######################################## # Heteronuclear T2 relaxation values # ######################################## save_heteronuclear_T2_list_1 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronuclear_T2_list_1 _Heteronucl_T2_list.Entry_ID 18971 _Heteronucl_T2_list.ID 1 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'no temperature control applied' _Heteronucl_T2_list.Spectrometer_frequency_1H 600.17 _Heteronucl_T2_list.T2_coherence_type S(+,-) _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 25 '2D 1H-15N R2 relaxation' . . . 18971 1 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 MET N N 15 3.72 0.268 . . . . 418 M . 18971 1 2 . 1 1 4 4 GLU N N 15 2.51 0.0878 . . . . 419 E . 18971 1 3 . 1 1 5 5 GLN N N 15 2.94 0.1029 . . . . 420 Q . 18971 1 4 . 1 1 6 6 GLY N N 15 3.34 0.1169 . . . . 421 G . 18971 1 5 . 1 1 7 7 PHE N N 15 4.03 0.1411 . . . . 422 F . 18971 1 6 . 1 1 8 8 LEU N N 15 5.02 0.1757 . . . . 423 L . 18971 1 7 . 1 1 10 10 LYS N N 15 5.67 0.1985 . . . . 425 K . 18971 1 8 . 1 1 12 12 TRP N N 15 6.85 0.2398 . . . . 427 W . 18971 1 9 . 1 1 13 13 GLU N N 15 6.09 0.2132 . . . . 428 E . 18971 1 10 . 1 1 14 14 VAL N N 15 5.96 0.2086 . . . . 429 V . 18971 1 11 . 1 1 15 15 ARG N N 15 7.87 0.2755 . . . . 430 R . 18971 1 12 . 1 1 16 16 HIS N N 15 5.73 0.2006 . . . . 431 H . 18971 1 13 . 1 1 17 17 ALA N N 15 5.85 0.2048 . . . . 432 A . 18971 1 14 . 1 1 19 19 ASN N N 15 5.93 0.2076 . . . . 434 N . 18971 1 15 . 1 1 20 20 GLY N N 15 5.78 0.2023 . . . . 435 G . 18971 1 16 . 1 1 21 21 ARG N N 15 6.26 0.2191 . . . . 436 R . 18971 1 17 . 1 1 23 23 PHE N N 15 6.24 0.2184 . . . . 438 F . 18971 1 18 . 1 1 24 24 PHE N N 15 6.46 0.2261 . . . . 439 F . 18971 1 19 . 1 1 25 25 ILE N N 15 6.7 0.2345 . . . . 440 I . 18971 1 20 . 1 1 26 26 ASP N N 15 6.17 0.216 . . . . 441 D . 18971 1 21 . 1 1 27 27 HIS N N 15 6.29 0.2202 . . . . 442 H . 18971 1 22 . 1 1 28 28 ASN N N 15 6.49 0.2272 . . . . 443 N . 18971 1 23 . 1 1 29 29 THR N N 15 8.2 0.287 . . . . 444 T . 18971 1 24 . 1 1 30 30 LYS N N 15 6.79 0.2377 . . . . 445 K . 18971 1 25 . 1 1 31 31 THR N N 15 8.34 0.2919 . . . . 446 T . 18971 1 26 . 1 1 32 32 THR N N 15 9.92 0.3472 . . . . 447 T . 18971 1 27 . 1 1 34 34 TRP N N 15 6.21 0.2174 . . . . 449 W . 18971 1 28 . 1 1 35 35 GLU N N 15 6.53 0.2286 . . . . 450 E . 18971 1 29 . 1 1 36 36 ASP N N 15 5.63 0.1971 . . . . 451 D . 18971 1 30 . 1 1 38 38 ARG N N 15 5.96 0.2086 . . . . 453 R . 18971 1 31 . 1 1 39 39 LEU N N 15 5.83 0.2041 . . . . 454 L . 18971 1 32 . 1 1 40 40 LYS N N 15 3.91 0.1369 . . . . 455 K . 18971 1 33 . 1 1 41 41 ILE N N 15 2.59 0.0907 . . . . 456 I . 18971 1 34 . 1 1 43 43 ALA N N 15 1.05 0.0368 . . . . 