########################################### # Heteronuclear T1rho relaxation values # ########################################### save_heteronuclear_T1rho_list_1 _Heteronucl_T1rho_list.Sf_category heteronucl_T1rho_relaxation _Heteronucl_T1rho_list.Sf_framecode heteronuclear_T1rho_list_1 _Heteronucl_T1rho_list.Entry_ID 26503 _Heteronucl_T1rho_list.ID 1 _Heteronucl_T1rho_list.Sample_condition_list_ID 1 _Heteronucl_T1rho_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T1rho_list.Spectrometer_frequency_1H 500 _Heteronucl_T1rho_list.Temp_calibration_method methanol _Heteronucl_T1rho_list.Temp_control_method 'no temperature control applied' _Heteronucl_T1rho_list.T1rho_coherence_type S(+,-) _Heteronucl_T1rho_list.T1rho_val_units s-1 _Heteronucl_T1rho_list.Rex_units s-1 _Heteronucl_T1rho_list.Details . _Heteronucl_T1rho_list.Text_data_format . _Heteronucl_T1rho_list.Text_data . loop_ _Heteronucl_T1rho_experiment.Experiment_ID _Heteronucl_T1rho_experiment.Experiment_name _Heteronucl_T1rho_experiment.Sample_ID _Heteronucl_T1rho_experiment.Sample_label _Heteronucl_T1rho_experiment.Sample_state _Heteronucl_T1rho_experiment.Entry_ID _Heteronucl_T1rho_experiment.Heteronucl_T1rho_list_ID 1 '13C HSQC 1' 1 $sample_1 . 26503 1 stop_ loop_ _T1rho.ID _T1rho.Assembly_atom_ID _T1rho.Entity_assembly_ID _T1rho.Entity_ID _T1rho.Comp_index_ID _T1rho.Seq_ID _T1rho.Comp_ID _T1rho.Atom_ID _T1rho.Atom_type _T1rho.Atom_isotope_number _T1rho.T1rho_val _T1rho.T1rho_val_err _T1rho.Rex_val _T1rho.Rex_val_err _T1rho.Resonance_ID _T1rho.Auth_entity_assembly_ID _T1rho.Auth_seq_ID _T1rho.Auth_comp_ID _T1rho.Auth_atom_ID _T1rho.Entry_ID _T1rho.Heteronucl_T1rho_list_ID 1 . 1 1 12 12 PHE CD2 C 13 24.99 0.212 . . . . . . . 26503 1 2 . 1 1 19 19 PHE CD2 C 13 24.65 0.190 . . . . . . . 26503 1 3 . 1 1 65 65 PHE CD2 C 13 40.92 0.505 . . . . . . . 26503 1 4 . 1 1 68 68 PHE CD2 C 13 52.60 0.748 . . . . . . . 26503 1 5 . 1 1 89 89 PHE CD2 C 13 42.53 0.319 . . . . . . . 26503 1 6 . 1 1 92 92 PHE CD2 C 13 20.43 0.079 . . . . . . . 26503 1 7 . 1 1 99 99 TYR CD2 C 13 37.19 0.279 . . . . . . . 26503 1 8 . 1 1 138 138 TYR CD2 C 13 39.13 0.235 . . . . . . . 26503 1 9 . 1 1 141 141 PHE CD2 C 13 47.75 0.340 . . . . . . . 26503 1 stop_ save_ ########################################### # Heteronuclear T1rho relaxation values # ########################################### save_heteronuclear_T1rho_list_2 _Heteronucl_T1rho_list.Sf_category heteronucl_T1rho_relaxation _Heteronucl_T1rho_list.Sf_framecode heteronuclear_T1rho_list_2 _Heteronucl_T1rho_list.Entry_ID 26503 _Heteronucl_T1rho_list.ID 2 _Heteronucl_T1rho_list.Sample_condition_list_ID 1 _Heteronucl_T1rho_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T1rho_list.Spectrometer_frequency_1H 