######################################## # Heteronuclear T2 relaxation values # ######################################## save_backbone_15N_T2_500 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode backbone_15N_T2_500 _Heteronucl_T2_list.Entry_ID 27721 _Heteronucl_T2_list.ID 1 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method Thermocouple _Heteronucl_T2_list.Temp_control_method 'single scan interleaving' _Heteronucl_T2_list.Spectrometer_frequency_1H 499260345 _Heteronucl_T2_list.T2_coherence_type S(+,-) _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 8 '15N R2' . . . 27721 1 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 3 $Analysis . . 27721 1 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ILE N N 15 7.954380 0.132580 . . . . 115 ILE N 27721 1 2 . 1 1 4 4 VAL N N 15 8.812790 0.127170 . . . . 116 VAL N 27721 1 3 . 1 1 6 6 TYR N N 15 9.414020 0.208970 . . . . 118 TYR N 27721 1 4 . 1 1 7 7 ASN N N 15 9.646380 0.423710 . . . . 119 ASN N 27721 1 5 . 1 1 8 8 LEU N N 15 9.391380 0.219240 . . . . 120 LEU N 27721 1 6 . 1 1 10 10 LEU N N 15 9.092380 0.169040 . . . . 122 LEU N 27721 1 7 . 1 1 13 13 GLY N N 15 9.961000 0.192770 . . . . 125 GLY N 27721 1 8 . 1 1 14 14 VAL N N 15 9.415280 0.195790 . . . . 126 VAL N 27721 1 9 . 1 1 15 15 VAL N N 15 10.708330 0.286590 . . . . 127 VAL N 27721 1 10 . 1 1 17 17 ARG N N 15 10.559550 0.233250 . . . . 129 ARG N 27721 1 11 . 1 1 18 18 MET N N 15 9.679890 0.231400 . . . . 130 MET N 27721 1 12 . 1 1 19 19 LEU N N 15 9.835870 0.300290 . . . . 131 LEU N 27721 1 13 . 1 1 20 20 ILE N N 15 9.803400 0.227180 . . . . 132 ILE N 27721 1 14 . 1 1 22 22 ILE N N 15 9.896680 0.122700 . . . . 134 ILE N 27721 1 15 . 1 1 23 23 LEU N N 15 9.828990 0.220110 . . . . 135 LEU N 27721 1 16 . 1 1 24 24 GLY N N 15 9.874100 0.205170 . . . . 136 GLY N 27721 1 17 . 1 1 25 25 THR N N 15 9.192810 0.122450 . . . . 137 THR N 27721 1 18 . 1 1 27 27 LYS N N 15 10.057730 0.146220 . . . . 139 LYS N 27721 1 19 . 1 1 30 30 ALA N N 15 8.840020 0.209840 . . . . 142 ALA N 27721 1 20 . 1 1 31 31 ASN N N 15 9.717730 0.342550 . . . . 143 ASN N 27721 1 21 . 1 1 33 33 ILE N N 15 10.158800 0.368720 . . . . 145 ILE N 27721 1 22 . 1 1 34 34 ALA N N 15 10.841900 0.397750 . . . . 146 ALA N 27721 1 23 . 1 1 35 35 LEU N N 15 11.554630 0.421840 . . . . 147 LEU N 27721 1 24 . 1 1 36 36 ASP N N 15 9.595330 0.228290 . . . . 148 ASP N 27721 1 25 . 1 1 38 38 GLN N N 15 9.627920 0.238490 . . . . 150 GLN N 27721 1 26 . 1 1 39 39 ARG N N 15 10.751340 0.242870 . . . . 151 ARG N 27721 1 27 . 1 1 42 42 ASP N N 15 10.203500 0.225360 . . . . 154 ASP N 27721 1 28 . 1 1 43 43 VAL N N 15 10.172860 0.239560 . . . . 155 VAL N 27721 1 29 . 1 1 45 45 PHE N N 15 10.470250 0.405430 . . . . 157 PHE N 27721 1 30 . 1 1 46 46 HIS N N 15 10.458460 0.528540 . . . . 158 HIS N 27721 1 31 . 1 1 47 47 PHE N N 15 9.952900 0.317340 . . . . 159 PHE N 27721 1 32 . 1 1 51 51 PHE N N 15 10.423300 0.149590 . . . . 163 PHE N 27721 1 33 . 1 1 55 55 ASN N N 15 9.819820 0.314050 . . . . 167 ASN N 27721 1 34 . 1 1 56 56 ARG N N 15 9.356840 0.179440 . . . . 168 ARG N 27721 1 35 . 1 1 57 57 ARG N N 15 8.995600 0.172620 . . . . 169 ARG N 27721 1 36 . 1 1 58 58 VAL N N 15 9.754520 0.243870 . . . . 170 VAL N 27721 1 37 . 1 1 59 59 ILE N N 15 12.280420 0.829670 . . . . 171 ILE N 27721 1 38 . 1 1 60 60 VAL N N 15 9.705350 0.290560 . . . . 172 VAL N 27721 1 39 . 1 1 61 61 CYS N N 15 11.242760 0.401550 . . . . 173 CYS N 27721 1 40 . 1 1 62 62 ASN N N 15 10.319000 0.152640 . . . . 174 ASN N 27721 1 41 . 1 1 63 63 THR N N 15 10.677240 0.459400 . . . . 175 THR N 27721 1 42 . 1 1 64 64 LYS N N 15 11.139600 0.230050 . . . . 176 LYS N 27721 1 43 . 1 1 65 65 LEU N N 15 10.472440 0.284570 . . . . 177 LEU N 27721 1 44 . 1 1 66 66 ASP N N 15 9.503850 0.228390 . . . . 178 ASP N 27721 1 45 . 1 1 67 67 ASN N N 15 11.065370 0.229770 . . . . 179 ASN N 27721 1 46 . 1 1 68 68 ASN N N 15 9.936620 0.158860 . . . . 180 ASN N 27721 1 47 . 1 1 69 69 TRP N N 15 10.404280 0.361970 . . . . 181 TRP N 27721 1 48 . 1 1 70 70 GLY N N 15 10.269500 0.246280 . . . . 182 GLY N 27721 1 49 . 1 1 71 71 ARG N N 15 10.020390 0.102350 . . . . 183 ARG N 27721 1 50 . 1 1 74 74 ARG N N 15 11.773720 1.089600 . . . . 186 ARG N 27721 1 51 . 1 1 75 75 GLN N N 15 9.737400 0.306760 . . . . 