 1 0.6286 0.0233 . . . 146 THR N . 146 THR H 17881 1 68 . 1 1 70 70 ALA N N 15 . 1 1 70 70 ALA H H 1 0.4811 0.0150 . . . 147 ALA N . 147 ALA H 17881 1 69 . 1 1 71 71 LYS N N 15 . 1 1 71 71 LYS H H 1 -0.0446 -0.0111 . . . 148 LYS N . 148 LYS H 17881 1 stop_ save_