500 _Heteronucl_T1rho_list.Temp_calibration_method methanol _Heteronucl_T1rho_list.Temp_control_method 'no temperature control applied' _Heteronucl_T1rho_list.T1rho_coherence_type S(+,-) _Heteronucl_T1rho_list.T1rho_val_units s-1 _Heteronucl_T1rho_list.Rex_units s-1 _Heteronucl_T1rho_list.Details . _Heteronucl_T1rho_list.Text_data_format . _Heteronucl_T1rho_list.Text_data . loop_ _Heteronucl_T1rho_experiment.Experiment_ID _Heteronucl_T1rho_experiment.Experiment_name _Heteronucl_T1rho_experiment.Sample_ID _Heteronucl_T1rho_experiment.Sample_label _Heteronucl_T1rho_experiment.Sample_state _Heteronucl_T1rho_experiment.Entry_ID _Heteronucl_T1rho_experiment.Heteronucl_T1rho_list_ID 2 '13C HSQC 2' 2 $sample_2 . 26503 2 stop_ loop_ _T1rho.ID _T1rho.Assembly_atom_ID _T1rho.Entity_assembly_ID _T1rho.Entity_ID _T1rho.Comp_index_ID _T1rho.Seq_ID _T1rho.Comp_ID _T1rho.Atom_ID _T1rho.Atom_type _T1rho.Atom_isotope_number _T1rho.T1rho_val _T1rho.T1rho_val_err _T1rho.Rex_val _T1rho.Rex_val_err _T1rho.Resonance_ID _T1rho.Auth_entity_assembly_ID _T1rho.Auth_seq_ID _T1rho.Auth_comp_ID _T1rho.Auth_atom_ID _T1rho.Entry_ID _T1rho.Heteronucl_T1rho_list_ID 1 . 1 1 12 12 PHE CD2 C 13 27.86 0.271 . . . . . . . 26503 2 2 . 1 1 19 19 PHE CD2 C 13 26.82 0.069 . . . . . . . 26503 2 3 . 1 1 65 65 PHE CD2 C 13 48.54 1.711 . . . . . . . 26503 2 4 . 1 1 68 68 PHE CD2 C 13 53.18 1.024 . . . . . . . 26503 2 5 . 1 1 89 89 PHE CD2 C 13 46.48 1.110 . . . . . . . 26503 2 6 . 1 1 92 92 PHE CD2 C 13 23.47 0.087 . . . . . . . 26503 2 7 . 1 1 99 99 TYR CD2 C 13 45.74 1.960 . . . . . . . 26503 2 8 . 1 1 138 138 TYR CD2 C 13 46.81 1.191 . . . . . . . 26503 2 9 . 1 1 141 141 PHE CD2 C 13 51.25 1.240 . . . . . . . 26503 2 stop_ save_ ########################################### # Heteronuclear T1rho relaxation values # ########################################### save_heteronuclear_T1rho_list_3 _Heteronucl_T1rho_list.Sf_category heteronucl_T1rho_relaxation _Heteronucl_T1rho_list.Sf_framecode heteronuclear_T1rho_list_3 _Heteronucl_T1rho_list.Entry_ID 26503 _Heteronucl_T1rho_list.ID 3 _Heteronucl_T1rho_list.Sample_condition_list_ID 1 _Heteronucl_T1rho_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T1rho_list.Spectrometer_frequency_1H 600 _Heteronucl_T1rho_list.Temp_calibration_method methanol _Heteronucl_T1rho_list.Temp_control_method 'no temperature control applied' _Heteronucl_T1rho_list.T1rho_coherence_type S(+,-) _Heteronucl_T1rho_list.T1rho_val_units s-1 _Heteronucl_T1rho_list.Rex_units s-1 _Heteronucl_T1rho_list.Details . _Heteronucl_T1rho_list.Text_data_format . _Heteronucl_T1rho_list.Text_data . loop_ _Heteronucl_T1rho_experiment.Experiment_ID _Heteronucl_T1rho_experiment.Experiment_name _Heteronucl_T1rho_experiment.Sample_ID _Heteronucl_T1rho_experiment.Sample_label _Heteronucl_T1rho_experiment.Sample_state _Heteronucl_T1rho_experiment.Entry_ID _Heteronucl_T1rho_experiment.Heteronucl_T1rho_list_ID 1 '13C HSQC 1' 1 $sample_1 . 