187 GLN N 27721 1 52 . 1 1 77 77 VAL N N 15 12.732990 0.241690 . . . . 189 VAL N 27721 1 53 . 1 1 78 78 PHE N N 15 10.929850 0.400770 . . . . 190 PHE N 27721 1 54 . 1 1 80 80 PHE N N 15 7.403880 0.170790 . . . . 192 PHE N 27721 1 55 . 1 1 82 82 SER N N 15 10.587440 0.397860 . . . . 194 SER N 27721 1 56 . 1 1 83 83 GLY N N 15 10.017460 0.373500 . . . . 195 GLY N 27721 1 57 . 1 1 84 84 LYS N N 15 9.672080 0.227410 . . . . 196 LYS N 27721 1 58 . 1 1 86 86 PHE N N 15 9.561740 0.213160 . . . . 198 PHE N 27721 1 59 . 1 1 87 87 LYS N N 15 9.854980 0.214260 . . . . 199 LYS N 27721 1 60 . 1 1 88 88 ILE N N 15 9.586540 0.176150 . . . . 200 ILE N 27721 1 61 . 1 1 90 90 VAL N N 15 10.084900 0.129790 . . . . 202 VAL N 27721 1 62 . 1 1 91 91 LEU N N 15 10.154860 0.271070 . . . . 203 LEU N 27721 1 63 . 1 1 92 92 VAL N N 15 10.306820 0.324640 . . . . 204 VAL N 27721 1 64 . 1 1 95 95 ASP N N 15 11.106200 0.563440 . . . . 207 ASP N 27721 1 65 . 1 1 96 96 HIS N N 15 11.923860 0.246560 . . . . 208 HIS N 27721 1 66 . 1 1 97 97 PHE N N 15 9.826250 0.235110 . . . . 209 PHE N 27721 1 67 . 1 1 98 98 LYS N N 15 13.452650 0.483130 . . . . 210 LYS N 27721 1 68 . 1 1 100 100 ALA N N 15 9.927470 0.184290 . . . . 212 ALA N 27721 1 69 . 1 1 101 101 VAL N N 15 10.669790 0.158720 . . . . 213 VAL N 27721 1 70 . 1 1 102 102 ASN N N 15 9.787150 0.309540 . . . . 214 ASN N 27721 1 71 . 1 1 103 103 ASP N N 15 11.191280 0.259000 . . . . 215 ASP N 27721 1 72 . 1 1 104 104 ALA N N 15 9.413040 0.178580 . . . . 216 ALA N 27721 1 73 . 1 1 107 107 LEU N N 15 15.692590 0.603040 . . . . 219 LEU N 27721 1 74 . 1 1 108 108 GLN N N 15 10.577370 0.124890 . . . . 220 GLN N 27721 1 75 . 1 1 110 110 ASN N N 15 10.296330 0.286950 . . . . 222 ASN N 27721 1 76 . 1 1 111 111 HIS N N 15 9.596700 0.148350 . . . . 223 HIS N 27721 1 77 . 1 1 112 112 ARG N N 15 10.688650 0.589980 . . . . 224 ARG N 27721 1 78 . 1 1 113 113 VAL N N 15 9.678110 0.326180 . . . . 225 VAL N 27721 1 79 . 1 1 115 115 LYS N N 15 11.016400 0.417660 . . . . 227 LYS N 27721 1 80 . 1 1 116 116 LEU N N 15 9.286700 0.270080 . . . . 228 LEU N 27721 1 81 . 1 1 117 117 ASN N N 15 10.174580 0.332950 . . . . 229 ASN N 27721 1 82 . 1 1 118 118 GLU N N 15 10.084170 0.317190 . . . . 230 GLU N 27721 1 83 . 1 1 119 119 ILE N N 15 9.915160 0.221630 . . . . 231 ILE N 27721 1 84 . 1 1 120 120 SER N N 15 8.591030 0.299120 . . . . 232 SER N 27721 1 85 . 1 1 121 121 LYS N N 15 10.401080 0.243780 . . . . 233 LYS N 27721 1 86 . 1 1 122 122 LEU N N 15 9.665710 0.132670 . . . . 234 LEU N 27721 1 87 . 1 1 123 123 GLY N N 15 10.770450 0.284320 . . . . 235 GLY N 27721 1 88 . 1 1 126 126 GLY N N 15 10.448760 0.673110 . . . . 238 GLY N 27721 1 89 . 1 1 127 127 ASP N N 15 10.353830 0.412190 . . . . 239 ASP N 27721 1 90 . 1 1 128 128 ILE N N 15 9.311990 0.512420 . . . . 240 ILE N 27721 1 91 . 1 1 129 129 ASP N N 15 9.593030 0.227420 . . . . 241 ASP N 27721 1 92 . 1 1 130 130 LEU N N 15 8.839780 0.172060 . . . . 242 LEU N 27721 1 93 . 1 1 131 131 THR N N 15 10.419000 0.187590 . . . . 243 THR N 27721 1 94 . 1 1 132 132 SER N N 15 10.039260 0.268240 . . . . 244 SER N 27721 1 95 . 1 1 133 133 ALA N N 15 9.990360 0.133840 . . . . 245 ALA N 27721 1 96 . 1 1 134 134 SER N N 15 9.530780 0.182920 . . . . 246 SER N 27721 1 97 . 1 1 135 135 TYR N N 15 9.611380 0.099380 . . . . 247 TYR N 27721 1 98 . 1 1 136 136 THR N N 15 9.968750 0.108610 . . . . 248 THR N 27721 1 99 . 1 1 137 137 MET N N 15 9.412520 0.091340 . . . . 249 MET N 27721 1 100 . 1 1 138 138 ILE N N 15 9.306290 0.087740 . . . . 250 ILE N 27721 1 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_backbone_15N_T2_600 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode backbone_15N_T2_600 _Heteronucl_T2_list.Entry_ID 27721 _Heteronucl_T2_list.ID 2 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method Thermocouple _Heteronucl_T2_list.Temp_control_method 'single scan interleaving' _Heteronucl_T2_list.Spectrometer_frequency_1H 599882216 _Heteronucl_T2_list.T2_coherence_type S(+,-) _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 8 '15N R2' . . . 27721 2 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 3 $Analysis . . 27721 2 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ILE N N 15 8.535890 0.060210 . . . . 115 ILE N 27721 2 2 . 