################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chem_shift_list_1 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chem_shift_list_1 _Assigned_chem_shift_list.Entry_ID 26024 _Assigned_chem_shift_list.ID 1 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_1 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 1 '2D 1H-13C HSQC' . . . 26024 1 2 '3D HCCH-TOCSY' . . . 26024 1 3 '2D NOESY13CHSQC' . . . 26024 1 4 '2D HCNTROSY' . . . 26024 1 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 1 1 G H1' H 1 5.891 . . . . . . A 1 G H1' . 26024 1 2 . 1 1 1 1 G H2' H 1 4.947 . . . . . . A 1 G H2' . 26024 1 3 . 1 1 1 1 G H3' H 1 4.577 . . . . . . A 1 G H3' . 26024 1 4 . 1 1 1 1 G H5' H 1 4.349 . . . . . . A 1 G H5' . 26024 1 5 . 1 1 1 1 G H8 H 1 8.265 . . . . . . A 1 G H8 . 26024 1 6 . 1 1 2 2 G H1' H 1 5.850 . . . . . . A 2 G H1' . 26024 1 7 . 1 1 2 2 G H2' H 1 4.576 . . . . . . A 2 G H2' . 26024 1 8 . 1 1 2 2 G H3' H 1 4.199 . . . . . . A 2 G H3' . 26024 1 9 . 1 1 2 2 G H8 H 1 7.654 . . . . . . A 2 G H8 . 26024 1 10 . 1 1 3 3 A H1' H 1 6.014 . . . . . . A 3 A H1' . 26024 1 11 . 1 1 3 3 A H2 H 1 7.778 . . . . . . A 3 A H2 . 26024 1 12 . 1 1 3 3 A H2' H 1 4.619 . . . . . . A 3 A H2' . 26024 1 13 . 1 1 3 3 A H3' H 1 4.630 . . . . . . A 3 A H3' . 26024 1 14 . 1 1 3 3 A H4' H 1 4.497 . . . . . . A 3 A H4' . 26024 1 15 . 1 1 3 3 A H5' H 1 5.032 . . . . . . A 3 A H5' . 26024 1 16 . 1 1 3 3 A H5'' H 1 4.098 . . . . . . A 3 A H5'' . 26024 1 17 . 1 1 3 3 A H8 H 1 7.785 . . . . . . A 3 A H8 . 26024 1 18 . 1 1 3 3 A C1' C 13 92.708 . . . . . . A 3 A C1' . 26024 1 19 . 1 1 3 3 A C2 C 13 154.162 . . . . . . A 3 A C2 . 26024 1 20 . 1 1 3 3 A C2' C 13 72.493 . . . . . . A 3 A C2' . 26024 1 21 . 1 1 3 3 A C3' C 13 75.694 . . . . . . A 3 A C3' . 26024 1 22 . 1 1 3 3 A C4' C 13 81.960 . . . . . . A 3 A C4' . 26024 1 23 . 1 1 3 3 A C5' C 13 64.625 . . . . . . A 3 A C5' . 26024 1 24 . 1 1 3 3 A C8 C 13 139.492 . . . . . . A 3 A C8 . 26024 1 25 . 1 1 3 3 A N9 N 15 171.384 . . . . . . A 3 A N9 . 26024 1 26 . 1 1 4 4 C H1' H 1 5.411 . . . . . . A 4 C H1' . 26024 1 27 . 1 1 4 4 C H2' H 1 4.473 . . . . . . A 4 C H2' . 26024 1 28 . 1 1 4 4 C H3' H 1 4.428 . . . . . . A 4 C H3' . 26024 1 29 . 