26503 3 stop_ loop_ _T1rho.ID _T1rho.Assembly_atom_ID _T1rho.Entity_assembly_ID _T1rho.Entity_ID _T1rho.Comp_index_ID _T1rho.Seq_ID _T1rho.Comp_ID _T1rho.Atom_ID _T1rho.Atom_type _T1rho.Atom_isotope_number _T1rho.T1rho_val _T1rho.T1rho_val_err _T1rho.Rex_val _T1rho.Rex_val_err _T1rho.Resonance_ID _T1rho.Auth_entity_assembly_ID _T1rho.Auth_seq_ID _T1rho.Auth_comp_ID _T1rho.Auth_atom_ID _T1rho.Entry_ID _T1rho.Heteronucl_T1rho_list_ID 1 . 1 1 12 12 PHE CD2 C 13 28.51 0.192 . . . . . . . 26503 3 2 . 1 1 19 19 PHE CD2 C 13 27.71 0.153 . . . . . . . 26503 3 3 . 1 1 65 65 PHE CD2 C 13 45.21 0.212 . . . . . . . 26503 3 4 . 1 1 68 68 PHE CD2 C 13 57.07 1.643 . . . . . . . 26503 3 5 . 1 1 89 89 PHE CD2 C 13 49.57 0.534 . . . . . . . 26503 3 6 . 1 1 92 92 PHE CD2 C 13 22.83 0.037 . . . . . . . 26503 3 7 . 1 1 99 99 TYR CD2 C 13 43.09 0.033 . . . . . . . 26503 3 8 . 1 1 138 138 TYR CD2 C 13 44.94 0.526 . . . . . . . 26503 3 9 . 1 1 141 141 PHE CD2 C 13 54.22 0.240 . . . . . . . 26503 3 stop_ save_ ########################################### # Heteronuclear T1rho relaxation values # ########################################### save_heteronuclear_T1rho_list_4 _Heteronucl_T1rho_list.Sf_category heteronucl_T1rho_relaxation _Heteronucl_T1rho_list.Sf_framecode heteronuclear_T1rho_list_4 _Heteronucl_T1rho_list.Entry_ID 26503 _Heteronucl_T1rho_list.ID 4 _Heteronucl_T1rho_list.Sample_condition_list_ID 1 _Heteronucl_T1rho_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T1rho_list.Spectrometer_frequency_1H 600 _Heteronucl_T1rho_list.Temp_calibration_method methanol _Heteronucl_T1rho_list.Temp_control_method 'no temperature control applied' _Heteronucl_T1rho_list.T1rho_coherence_type S(+,-) _Heteronucl_T1rho_list.T1rho_val_units s-1 _Heteronucl_T1rho_list.Rex_units s-1 _Heteronucl_T1rho_list.Details . _Heteronucl_T1rho_list.Text_data_format . _Heteronucl_T1rho_list.Text_data . loop_ _Heteronucl_T1rho_experiment.Experiment_ID _Heteronucl_T1rho_experiment.Experiment_name _Heteronucl_T1rho_experiment.Sample_ID _Heteronucl_T1rho_experiment.Sample_label _Heteronucl_T1rho_experiment.Sample_state _Heteronucl_T1rho_experiment.Entry_ID _Heteronucl_T1rho_experiment.Heteronucl_T1rho_list_ID 2 '13C HSQC 2' 2 $sample_2 . 