1 1 4 4 VAL N N 15 9.440460 0.099950 . . . . 116 VAL N 27721 2 3 . 1 1 6 6 TYR N N 15 10.060040 0.327300 . . . . 118 TYR N 27721 2 4 . 1 1 7 7 ASN N N 15 10.507180 0.162340 . . . . 119 ASN N 27721 2 5 . 1 1 8 8 LEU N N 15 10.182890 0.195140 . . . . 120 LEU N 27721 2 6 . 1 1 10 10 LEU N N 15 9.749350 0.117420 . . . . 122 LEU N 27721 2 7 . 1 1 13 13 GLY N N 15 10.451730 0.110340 . . . . 125 GLY N 27721 2 8 . 1 1 14 14 VAL N N 15 9.953380 0.165380 . . . . 126 VAL N 27721 2 9 . 1 1 15 15 VAL N N 15 11.116510 0.129250 . . . . 127 VAL N 27721 2 10 . 1 1 17 17 ARG N N 15 10.552120 0.158970 . . . . 129 ARG N 27721 2 11 . 1 1 18 18 MET N N 15 10.554000 0.056360 . . . . 130 MET N 27721 2 12 . 1 1 19 19 LEU N N 15 11.001740 0.157860 . . . . 131 LEU N 27721 2 13 . 1 1 20 20 ILE N N 15 10.249190 0.208380 . . . . 132 ILE N 27721 2 14 . 1 1 22 22 ILE N N 15 10.387160 0.116000 . . . . 134 ILE N 27721 2 15 . 1 1 23 23 LEU N N 15 10.803710 0.143590 . . . . 135 LEU N 27721 2 16 . 1 1 24 24 GLY N N 15 9.888180 0.281710 . . . . 136 GLY N 27721 2 17 . 1 1 25 25 THR N N 15 10.238450 0.163590 . . . . 137 THR N 27721 2 18 . 1 1 27 27 LYS N N 15 10.976390 0.328740 . . . . 139 LYS N 27721 2 19 . 1 1 30 30 ALA N N 15 9.354050 0.110130 . . . . 142 ALA N 27721 2 20 . 1 1 31 31 ASN N N 15 10.536560 0.194520 . . . . 143 ASN N 27721 2 21 . 1 1 33 33 ILE N N 15 9.972150 0.196890 . . . . 145 ILE N 27721 2 22 . 1 1 34 34 ALA N N 15 10.525570 0.210940 . . . . 146 ALA N 27721 2 23 . 1 1 35 35 LEU N N 15 12.408990 0.289990 . . . . 147 LEU N 27721 2 24 . 1 1 36 36 ASP N N 15 10.157590 0.197320 . . . . 148 ASP N 27721 2 25 . 1 1 38 38 GLN N N 15 10.282300 0.194230 . . . . 150 GLN N 27721 2 26 . 1 1 39 39 ARG N N 15 10.698930 0.145040 . . . . 151 ARG N 27721 2 27 . 1 1 42 42 ASP N N 15 11.365060 0.148430 . . . . 154 ASP N 27721 2 28 . 1 1 43 43 VAL N N 15 11.059100 0.148440 . . . . 155 VAL N 27721 2 29 . 1 1 45 45 PHE N N 15 10.982460 0.152140 . . . . 157 PHE N 27721 2 30 . 1 1 46 46 HIS N N 15 11.255150 0.414590 . . . . 158 HIS N 27721 2 31 . 1 1 47 47 PHE N N 15 10.381820 0.235650 . . . . 159 PHE N 27721 2 32 . 1 1 51 51 PHE N N 15 10.715610 0.317120 . . . . 163 PHE N 27721 2 33 . 1 1 55 55 ASN N N 15 9.963960 0.197840 . . . . 167 ASN N 27721 2 34 . 1 1 56 56 ARG N N 15 9.617280 0.126130 . . . . 168 ARG N 27721 2 35 . 1 1 57 57 ARG N N 15 9.153910 0.107850 . . . . 169 ARG N 27721 2 36 . 1 1 58 58 VAL N N 15 10.240570 0.111500 . . . . 170 VAL N 27721 2 37 . 1 1 59 59 ILE N N 15 11.858650 0.720330 . . . . 171 ILE N 27721 2 38 . 1 1 60 60 VAL N N 15 10.595460 0.279600 . . . . 172 VAL N 27721 2 39 . 1 1 61 61 CYS N N 15 11.702000 0.128100 . . . . 173 CYS N 27721 2 40 . 1 1 62 62 ASN N N 15 10.728040 0.251600 . . . . 174 ASN N 27721 2 41 . 1 1 63 63 THR N N 15 10.929210 0.178680 . . . . 175 THR N 27721 2 42 . 1 1 64 64 LYS N N 15 10.643570 0.334930 . . . . 176 LYS N 27721 2 43 . 1 1 65 65 LEU N N 15 10.695330 0.155100 . . . . 177 LEU N 27721 2 44 . 1 1 66 66 ASP N N 15 10.526540 0.235670 . . . . 178 ASP N 27721 2 45 . 1 1 67 67 ASN N N 15 11.230910 0.132900 . . . . 179 ASN N 27721 2 46 . 1 1 68 68 ASN N N 15 10.147790 0.123060 . . . . 180 ASN N 27721 2 47 . 1 1 69 69 TRP N N 15 11.009260 0.186430 . . . . 181 TRP N 27721 2 48 . 1 1 70 70 GLY N N 15 10.287070 0.219340 . . . . 182 GLY N 27721 2 49 . 1 1 71 71 ARG N N 15 10.799450 0.172930 . . . . 183 ARG N 27721 2 50 . 1 1 74 74 ARG N N 15 13.065600 0.486130 . . . . 186 ARG N 27721 2 51 . 1 1 75 75 GLN N N 15 10.546680 0.259660 . . . . 187 GLN N 27721 2 52 . 1 1 77 77 VAL N N 15 13.957200 0.112690 . . . . 189 VAL N 27721 2 53 . 1 1 78 78 PHE N N 15 11.432170 0.315850 . . . . 190 PHE N 27721 2 54 . 1 1 80 80 PHE N N 15 8.050090 0.145540 . . . . 192 PHE N 27721 2 55 . 1 1 82 82 SER N N 15 10.502190 0.228550 . . . . 194 SER N 27721 2 56 . 1 1 83 83 GLY N N 15 9.958420 0.206270 . . . . 195 GLY N 27721 2 57 . 1 1 84 84 LYS N N 15 10.220700 0.166100 . . . . 196 LYS N 27721 2 58 . 1 1 86 86 PHE N N 15 9.875130 0.104000 . . . . 198 PHE N 27721 2 59 . 1 1 87 87 LYS N N 15 10.677900 0.114750 . . . . 199 LYS N 27721 2 60 . 1 1 88 88 ILE N N 15 10.194740 0.136230 . . . . 200 ILE N 27721 2 61 . 1 1 90 90 VAL N N 15 10.590170 0.216080 . . . . 202 VAL N 27721 2 62 . 1 1 91 91 LEU N N 15 10.934880 0.263470 . . . . 203 LEU N 27721 2 63 . 