1 1 4 4 C H5 H 1 5.278 . . . . . . A 4 C H5 . 26024 1 30 . 1 1 4 4 C H6 H 1 7.572 . . . . . . A 4 C H6 . 26024 1 31 . 1 1 5 5 G H1' H 1 5.724 . . . . . . A 5 G H1' . 26024 1 32 . 1 1 5 5 G H2' H 1 4.433 . . . . . . A 5 G H2' . 26024 1 33 . 1 1 5 5 G H3' H 1 4.536 . . . . . . A 5 G H3' . 26024 1 34 . 1 1 5 5 G H5' H 1 4.099 . . . . . . A 5 G H5' . 26024 1 35 . 1 1 5 5 G H5'' H 1 4.027 . . . . . . A 5 G H5'' . 26024 1 36 . 1 1 5 5 G H8 H 1 7.545 . . . . . . A 5 G H8 . 26024 1 37 . 1 1 6 6 U H1' H 1 5.692 . . . . . . A 6 U H1' . 26024 1 38 . 1 1 6 6 U H2' H 1 4.514 . . . . . . A 6 U H2' . 26024 1 39 . 1 1 6 6 U H3' H 1 4.546 . . . . . . A 6 U H3' . 26024 1 40 . 1 1 6 6 U H4' H 1 4.398 . . . . . . A 6 U H4' . 26024 1 41 . 1 1 6 6 U H5 H 1 5.073 . . . . . . A 6 U H5 . 26024 1 42 . 1 1 6 6 U H5' H 1 4.246 . . . . . . A 6 U H5' . 26024 1 43 . 1 1 6 6 U H5'' H 1 4.051 . . . . . . A 6 U H5'' . 26024 1 44 . 1 1 6 6 U H6 H 1 7.878 . . . . . . A 6 U H6 . 26024 1 45 . 1 1 6 6 U C1' C 13 93.587 . . . . . . A 6 U C1' . 26024 1 46 . 1 1 6 6 U C2' C 13 75.329 . . . . . . A 6 U C2' . 26024 1 47 . 1 1 6 6 U C3' C 13 72.058 . . . . . . A 6 U C3' . 26024 1 48 . 1 1 6 6 U C4' C 13 82.049 . . . . . . A 6 U C4' . 26024 1 49 . 1 1 6 6 U C5 C 13 103.448 . . . . . . A 6 U C5 . 26024 1 50 . 1 1 6 6 U C5' C 13 64.298 . . . . . . A 6 U C5' . 26024 1 51 . 1 1 6 6 U C6 C 13 141.887 . . . . . . A 6 U C6 . 26024 1 52 . 1 1 6 6 U N1 N 15 147.021 . . . . . . A 6 U N1 . 26024 1 53 . 1 1 7 7 U H1' H 1 6.049 . . . . . . A 7 U H1' . 26024 1 54 . 1 1 7 7 U H2' H 1 4.908 . . . . . . A 7 U H2' . 26024 1 55 . 1 1 7 7 U H3' H 1 4.584 . . . . . . A 7 U H3' . 26024 1 56 . 1 1 7 7 U H4' H 1 4.631 . . . . . . A 7 U H4' . 26024 1 57 . 1 1 7 7 U H5 H 1 5.950 . . . . . . A 7 U H5 . 26024 1 58 . 1 1 7 7 U H5' H 1 4.283 . . . . . . A 7 U H5' . 26024 1 59 . 1 1 7 7 U H5'' H 1 4.377 . . . . . . A 7 U H5'' . 26024 1 60 . 1 1 7 7 U H6 H 1 7.949 . . . . . . A 7 U H6 . 26024 1 61 . 1 1 7 7 U C1' C 13 94.720 . . . . . . A 7 U C1' . 26024 1 62 . 1 1 7 7 U C2' C 13 75.676 . . . . . . A 7 U C2' . 26024 1 63 . 1 1 7 7 U C4' C 13 84.343 . . . . . . A 7 U C4' . 26024 1 64 . 1 1 7 7 U C5' C 13 68.874 . . . . . . A 7 U C5' . 26024 1 65 . 1 1 7 7 U C6 C 13 143.478 . . . . . . A 7 U C6 . 