26503 4 stop_ loop_ _T1rho.ID _T1rho.Assembly_atom_ID _T1rho.Entity_assembly_ID _T1rho.Entity_ID _T1rho.Comp_index_ID _T1rho.Seq_ID _T1rho.Comp_ID _T1rho.Atom_ID _T1rho.Atom_type _T1rho.Atom_isotope_number _T1rho.T1rho_val _T1rho.T1rho_val_err _T1rho.Rex_val _T1rho.Rex_val_err _T1rho.Resonance_ID _T1rho.Auth_entity_assembly_ID _T1rho.Auth_seq_ID _T1rho.Auth_comp_ID _T1rho.Auth_atom_ID _T1rho.Entry_ID _T1rho.Heteronucl_T1rho_list_ID 1 . 1 1 12 12 PHE CD2 C 13 32.91 0.155 . . . . . . . 26503 4 2 . 1 1 19 19 PHE CD2 C 13 31.49 0.295 . . . . . . . 26503 4 3 . 1 1 65 65 PHE CD2 C 13 48.81 0.327 . . . . . . . 26503 4 4 . 1 1 68 68 PHE CD2 C 13 59.31 0.217 . . . . . . . 26503 4 5 . 1 1 89 89 PHE CD2 C 13 52.53 0.295 . . . . . . . 26503 4 6 . 1 1 92 92 PHE CD2 C 13 25.85 0.006 . . . . . . . 26503 4 7 . 1 1 99 99 TYR CD2 C 13 49.96 0.733 . . . . . . . 26503 4 8 . 1 1 138 138 TYR CD2 C 13 50.40 0.851 . . . . . . . 26503 4 9 . 1 1 141 141 PHE CD2 C 13 56.65 0.669 . . . . . . . 26503 4 stop_ save_ ########################################### # Heteronuclear T1rho relaxation values # ########################################### save_heteronuclear_T1rho_list_5 _Heteronucl_T1rho_list.Sf_category heteronucl_T1rho_relaxation _Heteronucl_T1rho_list.Sf_framecode heteronuclear_T1rho_list_5 _Heteronucl_T1rho_list.Entry_ID 26503 _Heteronucl_T1rho_list.ID 5 _Heteronucl_T1rho_list.Sample_condition_list_ID 1 _Heteronucl_T1rho_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T1rho_list.Spectrometer_frequency_1H 750 _Heteronucl_T1rho_list.Temp_calibration_method methanol _Heteronucl_T1rho_list.Temp_control_method 'no temperature control applied' _Heteronucl_T1rho_list.T1rho_coherence_type S(+,-) _Heteronucl_T1rho_list.T1rho_val_units s-1 _Heteronucl_T1rho_list.Rex_units s-1 _Heteronucl_T1rho_list.Details . _Heteronucl_T1rho_list.Text_data_format . _Heteronucl_T1rho_list.Text_data . loop_ _Heteronucl_T1rho_experiment.Experiment_ID _Heteronucl_T1rho_experiment.Experiment_name _Heteronucl_T1rho_experiment.Sample_ID _Heteronucl_T1rho_experiment.Sample_label _Heteronucl_T1rho_experiment.Sample_state _Heteronucl_T1rho_experiment.Entry_ID _Heteronucl_T1rho_experiment.Heteronucl_T1rho_list_ID 1 '13C HSQC 1' 1 $sample_1 . 26503 5 stop_ loop_ _T1rho.ID _T1rho.Assembly_atom_ID _T1rho.Entity_assembly_ID _T1rho.Entity_ID _T1rho.Comp_index_ID _T1rho.Seq_ID _T1rho.Comp_ID _T1rho.Atom_ID _T1rho.Atom_type _T1rho.Atom_isotope_number _T1rho.T1rho_val _T1rho.T1rho_val_err _T1rho.Rex_val _T1rho.Rex_val_err _T1rho.Resonance_ID _T1rho.Auth_entity_assembly_ID _T1rho.Auth_seq_ID _T1rho.Auth_comp_ID _T1rho.Auth_atom_ID _T1rho.Entry_ID _T1rho.Heteronucl_T1rho_list_ID 1 . 1 1 12 12 PHE CD2 C 13 37.67 0.007 . . . . . . . 26503 5 2 . 1 1 16 16 PHE CD2 C 13 70.17 1.683 . . . . . . . 26503 5 3 . 1 1 19 19 PHE CD2 C 13 36.64 0.188 . . . . . . . 26503 5 4 . 1 1 65 65 PHE CD2 C 13 66.03 0.230 . . . . . . . 