######################################## # Heteronuclear T1 relaxation values # ######################################## save_T1_relaxation_750 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode T1_relaxation_750 _Heteronucl_T1_list.Entry_ID 4267 _Heteronucl_T1_list.ID 1 _Heteronucl_T1_list.Sample_condition_list_ID 1 _Heteronucl_T1_list.Sample_condition_list_label $sample_conditions_all _Heteronucl_T1_list.Spectrometer_frequency_1H 750 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units s _Heteronucl_T1_list.Details ; N15 T1 relaxation data with decoupling of CSA/DD cross-relaxation, water flipback. Interleaved acquisition mode. 750 MHz. ; _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 ASP N N 15 1.030 0.031 . . . . . 4267 1 2 . 1 1 4 4 SER N N 15 1.064 0.032 . . . . . 4267 1 3 . 1 1 5 5 THR N N 15 0.960 0.029 . . . . . 4267 1 4 . 1 1 6 6 SER N N 15 0.910 0.027 . . . . . 4267 1 5 . 1 1 7 7 ASP N N 15 0.487 0.013 . . . . . 4267 1 6 . 1 1 8 8 LEU N N 15 1.019 0.031 . . . . . 4267 1 7 . 1 1 9 9 ILE N N 15 1.225 0.055 . . . . . 4267 1 8 . 1 1 11 11 ALA N N 15 1.431 0.063 . . . . . 4267 1 9 . 1 1 14 14 LEU N N 15 1.337 0.040 . . . . . 4267 1 10 . 1 1 15 15 SER N N 15 1.348 0.040 . . . . . 4267 1 11 . 1 1 16 16 LYS N N 15 1.395 0.043 . . . . . 4267 1 12 . 1 1 17 17 VAL N N 15 1.508 0.045 . . . . . 4267 1 13 . 1 1 19 19 LEU N N 15 1.490 0.046 . . . . . 4267 1 14 . 1 1 20 20 GLN N N 15 1.390 0.044 . . . . . 4267 1 15 . 1 1 21 21 GLN N N 15 1.455 0.044 . . . . . 4267 1 16 . 1 1 22 22 ASN N N 15 1.514 0.045 . . . . . 4267 1 17 . 1 1 23 23 PHE N N 15 1.568 0.060 . . . . . 4267 1 18 . 1 1 24 24 GLN N N 15 1.765 0.063 . . . . . 4267 1 19 . 1 1 25 25 ASP N N 15 1.577 0.047 . . . . . 4267 1 20 . 1 1 26 26 ASN N N 15 1.386 0.046 . . . . . 4267 1 21 . 1 1 27 27 GLN N N 15 1.456 0.044 . . . . . 4267 1 22 . 1 1 28 28 PHE N N 15 1.520 0.046 . . . . . 4267 1 23 . 1 1 29 29 GLN N N 15 1.528 0.046 . . . . . 4267 1 24 . 1 1 30 30 GLY N N 15 1.504 0.057 . . . . . 4267 1 25 . 1 1 31 31 LYS N N 15 1.525 0.052 . . . . . 4267 1 26 . 1 1 32 32 TRP N N 15 1.598 0.087 . . . . . 4267 1 27 . 1 1 33 33 TYR N N 15 1.552 0.075 . . . . . 4267 1 28 . 1 1 34 34 VAL N N 15 1.694 0.051 . . . . . 4267 1 29 . 1 1 35 35 VAL N N 15 1.565 0.094 . . . . . 4267 1 30 . 1 1 36 36 GLY N N 15 1.458 0.063 . . . . . 4267 1 31 . 1 1 37 37 LEU N N 15 1.433 0.043 . . . . . 4267 1 32 . 