26024 1 66 . 1 1 7 7 U N1 N 15 143.938 . . . . . . A 7 U N1 . 26024 1 67 . 1 1 8 8 A H1' H 1 6.086 . . . . . . A 8 A H1' . 26024 1 68 . 1 1 8 8 A H2 H 1 7.904 . . . . . . A 8 A H2 . 26024 1 69 . 1 1 8 8 A H2' H 1 4.541 . . . . . . A 8 A H2' . 26024 1 70 . 1 1 8 8 A H3' H 1 4.829 . . . . . . A 8 A H3' . 26024 1 71 . 1 1 8 8 A H4' H 1 4.527 . . . . . . A 8 A H4' . 26024 1 72 . 1 1 8 8 A H5' H 1 4.311 . . . . . . A 8 A H5' . 26024 1 73 . 1 1 8 8 A H5'' H 1 4.138 . . . . . . A 8 A H5'' . 26024 1 74 . 1 1 8 8 A H8 H 1 8.434 . . . . . . A 8 A H8 . 26024 1 75 . 1 1 8 8 A C1' C 13 90.042 . . . . . . A 8 A C1' . 26024 1 76 . 1 1 8 8 A C2' C 13 75.466 . . . . . . A 8 A C2' . 26024 1 77 . 1 1 8 8 A C3' C 13 77.762 . . . . . . A 8 A C3' . 26024 1 78 . 1 1 8 8 A C4' C 13 84.961 . . . . . . A 8 A C4' . 26024 1 79 . 1 1 8 8 A C5' C 13 67.727 . . . . . . A 8 A C5' . 26024 1 80 . 1 1 8 8 A C8 C 13 142.115 . . . . . . A 8 A C8 . 26024 1 81 . 1 1 9 9 A H1' H 1 6.060 . . . . . . A 9 A H1' . 26024 1 82 . 1 1 9 9 A H2 H 1 8.057 . . . . . . A 9 A H2 . 26024 1 83 . 1 1 9 9 A H2' H 1 4.739 . . . . . . A 9 A H2' . 26024 1 84 . 1 1 9 9 A H3' H 1 4.689 . . . . . . A 9 A H3' . 26024 1 85 . 1 1 9 9 A H4' H 1 4.539 . . . . . . A 9 A H4' . 26024 1 86 . 1 1 9 9 A H5' H 1 4.518 . . . . . . A 9 A H5' . 26024 1 87 . 1 1 9 9 A H5'' H 1 4.270 . . . . . . A 9 A H5'' . 26024 1 88 . 1 1 9 9 A H8 H 1 8.319 . . . . . . A 9 A H8 . 26024 1 89 . 1 1 9 9 A C1' C 13 92.563 . . . . . . A 9 A C1' . 26024 1 90 . 1 1 9 9 A C2 C 13 154.767 . . . . . . A 9 A C2 . 26024 1 91 . 1 1 9 9 A C2' C 13 73.699 . . . . . . A 9 A C2' . 26024 1 92 . 1 1 9 9 A C3' C 13 76.900 . . . . . . A 9 A C3' . 26024 1 93 . 1 1 9 9 A C4' C 13 82.824 . . . . . . A 9 A C4' . 26024 1 94 . 1 1 9 9 A C5' C 13 65.842 . . . . . . A 9 A C5' . 26024 1 95 . 1 1 9 9 A C8 C 13 142.367 . . . . . . A 9 A C8 . 26024 1 96 . 1 1 9 9 A N9 N 15 168.640 . . . . . . A 9 A N9 . 26024 1 97 . 1 1 10 10 A H1' H 1 5.683 . . . . . . A 10 A H1' . 26024 1 98 . 1 1 10 10 A H2 H 1 7.611 . . . . . . A 10 A H2 . 26024 1 99 . 1 1 10 10 A H2' H 1 4.556 . . . . . . A 10 A H2' . 26024 1 100 . 1 1 10 10 A H3' H 1 4.541 . . . . . . A 10 A H3' . 26024 1 101 . 1 1 10 10 A H4' H 1 4.533 . . . . . . A 10 A H4' . 26024 1 102 . 