######################################## # Heteronuclear T2 relaxation values # ######################################## save_heteronuclear_T2_list_1 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronuclear_T2_list_1 _Heteronucl_T2_list.Entry_ID 26513 _Heteronucl_T2_list.ID 1 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method 'no calibration applied' _Heteronucl_T2_list.Temp_control_method 'no temperature control applied' _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type S(+,-) _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details ; T2 transverse 15N relaxation rates were determined using the following delays 35.2, 70.4, 105.6, 140.8, 176.0, 211.2, 246.4 and 281.6 ms ; _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '3D 1H, 1H-NOESY-15N TROSY' . . . 26513 1 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 2 $SPARKY . . 26513 1 6 $CARA . . 26513 1 4 $TOPSPIN . . 26513 1 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 4 4 GLY N N 15 503.6 43.3 . . . . 0 G N 26513 1 2 . 1 1 5 5 MET N N 15 231.9 10.2 . . . . 1 M N 26513 1 3 . 1 1 6 6 SER N N 15 277 17.7 . . . . 2 S N 26513 1 4 . 1 1 7 7 ASP N N 15 114.7 3.52 . . . . 3 D N 26513 1 5 . 1 1 9 9 LEU N N 15 69.3 1.09 . . . . 5 L N 26513 1 6 . 1 1 10 10 HIS N N 15 81.7 2.4 . . . . 6 H N 26513 1 7 . 1 1 11 11 VAL N N 15 74.6 2.87 . . . . 7 V N 26513 1 8 . 1 1 12 12 THR N N 15 86.4 2.31 . . . . 8 T N 26513 1 9 . 1 1 13 13 PHE N N 15 75.2 1.72 . . . . 9 F N 26513 1 10 . 1 1 14 14 VAL N N 15 81.2 1.86 . . . . 10 V N 26513 1 11 . 1 1 18 18 ASN N N 15 69.5 3.42 . . . . 14 N N 26513 1 12 . 1 1 24 24 MET N N 15 72.4 2.78 . . . . 20 M N 26513 1 13 . 1 1 25 25 ALA N N 15 69.8 3.33 . . . . 21 A N 26513 1 14 . 1 1 26 26 GLU N N 15 65.2 2.03 . . . . 22 E N 26513 1 15 . 1 1 27 27 LYS N N 15 72.9 3.39 . . . . 23 K N 26513 1 16 . 1 1 28 28 MET N N 15 70.9 1.64 . . . . 24 M N 26513 1 17 . 1 1 30 30 ALA N N 15 70.9 1.69 . . . . 26 A N 26513 1 18 . 1 1 31 31 GLN N N 15 68.9 1.96 . . . . 27 Q N 26513 1 19 . 1 1 32 32 GLN N N 15 73.4 1.64 . . . . 28 Q N 26513 1 20 . 1 1 34 34 ARG N N 15 70.5 1.28 . . . . 30 R N 26513 1 21 . 1 1 35 35 HIS N N 15 70.6 1.28 . . . . 31 H N 26513 1 22 . 1 1 36 36 ARG N N 15 79.3 1.88 . . . . 32 R N 26513 1 23 . 1 1 37 37 GLY N N 15 65 1.64 . . . . 33 G N 26513 1 24 . 1 1 38 38 LEU N N 15 71.8 1.55 . . . . 34 L N 26513 1 25 . 1 1 39 39 GLY N N 15 92 1.87 . . . . 35 G N 26513 1 26 . 1 1 40 40 ASP N N 15 81.8 1.84 . . . . 36 D N 26513 1 27 . 1 1 41 41 ALA N N 15 93.4 1.94 . . . . 37 A N 26513 1 28 . 1 1 42 42 VAL N N 15 75.6 1.39 . . . . 38 V N 26513 1 29 . 1 1 43 43 ARG N N 15 83.1 3.97 . . . . 39 R N 26513 1 30 . 1 1 44 44 VAL N N 15 70.5 2.54 . . . . 40 V N 26513 1 31 . 1 1 45 45 THR N N 15 76.5 3.19 . . . . 41 T N 26513 1 32 . 1 1 46 46 SER N N 15 66.4 1.75 . . . . 42 S N 26513 1 33 . 1 1 47 47 ALA N N 15 78.3 1.78 . . . . 43 A N 26513 1 34 . 1 1 48 48 GLY N N 15 66.8 3.02 . . . . 44 G N 26513 1 35 . 1 1 49 49 THR N N 15 70.6 2.72 . . . . 