1 1 38 38 ALA N N 15 1.467 0.056 . . . . . 4267 1 33 . 1 1 39 39 GLY N N 15 1.550 0.053 . . . . . 4267 1 34 . 1 1 40 40 ASN N N 15 1.586 0.048 . . . . . 4267 1 35 . 1 1 41 41 ALA N N 15 1.431 0.043 . . . . . 4267 1 36 . 1 1 42 42 ILE N N 15 1.458 0.067 . . . . . 4267 1 37 . 1 1 43 43 LEU N N 15 1.423 0.058 . . . . . 4267 1 38 . 1 1 46 46 ASP N N 15 1.160 0.051 . . . . . 4267 1 39 . 1 1 48 48 ASP N N 15 1.248 0.075 . . . . . 4267 1 40 . 1 1 52 52 MET N N 15 1.650 0.077 . . . . . 4267 1 41 . 1 1 53 53 TYR N N 15 1.700 0.102 . . . . . 4267 1 42 . 1 1 54 54 ALA N N 15 1.500 0.090 . . . . . 4267 1 43 . 1 1 55 55 THR N N 15 1.646 0.051 . . . . . 4267 1 44 . 1 1 56 56 ILE N N 15 1.700 0.102 . . . . . 4267 1 45 . 1 1 57 57 TYR N N 15 1.640 0.050 . . . . . 4267 1 46 . 1 1 58 58 GLU N N 15 1.658 0.056 . . . . . 4267 1 47 . 1 1 60 60 LYS N N 15 1.513 0.045 . . . . . 4267 1 48 . 1 1 61 61 GLU N N 15 1.435 0.043 . . . . . 4267 1 49 . 1 1 62 62 ASP N N 15 1.504 0.045 . . . . . 4267 1 50 . 1 1 63 63 LYS N N 15 1.495 0.054 . . . . . 4267 1 51 . 1 1 64 64 SER N N 15 1.450 0.044 . . . . . 4267 1 52 . 1 1 65 65 TYR N N 15 1.473 0.044 . . . . . 4267 1 53 . 1 1 66 66 ASN N N 15 1.560 0.053 . . . . . 4267 1 54 . 1 1 67 67 VAL N N 15 1.638 0.066 . . . . . 4267 1 55 . 1 1 68 68 THR N N 15 1.655 0.099 . . . . . 4267 1 56 . 1 1 69 69 SER N N 15 1.790 0.106 . . . . . 4267 1 57 . 1 1 71 71 LEU N N 15 1.570 0.047 . . . . . 4267 1 58 . 1 1 73 73 ARG N N 15 1.515 0.065 . . . . . 4267 1 59 . 1 1 74 74 LYS N N 15 1.450 0.075 . . . . . 4267 1 60 . 1 1 75 75 LYS N N 15 1.327 0.040 . . . . . 4267 1 61 . 1 1 76 76 LYS N N 15 1.317 0.040 . . . . . 4267 1 62 . 1 1 77 77 CYS N N 15 1.408 0.042 . . . . . 4267 1 63 . 1 1 78 78 ASP N N 15 1.484 0.067 . . . . . 4267 1 64 . 1 1 79 79 TYR N N 15 1.534 0.049 . . . . . 4267 1 65 . 1 1 80 80 TRP N N 15 1.677 0.083 . . . . . 4267 1 66 . 1 1 82 82 ARG N N 15 1.713 0.077 . . . . . 4267 1 67 . 1 1 83 83 THR N N 15 1.630 0.051 . . . . . 4267 1 68 . 1 1 84 84 PHE N N 15 1.593 0.049 . . . . . 4267 1 69 . 1 1 87 87 GLY N N 15 1.500 0.076 . . . . . 4267 1 70 . 1 1 88 88 CYS N N 15 1.400 0.050 . . . . . 4267 1 71 . 1 1 89 89 GLN N N 15 1.310 0.039 . . . . . 4267 1 72 . 1 1 92 92 GLU N N 15 1.350 0.041 . . . . . 4267 1 73 . 1 1 93 93 PHE N N 15 1.418 0.043 . . . . . 4267 1 74 . 1 1 94 94 THR N N 15 1.575 0.062 . . . . . 4267 1 75 . 1 1 95 95 LEU N N 15 1.650 0.058 . . . . . 