1 1 10 10 A H5' H 1 4.434 . . . . . . A 10 A H5' . 26024 1 103 . 1 1 10 10 A H5'' H 1 4.130 . . . . . . A 10 A H5'' . 26024 1 104 . 1 1 10 10 A H8 H 1 7.602 . . . . . . A 10 A H8 . 26024 1 105 . 1 1 10 10 A C1' C 13 92.638 . . . . . . A 10 A C1' . 26024 1 106 . 1 1 10 10 A C2 C 13 153.357 . . . . . . A 10 A C2 . 26024 1 107 . 1 1 10 10 A C2' C 13 75.625 . . . . . . A 10 A C2' . 26024 1 108 . 1 1 10 10 A C4' C 13 82.444 . . . . . . A 10 A C4' . 26024 1 109 . 1 1 10 10 A C5' C 13 66.113 . . . . . . A 10 A C5' . 26024 1 110 . 1 1 10 10 A C8 C 13 139.460 . . . . . . A 10 A C8 . 26024 1 111 . 1 1 10 10 A N9 N 15 170.048 . . . . . . A 10 A N9 . 26024 1 112 . 1 1 11 11 A H1' H 1 5.923 . . . . . . A 11 A H1' . 26024 1 113 . 1 1 11 11 A H2 H 1 7.840 . . . . . . A 11 A H2 . 26024 1 114 . 1 1 11 11 A H2' H 1 4.284 . . . . . . A 11 A H2' . 26024 1 115 . 1 1 11 11 A H3' H 1 4.253 . . . . . . A 11 A H3' . 26024 1 116 . 1 1 11 11 A H4' H 1 4.211 . . . . . . A 11 A H4' . 26024 1 117 . 1 1 11 11 A H5' H 1 4.415 . . . . . . A 11 A H5' . 26024 1 118 . 1 1 11 11 A H5'' H 1 4.027 . . . . . . A 11 A H5'' . 26024 1 119 . 1 1 11 11 A H8 H 1 7.983 . . . . . . A 11 A H8 . 26024 1 120 . 1 1 11 11 A C1' C 13 91.916 . . . . . . A 11 A C1' . 26024 1 121 . 1 1 11 11 A C2 C 13 153.855 . . . . . . A 11 A C2 . 26024 1 122 . 1 1 11 11 A C3' C 13 70.345 . . . . . . A 11 A C3' . 26024 1 123 . 1 1 11 11 A C4' C 13 83.959 . . . . . . A 11 A C4' . 26024 1 124 . 1 1 11 11 A C5' C 13 65.518 . . . . . . A 11 A C5' . 26024 1 125 . 1 1 11 11 A C8 C 13 140.341 . . . . . . A 11 A C8 . 26024 1 126 . 1 1 11 11 A N9 N 15 171.280 . . . . . . A 11 A N9 . 26024 1 127 . 1 1 12 12 G H1' H 1 5.733 . . . . . . A 12 G H1' . 26024 1 128 . 1 1 12 12 G H2' H 1 4.450 . . . . . . A 12 G H2' . 26024 1 129 . 1 1 12 12 G H3' H 1 4.492 . . . . . . A 12 G H3' . 26024 1 130 . 1 1 12 12 G H8 H 1 7.863 . . . . . . A 12 G H8 . 26024 1 131 . 1 1 13 13 G H1' H 1 5.825 . . . . . . A 13 G H1' . 26024 1 132 . 1 1 13 13 G H2' H 1 4.538 . . . . . . A 13 G H2' . 26024 1 133 . 1 1 13 13 G H3' H 1 4.508 . . . . . . A 13 G H3' . 26024 1 134 . 1 1 13 13 G H4' H 1 4.622 . . . . . . A 13 G H4' . 26024 1 135 . 1 1 13 13 G H5' H 1 4.070 . . . . . . A 13 G H5' . 26024 1 136 . 