1 1 92 92 VAL N N 15 11.199940 0.149590 . . . . 204 VAL N 27721 2 64 . 1 1 95 95 ASP N N 15 12.526020 0.558450 . . . . 207 ASP N 27721 2 65 . 1 1 96 96 HIS N N 15 12.546750 0.220560 . . . . 208 HIS N 27721 2 66 . 1 1 97 97 PHE N N 15 10.664210 0.170990 . . . . 209 PHE N 27721 2 67 . 1 1 98 98 LYS N N 15 16.049500 0.319470 . . . . 210 LYS N 27721 2 68 . 1 1 100 100 ALA N N 15 10.540510 0.170290 . . . . 212 ALA N 27721 2 69 . 1 1 101 101 VAL N N 15 11.618210 0.160050 . . . . 213 VAL N 27721 2 70 . 1 1 102 102 ASN N N 15 10.544750 0.262800 . . . . 214 ASN N 27721 2 71 . 1 1 103 103 ASP N N 15 11.547590 0.192940 . . . . 215 ASP N 27721 2 72 . 1 1 104 104 ALA N N 15 9.943100 0.118680 . . . . 216 ALA N 27721 2 73 . 1 1 107 107 LEU N N 15 16.519950 0.254450 . . . . 219 LEU N 27721 2 74 . 1 1 108 108 GLN N N 15 10.949700 0.148610 . . . . 220 GLN N 27721 2 75 . 1 1 110 110 ASN N N 15 11.094030 0.257540 . . . . 222 ASN N 27721 2 76 . 1 1 111 111 HIS N N 15 10.546160 0.218820 . . . . 223 HIS N 27721 2 77 . 1 1 112 112 ARG N N 15 11.408580 0.173400 . . . . 224 ARG N 27721 2 78 . 1 1 113 113 VAL N N 15 9.810010 0.067320 . . . . 225 VAL N 27721 2 79 . 1 1 115 115 LYS N N 15 10.452610 0.430000 . . . . 227 LYS N 27721 2 80 . 1 1 116 116 LEU N N 15 10.037490 0.117950 . . . . 228 LEU N 27721 2 81 . 1 1 117 117 ASN N N 15 11.101510 0.105850 . . . . 229 ASN N 27721 2 82 . 1 1 118 118 GLU N N 15 10.132400 0.167650 . . . . 230 GLU N 27721 2 83 . 1 1 119 119 ILE N N 15 10.779480 0.072930 . . . . 231 ILE N 27721 2 84 . 1 1 120 120 SER N N 15 9.089990 0.131110 . . . . 232 SER N 27721 2 85 . 1 1 121 121 LYS N N 15 11.278860 0.088610 . . . . 233 LYS N 27721 2 86 . 1 1 122 122 LEU N N 15 10.083810 0.136820 . . . . 234 LEU N 27721 2 87 . 1 1 123 123 GLY N N 15 10.543200 0.196070 . . . . 235 GLY N 27721 2 88 . 1 1 126 126 GLY N N 15 10.757060 0.464350 . . . . 238 GLY N 27721 2 89 . 1 1 127 127 ASP N N 15 11.066110 0.252260 . . . . 239 ASP N 27721 2 90 . 1 1 128 128 ILE N N 15 11.553830 0.204210 . . . . 240 ILE N 27721 2 91 . 1 1 129 129 ASP N N 15 10.222210 0.118190 . . . . 241 ASP N 27721 2 92 . 1 1 130 130 LEU N N 15 9.690680 0.103470 . . . . 242 LEU N 27721 2 93 . 1 1 131 131 THR N N 15 10.957810 0.256320 . . . . 243 THR N 27721 2 94 . 1 1 132 132 SER N N 15 10.092500 0.135160 . . . . 244 SER N 27721 2 95 . 1 1 133 133 ALA N N 15 10.258330 0.105030 . . . . 245 ALA N 27721 2 96 . 1 1 134 134 SER N N 15 10.329810 0.076900 . . . . 246 SER N 27721 2 97 . 1 1 135 135 TYR N N 15 10.404150 0.132210 . . . . 247 TYR N 27721 2 98 . 1 1 136 136 THR N N 15 10.636170 0.159850 . . . . 248 THR N 27721 2 99 . 1 1 137 137 MET N N 15 9.658880 0.152000 . . . . 249 MET N 27721 2 100 . 1 1 138 138 ILE N N 15 9.786110 0.079650 . . . . 250 ILE N 27721 2 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_backbone_15N_T2_900 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode backbone_15N_T2_900 _Heteronucl_T2_list.Entry_ID 27721 _Heteronucl_T2_list.ID 3 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method Thermocouple _Heteronucl_T2_list.Temp_control_method 'single scan interleaving' _Heteronucl_T2_list.Spectrometer_frequency_1H 899894229 _Heteronucl_T2_list.T2_coherence_type S(+,-) _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 8 '15N R2' . . . 27721 3 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 3 $Analysis . . 27721 3 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ILE N N 15 10.484320 0.143630 . . . . 115 ILE N 27721 3 2 . 1 1 4 4 VAL N N 15 11.475830 0.094610 . . . . 116 VAL N 27721 3 3 . 1 1 6 6 TYR N N 15 12.284580 0.166580 . . . . 118 TYR N 27721 3 4 . 1 1 7 7 ASN N N 15 10.675430 0.563910 . . . . 119 ASN N 27721 3 5 . 1 1 8 8 LEU N N 15 11.989460 0.289970 . . . . 120 LEU N 27721 3 6 . 1 1 10 10 LEU N N 15 11.083980 0.186430 . . . . 122 LEU N 27721 3 7 . 1 1 13 13 GLY N N 15 12.318820 0.646880 . . . . 125 GLY N 27721 3 8 . 1 1 14 14 VAL N N 15 12.133270 0.275710 . . . . 126 VAL N 27721 3 9 . 1 1 15 15 VAL N N 15 13.854950 0.092730 . . . . 127 VAL N 27721 3 10 . 1 1 17 17 ARG N N 15 12.143930 0.140260 . . . . 129 ARG N 27721 3 11 . 1 1 18 18 MET N N 15 13.747140 0.198080 . . . . 130 MET N 27721 3 12 . 1 1 19 19 LEU N N 15 13.473940 0.270310 . . . . 131 LEU N 27721 3 13 . 1 1 20 20 ILE N N 15 12.009980 0.180490 . . . . 