45 T N 26513 1 36 . 1 1 50 50 GLY N N 15 78.4 1.71 . . . . 46 G N 26513 1 37 . 1 1 51 51 ASN N N 15 72.9 2.64 . . . . 47 N N 26513 1 38 . 1 1 52 52 TRP N N 15 76.8 4.49 . . . . 48 W N 26513 1 39 . 1 1 53 53 HIS N N 15 66.3 2.43 . . . . 49 H N 26513 1 40 . 1 1 54 54 VAL N N 15 82 1.73 . . . . 50 V N 26513 1 41 . 1 1 55 55 GLY N N 15 73.8 1.93 . . . . 51 G N 26513 1 42 . 1 1 56 56 SER N N 15 75.3 0.98 . . . . 52 S N 26513 1 43 . 1 1 57 57 CYS N N 15 81 1.88 . . . . 53 C N 26513 1 44 . 1 1 59 59 ASP N N 15 77 1.92 . . . . 55 D N 26513 1 45 . 1 1 60 60 GLU N N 15 83.9 1.19 . . . . 56 E N 26513 1 46 . 1 1 61 61 ARG N N 15 76.3 2.42 . . . . 57 R N 26513 1 47 . 1 1 62 62 ALA N N 15 83.4 2.93 . . . . 58 A N 26513 1 48 . 1 1 63 63 ALA N N 15 79.6 1.49 . . . . 59 A N 26513 1 49 . 1 1 64 64 GLY N N 15 61 1.72 . . . . 60 G N 26513 1 50 . 1 1 65 65 VAL N N 15 64.7 1.48 . . . . 61 V N 26513 1 51 . 1 1 66 66 LEU N N 15 83.9 1.5 . . . . 62 L N 26513 1 52 . 1 1 67 67 ARG N N 15 77.5 1.3 . . . . 63 R N 26513 1 53 . 1 1 69 69 HIS N N 15 83.2 2.09 . . . . 65 H N 26513 1 54 . 1 1 70 70 GLY N N 15 56.4 1.54 . . . . 66 G N 26513 1 55 . 1 1 71 71 TYR N N 15 75.5 1.87 . . . . 67 Y N 26513 1 56 . 1 1 73 73 THR N N 15 93.1 2.2 . . . . 69 T N 26513 1 57 . 1 1 76 76 ARG N N 15 67.4 0.98 . . . . 72 R N 26513 1 58 . 1 1 77 77 ALA N N 15 75.8 1.45 . . . . 73 A N 26513 1 59 . 1 1 78 78 ALA N N 15 71.1 1 . . . . 74 A N 26513 1 60 . 1 1 79 79 GLN N N 15 56.6 3.96 . . . . 75 Q N 26513 1 61 . 1 1 80 80 VAL N N 15 63.9 1.72 . . . . 76 V N 26513 1 62 . 1 1 81 81 GLY N N 15 88.3 3.12 . . . . 77 G N 26513 1 63 . 1 1 82 82 THR N N 15 74.2 1.17 . . . . 78 T N 26513 1 64 . 1 1 83 83 GLU N N 15 70.6 1.3 . . . . 79 E N 26513 1 65 . 1 1 84 84 HIS N N 15 81.7 1.5 . . . . 80 H N 26513 1 66 . 1 1 85 85 LEU N N 15 72.6 1.5 . . . . 81 L N 26513 1 67 . 1 1 86 86 ALA N N 15 75.7 1.24 . . . . 82 A N 26513 1 68 . 1 1 87 87 ALA N N 15 70.6 1.15 . . . . 83 A N 26513 1 69 . 1 1 89 89 LEU N N 15 77 1.46 . . . . 85 L N 26513 1 70 . 1 1 90 90 LEU N N 15 66.6 3.44 . . . . 86 L N 26513 1 71 . 1 1 91 91 VAL N N 15 82.5 2.77 . . . . 87 V N 26513 1 72 . 1 1 92 92 ALA N N 15 83.3 2.51 . . . . 88 A N 26513 1 73 . 1 1 93 93 LEU N N 15 80.6 4.94 . . . . 89 L N 26513 1 74 . 1 1 95 95 ARG N N 15 68.6 3.09 . . . . 91 R N 26513 1 75 . 1 1 96 96 ASN N N 15 70.7 2.33 . . . . 92 N N 26513 1 76 . 1 1 98 98 ALA N N 15 80.8 6.18 . . . . 94 A N 26513 1 77 . 1 1 99 99 ARG N N 15 73.4 2.32 . . . . 95 R N 26513 1 78 . 1 1 100 100 LEU N N 15 74.6 1.91 . . . . 96 L N 26513 1 79 . 1 1 101 101 LEU N N 15 78.6 3.01 . . . . 97 L N 26513 1 80 . 1 1 102 102 ARG N N 15 73.2 1.04 . . . . 98 R N 26513 1 81 . 1 1 103 103 GLN N N 15 77.1 0.79 . . . . 99 Q N 26513 1 82 . 1 1 104 104 LEU N N 15 84.2 1.94 . . . . 100 L N 26513 1 83 . 1 1 105 105 GLY N N 15 90.6 2.14 . . . . 101 G N 26513 1 84 . 1 1 106 106 VAL N N 15 72.4 1.01 . . . . 102 V N 26513 1 85 . 1 1 107 107 GLU N N 15 84.4 1.76 . . . . 103 E N 26513 1 86 . 