1 1 13 13 G H5'' H 1 4.104 . . . . . . A 13 G H5'' . 26024 1 137 . 1 1 13 13 G H8 H 1 7.270 . . . . . . A 13 G H8 . 26024 1 138 . 1 1 14 14 C H1' H 1 5.544 . . . . . . A 14 C H1' . 26024 1 139 . 1 1 14 14 C H2' H 1 4.537 . . . . . . A 14 C H2' . 26024 1 140 . 1 1 14 14 C H3' H 1 4.246 . . . . . . A 14 C H3' . 26024 1 141 . 1 1 14 14 C H4' H 1 4.402 . . . . . . A 14 C H4' . 26024 1 142 . 1 1 14 14 C H5 H 1 5.204 . . . . . . A 14 C H5 . 26024 1 143 . 1 1 14 14 C H5' H 1 4.052 . . . . . . A 14 C H5' . 26024 1 144 . 1 1 14 14 C H5'' H 1 4.506 . . . . . . A 14 C H5'' . 26024 1 145 . 1 1 14 14 C H6 H 1 7.473 . . . . . . A 14 C H6 . 26024 1 146 . 1 1 15 15 U H1' H 1 5.678 . . . . . . A 15 U H1' . 26024 1 147 . 1 1 15 15 U H2' H 1 3.813 . . . . . . A 15 U H2' . 26024 1 148 . 1 1 15 15 U H3' H 1 4.526 . . . . . . A 15 U H3' . 26024 1 149 . 1 1 15 15 U H4' H 1 4.386 . . . . . . A 15 U H4' . 26024 1 150 . 1 1 15 15 U H5 H 1 5.724 . . . . . . A 15 U H5 . 26024 1 151 . 1 1 15 15 U H5' H 1 4.323 . . . . . . A 15 U H5' . 26024 1 152 . 1 1 15 15 U H5'' H 1 4.163 . . . . . . A 15 U H5'' . 26024 1 153 . 1 1 15 15 U H6 H 1 7.804 . . . . . . A 15 U H6 . 26024 1 154 . 1 1 15 15 U C1' C 13 94.644 . . . . . . A 15 U C1' . 26024 1 155 . 1 1 15 15 U C2' C 13 76.024 . . . . . . A 15 U C2' . 26024 1 156 . 1 1 15 15 U C3' C 13 73.234 . . . . . . A 15 U C3' . 26024 1 157 . 1 1 15 15 U C4' C 13 82.464 . . . . . . A 15 U C4' . 26024 1 158 . 1 1 15 15 U C5 C 13 105.007 . . . . . . A 15 U C5 . 26024 1 159 . 1 1 15 15 U C5' C 13 64.043 . . . . . . A 15 U C5' . 26024 1 160 . 1 1 15 15 U C6 C 13 140.773 . . . . . . A 15 U C6 . 26024 1 161 . 1 1 15 15 U N1 N 15 147.169 . . . . . . A 15 U N1 . 26024 1 162 . 1 1 16 16 U H1' H 1 6.105 . . . . . . A 16 U H1' . 26024 1 163 . 1 1 16 16 U H2' H 1 4.688 . . . . . . A 16 U H2' . 26024 1 164 . 1 1 16 16 U H3' H 1 4.031 . . . . . . A 16 U H3' . 26024 1 165 . 1 1 16 16 U H4' H 1 4.483 . . . . . . A 16 U H4' . 26024 1 166 . 1 1 16 16 U H5 H 1 5.872 . . . . . . A 16 U H5 . 26024 1 167 . 1 1 16 16 U H5' H 1 4.249 . . . . . . A 16 U H5' . 26024 1 168 . 1 1 16 16 U H5'' H 1 4.106 . . . . . . A 16 U H5'' . 26024 1 169 . 1 1 16 16 U H6 H 1 8.041 . . . . . . A 16 U H6 . 26024 1 170 . 1 1 16 16 U C1' C 13 89.213 . . . . . . A 16 U C1' . 