132 ILE N 27721 3 14 . 1 1 22 22 ILE N N 15 12.274950 0.179140 . . . . 134 ILE N 27721 3 15 . 1 1 23 23 LEU N N 15 12.182250 0.251590 . . . . 135 LEU N 27721 3 16 . 1 1 24 24 GLY N N 15 12.652010 0.300630 . . . . 136 GLY N 27721 3 17 . 1 1 25 25 THR N N 15 11.293040 0.221850 . . . . 137 THR N 27721 3 18 . 1 1 27 27 LYS N N 15 13.589160 0.233480 . . . . 139 LYS N 27721 3 19 . 1 1 30 30 ALA N N 15 11.662370 0.451450 . . . . 142 ALA N 27721 3 20 . 1 1 31 31 ASN N N 15 11.446040 0.218530 . . . . 143 ASN N 27721 3 21 . 1 1 33 33 ILE N N 15 11.818100 0.306840 . . . . 145 ILE N 27721 3 22 . 1 1 34 34 ALA N N 15 12.892300 0.208100 . . . . 146 ALA N 27721 3 23 . 1 1 35 35 LEU N N 15 13.419630 0.424980 . . . . 147 LEU N 27721 3 24 . 1 1 36 36 ASP N N 15 11.525420 0.288140 . . . . 148 ASP N 27721 3 25 . 1 1 38 38 GLN N N 15 11.726200 0.411700 . . . . 150 GLN N 27721 3 26 . 1 1 39 39 ARG N N 15 11.673250 0.444920 . . . . 151 ARG N 27721 3 27 . 1 1 42 42 ASP N N 15 12.753100 0.663600 . . . . 154 ASP N 27721 3 28 . 1 1 43 43 VAL N N 15 12.154070 0.371710 . . . . 155 VAL N 27721 3 29 . 1 1 45 45 PHE N N 15 12.627300 0.289250 . . . . 157 PHE N 27721 3 30 . 1 1 46 46 HIS N N 15 12.346000 0.466380 . . . . 158 HIS N 27721 3 31 . 1 1 47 47 PHE N N 15 12.283300 0.442970 . . . . 159 PHE N 27721 3 32 . 1 1 51 51 PHE N N 15 12.059520 0.423110 . . . . 163 PHE N 27721 3 33 . 1 1 55 55 ASN N N 15 10.696490 0.616970 . . . . 167 ASN N 27721 3 34 . 1 1 56 56 ARG N N 15 11.113960 0.383550 . . . . 168 ARG N 27721 3 35 . 1 1 57 57 ARG N N 15 10.811140 0.335500 . . . . 169 ARG N 27721 3 36 . 1 1 58 58 VAL N N 15 12.131660 0.409560 . . . . 170 VAL N 27721 3 37 . 1 1 59 59 ILE N N 15 13.548380 0.920670 . . . . 171 ILE N 27721 3 38 . 1 1 60 60 VAL N N 15 11.898960 0.449240 . . . . 172 VAL N 27721 3 39 . 1 1 61 61 CYS N N 15 13.855180 0.444250 . . . . 173 CYS N 27721 3 40 . 1 1 62 62 ASN N N 15 12.346810 0.513270 . . . . 174 ASN N 27721 3 41 . 1 1 63 63 THR N N 15 11.013620 0.625940 . . . . 175 THR N 27721 3 42 . 1 1 64 64 LYS N N 15 12.957860 0.556950 . . . . 176 LYS N 27721 3 43 . 1 1 65 65 LEU N N 15 11.571110 0.283300 . . . . 177 LEU N 27721 3 44 . 1 1 66 66 ASP N N 15 11.410310 0.300900 . . . . 178 ASP N 27721 3 45 . 1 1 67 67 ASN N N 15 13.695250 0.483270 . . . . 179 ASN N 27721 3 46 . 1 1 68 68 ASN N N 15 11.783890 0.466600 . . . . 180 ASN N 27721 3 47 . 1 1 69 69 TRP N N 15 10.930440 0.837300 . . . . 181 TRP N 27721 3 48 . 1 1 70 70 GLY N N 15 10.948400 0.642280 . . . . 182 GLY N 27721 3 49 . 1 1 71 71 ARG N N 15 11.502340 0.354590 . . . . 183 ARG N 27721 3 50 . 1 1 74 74 ARG N N 15 12.298850 1.280730 . . . . 186 ARG N 27721 3 51 . 1 1 75 75 GLN N N 15 11.560630 0.450120 . . . . 187 GLN N 27721 3 52 . 1 1 77 77 VAL N N 15 18.539050 0.554150 . . . . 189 VAL N 27721 3 53 . 1 1 78 78 PHE N N 15 11.545200 0.718360 . . . . 190 PHE N 27721 3 54 . 1 1 80 80 PHE N N 15 9.856860 0.194470 . . . . 192 PHE N 27721 3 55 . 1 1 82 82 SER N N 15 10.978780 0.895340 . . . . 194 SER N 27721 3 56 . 1 1 83 83 GLY N N 15 11.382440 0.249290 . . . . 195 GLY N 27721 3 57 . 1 1 84 84 LYS N N 15 12.705270 0.225850 . . . . 196 LYS N 27721 3 58 . 1 1 86 86 PHE N N 15 12.117600 0.199880 . . . . 198 PHE N 27721 3 59 . 1 1 87 87 LYS N N 15 12.147410 0.226870 . . . . 199 LYS N 27721 3 60 . 1 1 88 88 ILE N N 15 11.865120 0.297180 . . . . 200 ILE N 27721 3 61 . 1 1 90 90 VAL N N 15 12.877200 0.183590 . . . . 202 VAL N 27721 3 62 . 1 1 91 91 LEU N N 15 13.142730 0.309060 . . . . 203 LEU N 27721 3 63 . 1 1 92 92 VAL N N 15 14.133010 0.244560 . . . . 204 VAL N 27721 3 64 . 1 1 95 95 ASP N N 15 20.510130 0.974070 . . . . 207 ASP N 27721 3 65 . 1 1 96 96 HIS N N 15 17.130930 0.513890 . . . . 208 HIS N 27721 3 66 . 1 1 97 97 PHE N N 15 12.181580 0.442260 . . . . 209 PHE N 27721 3 67 . 1 1 98 98 LYS N N 15 24.861050 0.380730 . . . . 210 LYS N 27721 3 68 . 1 1 100 100 ALA N N 15 13.411060 0.236800 . . . . 212 ALA N 27721 3 69 . 1 1 101 101 VAL N N 15 13.130180 0.197930 . . . . 213 VAL N 27721 3 70 . 1 1 102 102 ASN N N 15 12.405320 0.322360 . . . . 214 ASN N 27721 3 71 . 1 1 103 103 ASP N N 15 13.976740 0.395500 . . . . 215 ASP N 27721 3 72 . 1 1 104 104 ALA N N 15 11.867700 0.356250 . . . . 216 ALA N 27721 3 73 . 1 1 107 107 LEU N N 15 18.859160 0.455140 . . . . 