1 1 108 108 ALA N N 15 71.5 2.22 . . . . 104 A N 26513 1 87 . 1 1 109 109 ALA N N 15 72.8 2.58 . . . . 105 A N 26513 1 88 . 1 1 110 110 ARG N N 15 77.2 1.65 . . . . 106 R N 26513 1 89 . 1 1 111 111 VAL N N 15 80 1.25 . . . . 107 V N 26513 1 90 . 1 1 112 112 ARG N N 15 66.7 1.68 . . . . 108 R N 26513 1 91 . 1 1 113 113 MET N N 15 84.3 3.27 . . . . 109 M N 26513 1 92 . 1 1 114 114 LEU N N 15 70.7 1.23 . . . . 110 L N 26513 1 93 . 1 1 115 115 ARG N N 15 76.9 2.33 . . . . 111 R N 26513 1 94 . 1 1 116 116 SER N N 15 72.2 2.3 . . . . 112 S N 26513 1 95 . 1 1 117 117 PHE N N 15 65.4 2.24 . . . . 113 F N 26513 1 96 . 1 1 120 120 ARG N N 15 75.1 2.39 . . . . 116 R N 26513 1 97 . 1 1 122 122 GLY N N 15 114.6 5.92 . . . . 118 G N 26513 1 98 . 1 1 126 126 LEU N N 15 84.2 1.59 . . . . 122 L N 26513 1 99 . 1 1 127 127 ASP N N 15 82.7 1.22 . . . . 123 D N 26513 1 100 . 1 1 128 128 VAL N N 15 96.6 3.04 . . . . 124 V N 26513 1 101 . 1 1 129 129 GLU N N 15 81.8 2.46 . . . . 125 E N 26513 1 102 . 1 1 130 130 ASP N N 15 69.6 3.72 . . . . 126 D N 26513 1 103 . 1 1 132 132 TYR N N 15 79.9 3.01 . . . . 128 Y N 26513 1 104 . 1 1 133 133 TYR N N 15 71.8 1.16 . . . . 129 Y N 26513 1 105 . 1 1 134 134 GLY N N 15 75.6 2.33 . . . . 130 G N 26513 1 106 . 1 1 135 135 ASP N N 15 78.6 3.35 . . . . 131 D N 26513 1 107 . 1 1 137 137 SER N N 15 69 1.32 . . . . 133 S N 26513 1 108 . 1 1 138 138 ASP N N 15 63.7 1.9 . . . . 134 D N 26513 1 109 . 1 1 139 139 PHE N N 15 68.6 2.38 . . . . 135 F N 26513 1 110 . 1 1 140 140 GLU N N 15 71.1 1.58 . . . . 136 E N 26513 1 111 . 1 1 141 141 GLU N N 15 76.8 1.11 . . . . 137 E N 26513 1 112 . 1 1 142 142 VAL N N 15 73.6 1.25 . . . . 138 V N 26513 1 113 . 1 1 143 143 PHE N N 15 60.5 1.79 . . . . 139 F N 26513 1 114 . 1 1 144 144 ALA N N 15 68.7 1.85 . . . . 140 A N 26513 1 115 . 1 1 145 145 VAL N N 15 69.6 3.07 . . . . 141 V N 26513 1 116 . 1 1 146 146 ILE N N 15 72.9 1.38 . . . . 142 I N 26513 1 117 . 1 1 147 147 GLU N N 15 71 3.55 . . . . 143 E N 26513 1 118 . 1 1 148 148 SER N N 15 74 1.15 . . . . 144 S N 26513 1 119 . 1 1 149 149 ALA N N 15 53.5 1.74 . . . . 145 A N 26513 1 120 . 1 1 150 150 LEU N N 15 73.3 1.19 . . . . 146 L N 26513 1 121 . 1 1 152 152 GLY N N 15 71.2 3.46 . . . . 148 G N 26513 1 122 . 1 1 153 153 LEU N N 15 68.5 2.1 . . . . 149 L N 26513 1 123 . 1 1 154 154 HIS N N 15 72 1.33 . . . . 150 H N 26513 1 124 . 1 1 155 155 ASP N N 15 68.3 1.17 . . . . 151 D N 26513 1 125 . 1 1 157 157 VAL N N 15 83.8 2.44 . . . . 153 V N 26513 1 126 . 1 1 158 158 ASP N N 15 66.9 2.07 . . . . 154 D N 26513 1 127 . 1 1 159 159 GLU N N 15 68.9 1.51 . . . . 155 E N 26513 1 128 . 1 1 160 160 ARG N N 15 75.3 1.51 . . . . 156 R N 26513 1 129 . 1 1 162 162 ALA N N 15 85.7 2.82 . . . . 158 A N 26513 1 130 . 1 1 163 163 ARG N N 15 102.4 1.52 . . . . 159 R N 26513 1 131 . 1 1 164 164 ASN N N 15 172.8 3.49 . . . . 160 N N 26513 1 132 . 1 1 165 165 GLY N N 15 332.9 12.3 . . . . 161 G N 26513 1 133 . 1 1 167 167 SER N N 15 525.3 18.1 . . . . 163 S N 26513 1 stop_ save_