26024 1 171 . 1 1 16 16 U C2' C 13 74.630 . . . . . . A 16 U C2' . 26024 1 172 . 1 1 16 16 U C3' C 13 77.867 . . . . . . A 16 U C3' . 26024 1 173 . 1 1 16 16 U C4' C 13 83.713 . . . . . . A 16 U C4' . 26024 1 174 . 1 1 16 16 U C5 C 13 105.494 . . . . . . A 16 U C5 . 26024 1 175 . 1 1 16 16 U C5' C 13 67.870 . . . . . . A 16 U C5' . 26024 1 176 . 1 1 16 16 U C6 C 13 144.688 . . . . . . A 16 U C6 . 26024 1 177 . 1 1 16 16 U N1 N 15 143.878 . . . . . . A 16 U N1 . 26024 1 178 . 1 1 17 17 C H1' H 1 5.974 . . . . . . A 17 C H1' . 26024 1 179 . 1 1 17 17 C H2' H 1 4.127 . . . . . . A 17 C H2' . 26024 1 180 . 1 1 17 17 C H3' H 1 4.502 . . . . . . A 17 C H3' . 26024 1 181 . 1 1 17 17 C H4' H 1 3.814 . . . . . . A 17 C H4' . 26024 1 182 . 1 1 17 17 C H5 H 1 6.154 . . . . . . A 17 C H5 . 26024 1 183 . 1 1 17 17 C H5' H 1 3.627 . . . . . . A 17 C H5' . 26024 1 184 . 1 1 17 17 C H5'' H 1 2.738 . . . . . . A 17 C H5'' . 26024 1 185 . 1 1 17 17 C H6 H 1 7.716 . . . . . . A 17 C H6 . 26024 1 186 . 1 1 18 18 G H1' H 1 5.974 . . . . . . A 18 G H1' . 26024 1 187 . 1 1 18 18 G H2' H 1 4.856 . . . . . . A 18 G H2' . 26024 1 188 . 1 1 18 18 G H3' H 1 5.630 . . . . . . A 18 G H3' . 26024 1 189 . 1 1 18 18 G H4' H 1 4.414 . . . . . . A 18 G H4' . 26024 1 190 . 1 1 18 18 G H5'' H 1 4.200 . . . . . . A 18 G H5'' . 26024 1 191 . 1 1 18 18 G H8 H 1 7.868 . . . . . . A 18 G H8 . 26024 1 192 . 1 1 19 19 G H1' H 1 4.465 . . . . . . A 19 G H1' . 26024 1 193 . 1 1 19 19 G H2' H 1 4.402 . . . . . . A 19 G H2' . 26024 1 194 . 1 1 19 19 G H5' H 1 4.230 . . . . . . A 19 G H5' . 26024 1 195 . 1 1 19 19 G H8 H 1 8.302 . . . . . . A 19 G H8 . 26024 1 196 . 1 1 20 20 C H1' H 1 5.633 . . . . . . A 20 C H1' . 26024 1 197 . 1 1 20 20 C H2' H 1 4.466 . . . . . . A 20 C H2' . 26024 1 198 . 1 1 20 20 C H3' H 1 4.232 . . . . . . A 20 C H3' . 26024 1 199 . 1 1 20 20 C H5 H 1 5.202 . . . . . . A 20 C H5 . 26024 1 200 . 1 1 20 20 C H6 H 1 7.685 . . . . . . A 20 C H6 . 26024 1 201 . 1 1 21 21 C H1' H 1 5.543 . . . . . . A 21 C H1' . 26024 1 202 . 1 1 21 21 C H2' H 1 4.667 . . . . . . A 21 C H2' . 26024 1 203 . 1 1 21 21 C H3' H 1 4.399 . . . . . . A 21 C H3' . 26024 1 204 . 1 1 21 21 C H5 H 1 5.393 . . . . . . A 21 C H5 . 26024 1 205 . 