26503 5 5 . 1 1 68 68 PHE CD2 C 13 79.56 2.540 . . . . . . . 26503 5 6 . 1 1 89 89 PHE CD2 C 13 64.29 0.503 . . . . . . . 26503 5 7 . 1 1 92 92 PHE CD2 C 13 30.14 0.125 . . . . . . . 26503 5 8 . 1 1 99 99 TYR CD2 C 13 57.70 0.454 . . . . . . . 26503 5 9 . 1 1 138 138 TYR CD2 C 13 56.18 0.128 . . . . . . . 26503 5 10 . 1 1 141 141 PHE CD2 C 13 75.17 0.155 . . . . . . . 26503 5 stop_ save_ ########################################### # Heteronuclear T1rho relaxation values # ########################################### save_heteronuclear_T1rho_list_6 _Heteronucl_T1rho_list.Sf_category heteronucl_T1rho_relaxation _Heteronucl_T1rho_list.Sf_framecode heteronuclear_T1rho_list_6 _Heteronucl_T1rho_list.Entry_ID 26503 _Heteronucl_T1rho_list.ID 6 _Heteronucl_T1rho_list.Sample_condition_list_ID 1 _Heteronucl_T1rho_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T1rho_list.Spectrometer_frequency_1H 750 _Heteronucl_T1rho_list.Temp_calibration_method methanol _Heteronucl_T1rho_list.Temp_control_method 'no temperature control applied' _Heteronucl_T1rho_list.T1rho_coherence_type S(+,-) _Heteronucl_T1rho_list.T1rho_val_units s-1 _Heteronucl_T1rho_list.Rex_units s-1 _Heteronucl_T1rho_list.Details . _Heteronucl_T1rho_list.Text_data_format . _Heteronucl_T1rho_list.Text_data . loop_ _Heteronucl_T1rho_experiment.Experiment_ID _Heteronucl_T1rho_experiment.Experiment_name _Heteronucl_T1rho_experiment.Sample_ID _Heteronucl_T1rho_experiment.Sample_label _Heteronucl_T1rho_experiment.Sample_state _Heteronucl_T1rho_experiment.Entry_ID _Heteronucl_T1rho_experiment.Heteronucl_T1rho_list_ID 2 '13C HSQC 2' 2 $sample_2 . 26503 6 stop_ loop_ _T1rho.ID _T1rho.Assembly_atom_ID _T1rho.Entity_assembly_ID _T1rho.Entity_ID _T1rho.Comp_index_ID _T1rho.Seq_ID _T1rho.Comp_ID _T1rho.Atom_ID _T1rho.Atom_type _T1rho.Atom_isotope_number _T1rho.T1rho_val _T1rho.T1rho_val_err _T1rho.Rex_val _T1rho.Rex_val_err _T1rho.Resonance_ID _T1rho.Auth_entity_assembly_ID _T1rho.Auth_seq_ID _T1rho.Auth_comp_ID _T1rho.Auth_atom_ID _T1rho.Entry_ID _T1rho.Heteronucl_T1rho_list_ID 1 . 1 1 12 12 PHE CD2 C 13 40.99 0.080 . . . . . . . 26503 6 2 . 1 1 16 16 PHE CD2 C 13 70.69 3.376 . . . . . . . 26503 6 3 . 1 1 19 19 PHE CD2 C 13 40.86 0.571 . . . . . . . 26503 6 4 . 1 1 65 65 PHE CD2 C 13 67.31 0.224 . . . . . . . 26503 6 5 . 1 1 68 68 PHE CD2 C 13 75.26 1.161 . . . . . . . 26503 6 6 . 1 1 89 89 PHE CD2 C 13 66.12 0.284 . . . . . . . 26503 6 7 . 1 1 92 92 PHE CD2 C 13 33.82 0.387 . . . . . . . 26503 6 8 . 1 1 99 99 TYR CD2 C 13 63.25 0.337 . . . . . . . 26503 6 9 . 1 1 138 138 TYR CD2 C 13 63.62 0.541 . . . . . . . 26503 6 10 . 1 1 141 141 PHE CD2 C 13 73.58 0.221 . . . . . . . 26503 6 stop_ save_