4267 1 76 . 1 1 96 96 GLY N N 15 1.393 0.067 . . . . . 4267 1 77 . 1 1 97 97 ASN N N 15 1.480 0.044 . . . . . 4267 1 78 . 1 1 98 98 ILE N N 15 1.487 0.045 . . . . . 4267 1 79 . 1 1 99 99 LYS N N 15 1.300 0.039 . . . . . 4267 1 80 . 1 1 100 100 SER N N 15 1.474 0.047 . . . . . 4267 1 81 . 1 1 101 101 TYR N N 15 1.463 0.044 . . . . . 4267 1 82 . 1 1 104 104 LEU N N 15 1.490 0.045 . . . . . 4267 1 83 . 1 1 105 105 THR N N 15 1.440 0.086 . . . . . 4267 1 84 . 1 1 106 106 SER N N 15 1.515 0.053 . . . . . 4267 1 85 . 1 1 107 107 TYR N N 15 1.480 0.044 . . . . . 4267 1 86 . 1 1 108 108 LEU N N 15 1.385 0.050 . . . . . 4267 1 87 . 1 1 109 109 VAL N N 15 1.545 0.077 . . . . . 4267 1 88 . 1 1 110 110 ARG N N 15 1.487 0.060 . . . . . 4267 1 89 . 1 1 112 112 VAL N N 15 1.290 0.077 . . . . . 4267 1 90 . 1 1 113 113 SER N N 15 1.535 0.046 . . . . . 4267 1 91 . 1 1 114 114 THR N N 15 1.485 0.045 . . . . . 4267 1 92 . 1 1 115 115 ASN N N 15 1.566 0.050 . . . . . 4267 1 93 . 1 1 116 116 TYR N N 15 1.540 0.092 . . . . . 4267 1 94 . 1 1 117 117 ASN N N 15 1.547 0.049 . . . . . 4267 1 95 . 1 1 118 118 GLN N N 15 1.583 0.055 . . . . . 4267 1 96 . 1 1 119 119 HIS N N 15 1.465 0.056 . . . . . 4267 1 97 . 1 1 120 120 ALA N N 15 1.536 0.046 . . . . . 4267 1 98 . 1 1 122 122 VAL N N 15 1.540 0.092 . . . . . 4267 1 99 . 1 1 123 123 PHE N N 15 1.535 0.074 . . . . . 4267 1 100 . 1 1 124 124 PHE N N 15 1.540 0.062 . . . . . 4267 1 101 . 1 1 125 125 LYS N N 15 1.605 0.077 . . . . . 4267 1 102 . 1 1 127 127 VAL N N 15 1.617 0.090 . . . . . 4267 1 103 . 1 1 128 128 SER N N 15 1.446 0.061 . . . . . 4267 1 104 . 1 1 129 129 GLN N N 15 1.363 0.041 . . . . . 4267 1 105 . 1 1 130 130 ASN N N 15 1.405 0.042 . . . . . 4267 1 106 . 1 1 131 131 ARG N N 15 1.495 0.045 . . . . . 4267 1 107 . 1 1 132 132 GLU N N 15 1.557 0.055 . . . . . 4267 1 108 . 1 1 133 133 TYR N N 15 1.560 0.060 . . . . . 4267 1 109 . 1 1 134 134 PHE N N 15 1.478 0.044 . . . . . 4267 1 110 . 1 1 135 135 LYS N N 15 1.556 0.051 . . . . . 4267 1 111 . 1 1 136 136 ILE N N 15 1.560 0.068 . . . . . 4267 1 112 . 1 1 137 137 THR N N 15 1.490 0.076 . . . . . 4267 1 113 . 1 1 138 138 LEU N N 15 1.725 0.104 . . . . . 4267 1 114 . 1 1 139 139 TYR N N 15 1.550 0.078 . . . . . 4267 1 115 . 1 1 140 140 GLY N N 15 1.570 0.094 . . . . . 4267 1 116 . 1 1 141 141 ARG N N 15 1.525 0.086 . . . . . 4267 1 117 . 