1 1 21 21 C H6 H 1 7.698 . . . . . . A 21 C H6 . 26024 1 206 . 1 1 22 22 U H1' H 1 5.596 . . . . . . A 22 U H1' . 26024 1 207 . 1 1 22 22 U H2' H 1 4.654 . . . . . . A 22 U H2' . 26024 1 208 . 1 1 22 22 U H3' H 1 4.388 . . . . . . A 22 U H3' . 26024 1 209 . 1 1 22 22 U H4' H 1 4.496 . . . . . . A 22 U H4' . 26024 1 210 . 1 1 22 22 U H5 H 1 4.905 . . . . . . A 22 U H5 . 26024 1 211 . 1 1 22 22 U H5' H 1 4.487 . . . . . . A 22 U H5' . 26024 1 212 . 1 1 22 22 U H5'' H 1 4.174 . . . . . . A 22 U H5'' . 26024 1 213 . 1 1 22 22 U H6 H 1 7.522 . . . . . . A 22 U H6 . 26024 1 214 . 1 1 22 22 U C1' C 13 93.315 . . . . . . A 22 U C1' . 26024 1 215 . 1 1 22 22 U C2' C 13 75.835 . . . . . . A 22 U C2' . 26024 1 216 . 1 1 22 22 U C3' C 13 73.501 . . . . . . A 22 U C3' . 26024 1 217 . 1 1 22 22 U C4' C 13 82.529 . . . . . . A 22 U C4' . 26024 1 218 . 1 1 22 22 U C5' C 13 65.642 . . . . . . A 22 U C5' . 26024 1 219 . 1 1 22 22 U C6 C 13 141.109 . . . . . . A 22 U C6 . 26024 1 220 . 1 1 22 22 U N1 N 15 145.854 . . . . . . A 22 U N1 . 26024 1 221 . 1 1 23 23 A H1' H 1 5.608 . . . . . . A 23 A H1' . 26024 1 222 . 1 1 23 23 A H2 H 1 8.042 . . . . . . A 23 A H2 . 26024 1 223 . 1 1 23 23 A H2' H 1 3.994 . . . . . . A 23 A H2' . 26024 1 224 . 1 1 23 23 A H3' H 1 4.141 . . . . . . A 23 A H3' . 26024 1 225 . 1 1 23 23 A H4' H 1 4.216 . . . . . . A 23 A H4' . 26024 1 226 . 1 1 23 23 A H5' H 1 4.296 . . . . . . A 23 A H5' . 26024 1 227 . 1 1 23 23 A H5'' H 1 3.991 . . . . . . A 23 A H5'' . 26024 1 228 . 1 1 23 23 A H8 H 1 8.392 . . . . . . A 23 A H8 . 26024 1 229 . 1 1 23 23 A C1' C 13 92.142 . . . . . . A 23 A C1' . 26024 1 230 . 1 1 23 23 A C2 C 13 154.617 . . . . . . A 23 A C2 . 26024 1 231 . 1 1 23 23 A C2' C 13 77.348 . . . . . . A 23 A C2' . 26024 1 232 . 1 1 23 23 A C3' C 13 70.348 . . . . . . A 23 A C3' . 26024 1 233 . 1 1 23 23 A C4' C 13 84.221 . . . . . . A 23 A C4' . 26024 1 234 . 1 1 23 23 A C5' C 13 65.418 . . . . . . A 23 A C5' . 26024 1 235 . 1 1 23 23 A C8 C 13 139.414 . . . . . . A 23 A C8 . 26024 1 236 . 1 1 23 23 A N9 N 15 171.109 . . . . . . A 23 A N9 . 26024 1 237 . 1 1 24 24 C H1' H 1 5.610 . . . . . . A 24 C H1' . 26024 1 238 . 1 1 24 24 C H2' H 1 4.480 . . . . . . A 24 C H2' . 26024 1 239 . 1 1 24 24 C H3' H 1 4.287 . . . . . . A 24 C H3' . 