458 A . 18971 1 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_heteronuclear_T2_list_2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronuclear_T2_list_2 _Heteronucl_T2_list.Entry_ID 18971 _Heteronucl_T2_list.ID 2 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'no temperature control applied' _Heteronucl_T2_list.Spectrometer_frequency_1H 799.857 _Heteronucl_T2_list.T2_coherence_type S(+,-) _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 28 '2D 1H-15N R1rho relaxation' . . . 18971 2 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 MET N N 15 4.301 0.1505 . . . . 418 M . 18971 2 2 . 1 1 4 4 GLU N N 15 2.982 0.1044 . . . . 419 E . 18971 2 3 . 1 1 5 5 GLN N N 15 3.2 0.112 . . . . 420 Q . 18971 2 4 . 1 1 6 6 GLY N N 15 3.615 0.1265 . . . . 421 G . 18971 2 5 . 1 1 7 7 PHE N N 15 4.463 0.1562 . . . . 422 F . 18971 2 6 . 1 1 8 8 LEU N N 15 5.912 0.2069 . . . . 423 L . 18971 2 7 . 1 1 10 10 LYS N N 15 6.415 0.2245 . . . . 425 K . 18971 2 8 . 1 1 12 12 TRP N N 15 8.318 0.2911 . . . . 427 W . 18971 2 9 . 1 1 13 13 GLU N N 15 6.929 0.2425 . . . . 428 E . 18971 2 10 . 1 1 14 14 VAL N N 15 6.724 0.2353 . . . . 429 V . 18971 2 11 . 1 1 15 15 ARG N N 15 7.413 0.2595 . . . . 430 R . 18971 2 12 . 1 1 16 16 HIS N N 15 6.673 0.2336 . . . . 431 H . 18971 2 13 . 1 1 17 17 ALA N N 15 7.067 0.2473 . . . . 432 A . 18971 2 14 . 1 1 19 19 ASN N N 15 7.531 0.2636 . . . . 434 N . 18971 2 15 . 1 1 20 20 GLY N N 15 6.573 0.2301 . . . . 435 G . 18971 2 16 . 1 1 21 21 ARG N N 15 7.001 0.245 . . . . 436 R . 18971 2 17 . 1 1 23 23 PHE N N 15 7.027 0.2459 . . . . 438 F . 18971 2 18 . 1 1 24 24 PHE N N 15 7.974 0.2791 . . . . 439 F . 18971 2 19 . 1 1 25 25 ILE N N 15 6.855 0.2399 . . . . 440 I . 18971 2 20 . 1 1 26 26 ASP N N 15 6.969 0.2439 . . . . 441 D . 18971 2 21 . 1 1 27 27 HIS N N 15 7.304 0.2556 . . . . 442 H . 18971 2 22 . 1 1 28 28 ASN N N 15 8.092 0.2832 . . . . 443 N . 18971 2 23 . 1 1 29 29 THR N N 15 15.35 0.5373 . . . . 444 T . 18971 2 24 . 1 1 30 30 LYS N N 15 8.539 0.2989 . . . . 445 K . 18971 2 25 . 1 1 31 31 THR N N 15 13.761 0.4816 . . . . 446 T . 18971 2 26 . 1 1 32 32 THR N N 15 17.396 0.6089 . . . . 447 T . 18971 2 27 . 1 1 34 34 TRP N N 15 7.051 0.2468 . . . . 449 W . 18971 2 28 . 1 1 35 35 GLU N N 15 7.993 0.2798 . . . . 450 E . 18971 2 29 . 1 1 36 36 ASP N N 15 6.805 0.2382 . . . . 451 D . 18971 2 30 . 1 1 38 38 ARG N N 15 6.591 0.2307 . . . . 453 R . 18971 2 31 . 1 1 39 39 LEU N N 15 6.693 0.2343 . . . . 454 L . 18971 2 32 . 1 1 40 40 LYS N N 15 4.477 0.1567 . . . . 455 K . 18971 2 33 . 1 1 41 41 ILE N N 15 3.003 0.1051 . . . . 456 I . 18971 2 34 . 1 1 43 43 ALA N N 15 1.699 0.0595 . . . . 458 A . 