219 LEU N 27721 3 74 . 1 1 108 108 GLN N N 15 13.836620 0.426620 . . . . 220 GLN N 27721 3 75 . 1 1 110 110 ASN N N 15 12.860080 0.606140 . . . . 222 ASN N 27721 3 76 . 1 1 111 111 HIS N N 15 12.037610 0.468910 . . . . 223 HIS N 27721 3 77 . 1 1 112 112 ARG N N 15 11.384660 0.771410 . . . . 224 ARG N 27721 3 78 . 1 1 113 113 VAL N N 15 9.835560 0.639480 . . . . 225 VAL N 27721 3 79 . 1 1 115 115 LYS N N 15 10.401360 1.092110 . . . . 227 LYS N 27721 3 80 . 1 1 116 116 LEU N N 15 11.136450 0.378540 . . . . 228 LEU N 27721 3 81 . 1 1 117 117 ASN N N 15 12.653810 0.397830 . . . . 229 ASN N 27721 3 82 . 1 1 118 118 GLU N N 15 11.641840 0.427830 . . . . 230 GLU N 27721 3 83 . 1 1 119 119 ILE N N 15 12.660340 0.325640 . . . . 231 ILE N 27721 3 84 . 1 1 120 120 SER N N 15 9.865410 0.403390 . . . . 232 SER N 27721 3 85 . 1 1 121 121 LYS N N 15 14.212580 0.313900 . . . . 233 LYS N 27721 3 86 . 1 1 122 122 LEU N N 15 11.942800 0.219540 . . . . 234 LEU N 27721 3 87 . 1 1 123 123 GLY N N 15 12.157780 0.236980 . . . . 235 GLY N 27721 3 88 . 1 1 126 126 GLY N N 15 12.397000 0.438220 . . . . 238 GLY N 27721 3 89 . 1 1 127 127 ASP N N 15 11.870460 0.284150 . . . . 239 ASP N 27721 3 90 . 1 1 128 128 ILE N N 15 12.832110 0.187020 . . . . 240 ILE N 27721 3 91 . 1 1 129 129 ASP N N 15 11.808040 0.209290 . . . . 241 ASP N 27721 3 92 . 1 1 130 130 LEU N N 15 10.360850 0.152150 . . . . 242 LEU N 27721 3 93 . 1 1 131 131 THR N N 15 13.605020 0.298480 . . . . 243 THR N 27721 3 94 . 1 1 132 132 SER N N 15 12.230160 0.163860 . . . . 244 SER N 27721 3 95 . 1 1 133 133 ALA N N 15 11.763330 0.323400 . . . . 245 ALA N 27721 3 96 . 1 1 134 134 SER N N 15 11.730610 0.242630 . . . . 246 SER N 27721 3 97 . 1 1 135 135 TYR N N 15 11.857360 0.377870 . . . . 247 TYR N 27721 3 98 . 1 1 136 136 THR N N 15 11.522620 0.264290 . . . . 248 THR N 27721 3 99 . 1 1 137 137 MET N N 15 10.506330 0.540290 . . . . 249 MET N 27721 3 100 . 1 1 138 138 ILE N N 15 11.141090 0.233090 . . . . 250 ILE N 27721 3 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_Methyl_T2_500 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode Methyl_T2_500 _Heteronucl_T2_list.Entry_ID 27721 _Heteronucl_T2_list.ID 4 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method Thermocouple _Heteronucl_T2_list.Temp_control_method 'single scan interleaving' _Heteronucl_T2_list.Spectrometer_frequency_1H 499260345 _Heteronucl_T2_list.T2_coherence_type I(+,-) _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 18 R2(D+) . . . 27721 4 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 5 $PINT . . 27721 4 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 2 2 LEU CD1 C 13 73.163 4.051 . . . . 114 LEU CD1 27721 4 2 . 1 1 2 2 LEU CD2 C 13 68.917 3.035 . . . . 114 LEU CD2 27721 4 3 . 1 1 3 3 ILE CD1 C 13 36.856 1.148 . . . . 115 ILE CD1 27721 4 4 . 1 1 3 3 ILE CG2 C 13 69.086 1.754 . . . . 115 ILE CG2 27721 4 5 . 1 1 8 8 LEU CD2 C 13 98.258 11.482 . . . . 120 LEU CD2 27721 4 6 . 1 1 10 10 LEU CD1 C 13 88.938 13.203 . . . . 122 LEU CD1 27721 4 7 . 1 1 14 14 VAL CG1 C 13 121.854 11.618 . . . . 126 VAL CG1 27721 4 8 . 1 1 14 14 VAL CG2 C 13 113.146 8.949 . . . . 126 VAL CG2 27721 4 9 . 1 1 15 15 VAL CG2 C 13 61.472 2.084 . . . . 127 VAL CG2 27721 4 10 . 1 1 18 18 MET CE C 13 55.460 1.137 . . . . 130 MET CE 27721 4 11 . 1 1 19 19 LEU CD2 C 13 72.444 4.500 . . . . 131 LEU CD2 27721 4 12 . 1 1 20 20 ILE CD1 C 13 43.730 3.757 . . . . 132 ILE CD1 27721 4 13 . 1 1 20 20 ILE CG2 C 13 115.574 26.797 . . . . 132 ILE CG2 27721 4 14 . 1 1 21 21 THR CG2 C 13 124.945 10.521 . . . . 133 THR CG2 27721 4 15 . 1 1 22 22 ILE CG2 C 13 114.738 6.552 . . . . 134 ILE CG2 27721 4 16 . 1 1 25 25 THR CG2 C 13 100.219 6.788 . . . . 137 THR CG2 27721 4 17 . 1 1 26 26 VAL CG2 C 13 124.560 12.874 . . . . 138 VAL CG2 27721 4 18 . 1 1 30 30 ALA C2 C 13 127.170 15.600 . . . . 142 ALA C2 27721 4 19 . 1 1 33 33 ILE CD1 C 13 119.206 48.501 . . . . 145 ILE CD1 27721 4 20 . 1 1 33 33 ILE CG2 C 13 99.555 9.410 . . . . 145 ILE CG2 27721 4 21 . 1 1 35 35 LEU CD1 C 13 58.106 3.127 . . . . 147 LEU CD1 27721 4 22 . 1 1 35 35 LEU CD2 C 13 66.971 6.409 . . . . 147 LEU CD2 27721 4 23 . 1 1 43 43 VAL CG1 C 13 107.008 11.349 . . . . 155 VAL CG1 27721 4 24 . 1 1 43 43 VAL CG2 C 13 180.800 35.023 . . . . 155 VAL CG2 27721 4 25 . 