26024 1 240 . 1 1 24 24 C H5 H 1 5.629 . . . . . . A 24 C H5 . 26024 1 241 . 1 1 24 24 C H6 H 1 7.708 . . . . . . A 24 C H6 . 26024 1 242 . 1 1 25 25 G H1' H 1 5.422 . . . . . . A 25 G H1' . 26024 1 243 . 1 1 25 25 G H2' H 1 4.437 . . . . . . A 25 G H2' . 26024 1 244 . 1 1 25 25 G H8 H 1 7.816 . . . . . . A 25 G H8 . 26024 1 245 . 1 1 26 26 U H1' H 1 5.625 . . . . . . A 26 U H1' . 26024 1 246 . 1 1 26 26 U H2' H 1 4.566 . . . . . . A 26 U H2' . 26024 1 247 . 1 1 26 26 U H3' H 1 4.364 . . . . . . A 26 U H3' . 26024 1 248 . 1 1 26 26 U H4' H 1 4.353 . . . . . . A 26 U H4' . 26024 1 249 . 1 1 26 26 U H5 H 1 5.089 . . . . . . A 26 U H5 . 26024 1 250 . 1 1 26 26 U H5' H 1 4.529 . . . . . . A 26 U H5' . 26024 1 251 . 1 1 26 26 U H5'' H 1 4.073 . . . . . . A 26 U H5'' . 26024 1 252 . 1 1 26 26 U H6 H 1 7.853 . . . . . . A 26 U H6 . 26024 1 253 . 1 1 26 26 U C1' C 13 93.624 . . . . . . A 26 U C1' . 26024 1 254 . 1 1 26 26 U C2' C 13 75.880 . . . . . . A 26 U C2' . 26024 1 255 . 1 1 26 26 U C3' C 13 73.280 . . . . . . A 26 U C3' . 26024 1 256 . 1 1 26 26 U C4' C 13 82.752 . . . . . . A 26 U C4' . 26024 1 257 . 1 1 26 26 U C5 C 13 102.494 . . . . . . A 26 U C5 . 26024 1 258 . 1 1 26 26 U C5' C 13 64.805 . . . . . . A 26 U C5' . 26024 1 259 . 1 1 26 26 U C6 C 13 142.331 . . . . . . A 26 U C6 . 26024 1 260 . 1 1 26 26 U N1 N 15 147.180 . . . . . . A 26 U N1 . 26024 1 261 . 1 1 27 27 C H1' H 1 5.610 . . . . . . A 27 C H1' . 26024 1 262 . 1 1 27 27 C H2' H 1 4.357 . . . . . . A 27 C H2' . 26024 1 263 . 1 1 27 27 C H3' H 1 4.437 . . . . . . A 27 C H3' . 26024 1 264 . 1 1 27 27 C H4' H 1 4.094 . . . . . . A 27 C H4' . 26024 1 265 . 1 1 27 27 C H5 H 1 5.511 . . . . . . A 27 C H5 . 26024 1 266 . 1 1 27 27 C H5'' H 1 3.994 . . . . . . A 27 C H5'' . 26024 1 267 . 1 1 27 27 C H6 H 1 7.667 . . . . . . A 27 C H6 . 26024 1 268 . 1 1 28 28 C H1' H 1 5.546 . . . . . . A 28 C H1' . 26024 1 269 . 1 1 28 28 C H2' H 1 4.487 . . . . . . A 28 C H2' . 26024 1 270 . 1 1 28 28 C H3' H 1 4.456 . . . . . . A 28 C H3' . 26024 1 271 . 1 1 28 28 C H5 H 1 5.543 . . . . . . A 28 C H5 . 26024 1 272 . 1 1 28 28 C H5' H 1 4.095 . . . . . . A 28 C H5' . 26024 1 273 . 1 1 28 28 C H6 H 1 7.933 . . . . . . A 28 C H6 . 26024 1 stop_ save_