18971 2 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_heteronuclear_T2_list_3 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronuclear_T2_list_3 _Heteronucl_T2_list.Entry_ID 18971 _Heteronucl_T2_list.ID 3 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'no temperature control applied' _Heteronucl_T2_list.Spectrometer_frequency_1H 899.864 _Heteronucl_T2_list.T2_coherence_type S(+,-) _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 28 '2D 1H-15N R1rho relaxation' . . . 18971 3 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 MET N N 15 4.801 0.168 . . . . 418 M . 18971 3 2 . 1 1 4 4 GLU N N 15 2.911 0.1019 . . . . 419 E . 18971 3 3 . 1 1 5 5 GLN N N 15 3.483 0.1219 . . . . 420 Q . 18971 3 4 . 1 1 6 6 GLY N N 15 3.814 0.1335 . . . . 421 G . 18971 3 5 . 1 1 7 7 PHE N N 15 4.99 0.1747 . . . . 422 F . 18971 3 6 . 1 1 8 8 LEU N N 15 6.257 0.219 . . . . 423 L . 18971 3 7 . 1 1 10 10 LYS N N 15 6.994 0.2448 . . . . 425 K . 18971 3 8 . 1 1 12 12 TRP N N 15 8.972 0.314 . . . . 427 W . 18971 3 9 . 1 1 13 13 GLU N N 15 7.607 0.2662 . . . . 428 E . 18971 3 10 . 1 1 14 14 VAL N N 15 7.517 0.2631 . . . . 429 V . 18971 3 11 . 1 1 15 15 ARG N N 15 7.82 0.2737 . . . . 430 R . 18971 3 12 . 1 1 16 16 HIS N N 15 7.477 0.2617 . . . . 431 H . 18971 3 13 . 1 1 17 17 ALA N N 15 7.158 0.2505 . . . . 432 A . 18971 3 14 . 1 1 19 19 ASN N N 15 8.469 0.2964 . . . . 434 N . 18971 3 15 . 1 1 20 20 GLY N N 15 6.785 0.2375 . . . . 435 G . 18971 3 16 . 1 1 21 21 ARG N N 15 7.561 0.2646 . . . . 436 R . 18971 3 17 . 1 1 23 23 PHE N N 15 7.576 0.2652 . . . . 438 F . 18971 3 18 . 1 1 24 24 PHE N N 15 8.687 0.304 . . . . 439 F . 18971 3 19 . 1 1 25 25 ILE N N 15 7.18 0.2513 . . . . 440 I . 18971 3 20 . 1 1 26 26 ASP N N 15 7.255 0.2539 . . . . 441 D . 18971 3 21 . 1 1 27 27 HIS N N 15 7.634 0.2672 . . . . 442 H . 18971 3 22 . 1 1 28 28 ASN N N 15 8.92 0.3122 . . . . 443 N . 18971 3 23 . 1 1 29 29 THR N N 15 17.887 0.626 . . . . 444 T . 18971 3 24 . 1 1 30 30 LYS N N 15 10.135 0.3547 . . . . 445 K . 18971 3 25 . 1 1 31 31 THR N N 15 15.561 0.5446 . . . . 446 T . 18971 3 26 . 1 1 32 32 THR N N 15 19.882 0.6959 . . . . 447 T . 18971 3 27 . 1 1 34 34 TRP N N 15 7.449 0.2607 . . . . 449 W . 18971 3 28 . 1 1 35 35 GLU N N 15 8.675 0.3036 . . . . 450 E . 18971 3 29 . 1 1 36 36 ASP N N 15 7.433 0.2602 . . . . 451 D . 18971 3 30 . 1 1 38 38 ARG N N 15 7.279 0.2548 . . . . 453 R . 18971 3 31 . 1 1 39 39 LEU N N 15 7.125 0.2494 . . . . 454 L . 18971 3 32 . 1 1 40 40 LYS N N 15 4.613 0.1615 . . . . 455 K . 18971 3 33 . 1 1 41 41 ILE N N 15 3.002 0.1051 . . . . 456 I . 18971 3 34 . 1 1 43 43 ALA N N 15 1.501 0.0525 . . . . 458 A . 18971 3 stop_ save_