1 1 44 44 ALA C2 C 13 151.916 23.047 . . . . 156 ALA C2 27721 4 26 . 1 1 58 58 VAL CG1 C 13 86.135 6.169 . . . . 170 VAL CG1 27721 4 27 . 1 1 59 59 ILE CG2 C 13 101.246 5.521 . . . . 171 ILE CG2 27721 4 28 . 1 1 60 60 VAL CG2 C 13 106.350 27.440 . . . . 172 VAL CG2 27721 4 29 . 1 1 63 63 THR CG2 C 13 122.007 9.945 . . . . 175 THR CG2 27721 4 30 . 1 1 77 77 VAL CG2 C 13 88.121 4.096 . . . . 189 VAL CG2 27721 4 31 . 1 1 88 88 ILE CG2 C 13 117.523 6.576 . . . . 200 ILE CG2 27721 4 32 . 1 1 91 91 LEU CD1 C 13 85.218 5.881 . . . . 203 LEU CD1 27721 4 33 . 1 1 92 92 VAL CG1 C 13 129.120 10.788 . . . . 204 VAL CG1 27721 4 34 . 1 1 92 92 VAL CG2 C 13 117.478 9.466 . . . . 204 VAL CG2 27721 4 35 . 1 1 99 99 VAL CG1 C 13 112.798 9.074 . . . . 211 VAL CG1 27721 4 36 . 1 1 100 100 ALA C2 C 13 138.785 7.835 . . . . 212 ALA C2 27721 4 37 . 1 1 101 101 VAL CG1 C 13 141.822 10.869 . . . . 213 VAL CG1 27721 4 38 . 1 1 104 104 ALA C2 C 13 124.792 5.267 . . . . 216 ALA C2 27721 4 39 . 1 1 106 106 LEU CD1 C 13 143.279 23.550 . . . . 218 LEU CD1 27721 4 40 . 1 1 106 106 LEU CD2 C 13 197.981 37.701 . . . . 218 LEU CD2 27721 4 41 . 1 1 107 107 LEU CD1 C 13 161.932 54.442 . . . . 219 LEU CD1 27721 4 42 . 1 1 116 116 LEU CD1 C 13 98.905 11.582 . . . . 228 LEU CD1 27721 4 43 . 1 1 116 116 LEU CD2 C 13 107.641 9.604 . . . . 228 LEU CD2 27721 4 44 . 1 1 119 119 ILE CD1 C 13 76.947 4.307 . . . . 231 ILE CD1 27721 4 45 . 1 1 119 119 ILE CG2 C 13 128.268 13.204 . . . . 231 ILE CG2 27721 4 46 . 1 1 122 122 LEU CD1 C 13 170.699 48.821 . . . . 234 LEU CD1 27721 4 47 . 1 1 122 122 LEU CD2 C 13 83.917 23.557 . . . . 234 LEU CD2 27721 4 48 . 1 1 124 124 ILE CD1 C 13 77.293 5.478 . . . . 236 ILE CD1 27721 4 49 . 1 1 124 124 ILE CG2 C 13 134.035 13.507 . . . . 236 ILE CG2 27721 4 50 . 1 1 136 136 THR CG2 C 13 85.788 4.031 . . . . 248 THR CG2 27721 4 51 . 1 1 137 137 MET CE C 13 60.610 0.810 . . . . 249 MET CE 27721 4 52 . 1 1 138 138 ILE CD1 C 13 55.837 1.890 . . . . 250 ILE CD1 27721 4 53 . 1 1 138 138 ILE CG2 C 13 85.193 2.673 . . . . 250 ILE CG2 27721 4 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_Methyl_T2_600 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode Methyl_T2_600 _Heteronucl_T2_list.Entry_ID 27721 _Heteronucl_T2_list.ID 5 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method Thermocouple _Heteronucl_T2_list.Temp_control_method 'single scan interleaving' _Heteronucl_T2_list.Spectrometer_frequency_1H 599882216 _Heteronucl_T2_list.T2_coherence_type I(+,-) _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 18 R2(D+) . . . 27721 5 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 5 $PINT . . 27721 5 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 2 2 LEU CD1 C 13 77.569 3.018 . . . . 114 LEU CD1 27721 5 2 . 1 1 2 2 LEU CD2 C 13 63.393 1.938 . . . . 114 LEU CD2 27721 5 3 . 1 1 3 3 ILE CD1 C 13 36.133 0.905 . . . . 115 ILE CD1 27721 5 4 . 1 1 3 3 ILE CG2 C 13 69.969 1.444 . . . . 115 ILE CG2 27721 5 5 . 1 1 8 8 LEU CD2 C 13 87.717 7.681 . . . . 120 LEU CD2 27721 5 6 . 1 1 10 10 LEU CD1 C 13 87.512 9.724 . . . . 122 LEU CD1 27721 5 7 . 1 1 14 14 VAL CG1 C 13 114.102 8.008 . . . . 126 VAL CG1 27721 5 8 . 1 1 14 14 VAL CG2 C 13 108.594 6.556 . . . . 126 VAL CG2 27721 5 9 . 1 1 15 15 VAL CG2 C 13 65.019 1.646 . . . . 127 VAL CG2 27721 5 10 . 1 1 18 18 MET CE C 13 57.353 0.963 . . . . 130 MET CE 27721 5 11 . 1 1 19 19 LEU CD1 C 13 101.671 17.819 . . . . 131 LEU CD1 27721 5 12 . 1 1 19 19 LEU CD2 C 13 84.338 3.342 . . . . 131 LEU CD2 27721 5 13 . 1 1 20 20 ILE CD1 C 13 45.420 3.242 . . . . 132 ILE CD1 27721 5 14 . 1 1 20 20 ILE CG2 C 13 124.089 28.358 . . . . 132 ILE CG2 27721 5 15 . 1 1 21 21 THR CG2 C 13 118.969 7.831 . . . . 133 THR CG2 27721 5 16 . 1 1 22 22 ILE CG2 C 13 107.483 5.684 . . . . 134 ILE CG2 27721 5 17 . 1 1 25 25 THR CG2 C 13 87.939 3.063 . . . . 137 THR CG2 27721 5 18 . 1 1 26 26 VAL CG1 C 13 169.572 43.024 . . . . 138 VAL CG1 27721 5 19 . 1 1 26 26 VAL CG2 C 13 139.289 13.268 . . . . 138 VAL CG2 27721 5 20 . 1 1 30 30 ALA C2 C 13 147.068 17.859 . . . . 142 ALA C2 27721 5 21 . 1 1 33 33 ILE CG2 C 13 107.041 9.807 . . . . 145 ILE CG2 27721 5 22 . 1 1 34 34 ALA C2 C 13 165.749 47.244 . . . . 146 ALA C2 27721 5 23 . 1 1 35 35 LEU CD1 C 13 58.094 2.175 . . . . 147 LEU CD1 27721 5 24 . 