1 1 142 142 THR N N 15 1.490 0.058 . . . . . 4267 1 118 . 1 1 143 143 LYS N N 15 1.660 0.075 . . . . . 4267 1 119 . 1 1 144 144 GLU N N 15 1.640 0.049 . . . . . 4267 1 120 . 1 1 145 145 LEU N N 15 1.560 0.080 . . . . . 4267 1 121 . 1 1 146 146 THR N N 15 1.725 0.052 . . . . . 4267 1 122 . 1 1 147 147 SER N N 15 1.880 0.057 . . . . . 4267 1 123 . 1 1 148 148 GLU N N 15 1.395 0.042 . . . . . 4267 1 124 . 1 1 150 150 LYS N N 15 1.410 0.047 . . . . . 4267 1 125 . 1 1 151 151 GLU N N 15 1.478 0.044 . . . . . 4267 1 126 . 1 1 152 152 ASN N N 15 1.388 0.042 . . . . . 4267 1 127 . 1 1 153 153 PHE N N 15 1.350 0.041 . . . . . 4267 1 128 . 1 1 154 154 ILE N N 15 1.357 0.047 . . . . . 4267 1 129 . 1 1 155 155 ARG N N 15 1.470 0.044 . . . . . 4267 1 130 . 1 1 156 156 PHE N N 15 1.420 0.043 . . . . . 4267 1 131 . 1 1 157 157 SER N N 15 1.395 0.042 . . . . . 4267 1 132 . 1 1 158 158 LYS N N 15 1.430 0.055 . . . . . 4267 1 133 . 1 1 159 159 SER N N 15 1.540 0.047 . . . . . 4267 1 134 . 1 1 160 160 LEU N N 15 1.423 0.043 . . . . . 4267 1 135 . 1 1 161 161 GLY N N 15 1.470 0.044 . . . . . 4267 1 136 . 1 1 162 162 LEU N N 15 1.490 0.057 . . . . . 4267 1 137 . 1 1 165 165 ASN N N 15 1.288 0.039 . . . . . 4267 1 138 . 1 1 167 167 ILE N N 15 1.533 0.046 . . . . . 4267 1 139 . 1 1 168 168 VAL N N 15 1.496 0.046 . . . . . 4267 1 140 . 1 1 169 169 PHE N N 15 1.590 0.100 . . . . . 4267 1 141 . 1 1 171 171 VAL N N 15 1.366 0.049 . . . . . 4267 1 142 . 1 1 173 173 ILE N N 15 1.600 0.100 . . . . . 4267 1 143 . 1 1 175 175 GLN N N 15 1.747 0.099 . . . . . 4267 1 144 . 1 1 176 176 CYS N N 15 1.555 0.063 . . . . . 4267 1 145 . 1 1 178 178 ASP N N 15 1.532 0.048 . . . . . 4267 1 146 . 1 1 179 179 GLY N N 15 1.127 0.034 . . . . . 4267 1 147 . 1 1 32 32 TRP NE1 N 15 1.950 0.059 . . . . . 4267 1 148 . 1 1 80 80 TRP NE1 N 15 1.378 0.041 . . . . . 4267 1 149 . 1 1 110 110 ARG NE N 15 1.700 0.102 . . . . . 4267 1 150 . 1 1 141 141 ARG NE N 15 1.245 0.075 . . . . . 4267 1 151 . 1 1 155 155 ARG NE N 15 1.830 0.110 . . . . . 4267 1 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_T1_relaxation_600 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode T1_relaxation_600 _Heteronucl_T1_list.Entry_ID 4267 _Heteronucl_T1_list.ID 2 _Heteronucl_T1_list.Sample_condition_list_ID 1 _Heteronucl_T1_list.Sample_condition_list_label $sample_conditions_all _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units s _Heteronucl_T1_list.Details ; N15 T1 relaxation data with decoupling of CSA/DD cross-relaxation, water flipback. Interleaved acquisition mode. 600 MHz. ; _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 ASP N N 15 0.792 0.020 . . . . . 