1 1 35 35 LEU CD2 C 13 59.836 4.712 . . . . 147 LEU CD2 27721 5 25 . 1 1 43 43 VAL CG1 C 13 109.253 9.979 . . . . 155 VAL CG1 27721 5 26 . 1 1 43 43 VAL CG2 C 13 161.074 34.243 . . . . 155 VAL CG2 27721 5 27 . 1 1 44 44 ALA C2 C 13 162.443 15.200 . . . . 156 ALA C2 27721 5 28 . 1 1 58 58 VAL CG1 C 13 81.498 5.850 . . . . 170 VAL CG1 27721 5 29 . 1 1 59 59 ILE CG2 C 13 107.917 5.052 . . . . 171 ILE CG2 27721 5 30 . 1 1 60 60 VAL CG2 C 13 137.110 36.554 . . . . 172 VAL CG2 27721 5 31 . 1 1 63 63 THR CG2 C 13 119.366 16.641 . . . . 175 THR CG2 27721 5 32 . 1 1 77 77 VAL CG2 C 13 89.729 3.209 . . . . 189 VAL CG2 27721 5 33 . 1 1 88 88 ILE CG2 C 13 106.745 5.266 . . . . 200 ILE CG2 27721 5 34 . 1 1 91 91 LEU CD1 C 13 81.343 3.611 . . . . 203 LEU CD1 27721 5 35 . 1 1 92 92 VAL CG1 C 13 122.518 7.911 . . . . 204 VAL CG1 27721 5 36 . 1 1 92 92 VAL CG2 C 13 115.443 6.251 . . . . 204 VAL CG2 27721 5 37 . 1 1 99 99 VAL CG1 C 13 107.223 7.664 . . . . 211 VAL CG1 27721 5 38 . 1 1 100 100 ALA C2 C 13 125.927 6.181 . . . . 212 ALA C2 27721 5 39 . 1 1 101 101 VAL CG1 C 13 116.799 8.874 . . . . 213 VAL CG1 27721 5 40 . 1 1 104 104 ALA C2 C 13 130.099 5.134 . . . . 216 ALA C2 27721 5 41 . 1 1 106 106 LEU CD1 C 13 135.994 18.047 . . . . 218 LEU CD1 27721 5 42 . 1 1 106 106 LEU CD2 C 13 102.663 20.499 . . . . 218 LEU CD2 27721 5 43 . 1 1 107 107 LEU CD1 C 13 127.236 26.427 . . . . 219 LEU CD1 27721 5 44 . 1 1 116 116 LEU CD1 C 13 96.483 7.443 . . . . 228 LEU CD1 27721 5 45 . 1 1 116 116 LEU CD2 C 13 102.242 6.279 . . . . 228 LEU CD2 27721 5 46 . 1 1 119 119 ILE CD1 C 13 84.579 4.857 . . . . 231 ILE CD1 27721 5 47 . 1 1 119 119 ILE CG2 C 13 128.712 11.842 . . . . 231 ILE CG2 27721 5 48 . 1 1 122 122 LEU CD1 C 13 111.237 30.715 . . . . 234 LEU CD1 27721 5 49 . 1 1 122 122 LEU CD2 C 13 134.158 28.081 . . . . 234 LEU CD2 27721 5 50 . 1 1 124 124 ILE CD1 C 13 64.575 3.566 . . . . 236 ILE CD1 27721 5 51 . 1 1 124 124 ILE CG2 C 13 149.991 16.062 . . . . 236 ILE CG2 27721 5 52 . 1 1 136 136 THR CG2 C 13 86.462 3.597 . . . . 248 THR CG2 27721 5 53 . 1 1 137 137 MET CE C 13 61.183 0.850 . . . . 249 MET CE 27721 5 54 . 1 1 138 138 ILE CD1 C 13 50.972 1.408 . . . . 250 ILE CD1 27721 5 55 . 1 1 138 138 ILE CG2 C 13 84.298 2.223 . . . . 250 ILE CG2 27721 5 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_Arg_Ne_T2_500 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode Arg_Ne_T2_500 _Heteronucl_T2_list.Entry_ID 27721 _Heteronucl_T2_list.ID 6 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method Thermocouple _Heteronucl_T2_list.Temp_control_method 'single scan interleaving' _Heteronucl_T2_list.Spectrometer_frequency_1H 499260345 _Heteronucl_T2_list.T2_coherence_type I(+,-) _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 8 '15N R2' . . . 27721 6 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 3 $Analysis . . 27721 6 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 17 17 ARG NE N 15 6.550260 0.478420 . . . . 129 ARG NE 27721 6 2 . 1 1 50 50 ARG NE N 15 13.837440 0.925240 . . . . 162 ARG NE 27721 6 3 . 1 1 56 56 ARG NE N 15 8.321850 0.379910 . . . . 168 ARG NE 27721 6 4 . 1 1 74 74 ARG NE N 15 10.392010 0.952370 . . . . 186 ARG NE 27721 6 5 . 1 1 112 112 ARG NE N 15 10.493050 0.594980 . . . . 224 ARG NE 27721 6 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_Arg_Ne_T2_600 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode Arg_Ne_T2_600 _Heteronucl_T2_list.Entry_ID 27721 _Heteronucl_T2_list.ID 7 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method Thermocouple _Heteronucl_T2_list.Temp_control_method 'single scan interleaving' _Heteronucl_T2_list.Spectrometer_frequency_1H 599882216 _Heteronucl_T2_list.T2_coherence_type I(+,-) _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 8 '15N R2' . . . 27721 7 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 3 $Analysis . . 27721 7 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 17 17 ARG NE N 15 7.253850 0.243890 . . . . 129 ARG NE 27721 7 2 . 1 1 50 50 ARG NE N 15 13.694760 0.356770 . . . . 162 ARG NE 27721 7 3 . 1 1 56 56 ARG NE N 15 8.339020 0.101380 . . . . 168 ARG NE 27721 7 4 . 1 1 74 74 ARG NE N 15 11.120810 0.172820 . . . . 186 ARG NE 27721 7 5 . 1 1 112 112 ARG NE N 15 10.986120 0.208750 . . . . 224 ARG NE 27721 7 stop_ save_