4267 2 2 . 1 1 4 4 SER N N 15 0.770 0.026 . . . . . 4267 2 3 . 1 1 5 5 THR N N 15 0.705 0.026 . . . . . 4267 2 4 . 1 1 6 6 SER N N 15 0.686 0.019 . . . . . 4267 2 5 . 1 1 7 7 ASP N N 15 0.670 0.013 . . . . . 4267 2 6 . 1 1 8 8 LEU N N 15 0.833 0.017 . . . . . 4267 2 7 . 1 1 9 9 ILE N N 15 0.990 0.047 . . . . . 4267 2 8 . 1 1 11 11 ALA N N 15 1.030 0.021 . . . . . 4267 2 9 . 1 1 14 14 LEU N N 15 1.019 0.020 . . . . . 4267 2 10 . 1 1 15 15 SER N N 15 0.942 0.033 . . . . . 4267 2 11 . 1 1 16 16 LYS N N 15 0.991 0.028 . . . . . 4267 2 12 . 1 1 17 17 VAL N N 15 1.034 0.021 . . . . . 4267 2 13 . 1 1 19 19 LEU N N 15 1.084 0.022 . . . . . 4267 2 14 . 1 1 20 20 GLN N N 15 0.996 0.033 . . . . . 4267 2 15 . 1 1 21 21 GLN N N 15 1.042 0.021 . . . . . 4267 2 16 . 1 1 22 22 ASN N N 15 0.948 0.022 . . . . . 4267 2 17 . 1 1 23 23 PHE N N 15 1.062 0.021 . . . . . 4267 2 18 . 1 1 24 24 GLN N N 15 1.106 0.055 . . . . . 4267 2 19 . 1 1 25 25 ASP N N 15 1.097 0.039 . . . . . 4267 2 20 . 1 1 26 26 ASN N N 15 0.992 0.020 . . . . . 4267 2 21 . 1 1 27 27 GLN N N 15 1.074 0.023 . . . . . 4267 2 22 . 1 1 28 28 PHE N N 15 1.049 0.033 . . . . . 4267 2 23 . 1 1 29 29 GLN N N 15 1.055 0.032 . . . . . 4267 2 24 . 1 1 30 30 GLY N N 15 1.008 0.037 . . . . . 4267 2 25 . 1 1 31 31 LYS N N 15 1.074 0.021 . . . . . 4267 2 26 . 1 1 32 32 TRP N N 15 0.992 0.035 . . . . . 4267 2 27 . 1 1 33 33 TYR N N 15 1.047 0.028 . . . . . 4267 2 28 . 1 1 34 34 VAL N N 15 1.093 0.055 . . . . . 4267 2 29 . 1 1 35 35 VAL N N 15 1.096 0.055 . . . . . 4267 2 30 . 1 1 36 36 GLY N N 15 1.091 0.034 . . . . . 4267 2 31 . 1 1 37 37 LEU N N 15 1.026 0.033 . . . . . 4267 2 32 . 1 1 38 38 ALA N N 15 1.094 0.032 . . . . . 4267 2 33 . 1 1 39 39 GLY N N 15 1.060 0.045 . . . . . 4267 2 34 . 1 1 40 40 ASN N N 15 1.020 0.046 . . . . . 4267 2 35 . 1 1 41 41 ALA N N 15 1.002 0.042 . . . . . 4267 2 36 . 1 1 42 42 ILE N N 15 1.060 0.039 . . . . . 4267 2 37 . 1 1 43 43 LEU N N 15 1.024 0.044 . . . . . 4267 2 38 . 1 1 46 46 ASP N N 15 0.890 0.045 . . . . . 4267 2 39 . 1 1 48 48 ASP N N 15 0.854 0.021 . . . . . 4267 2 40 . 1 1 52 52 MET N N 15 1.040 0.052 . . . . . 4267 2 41 . 1 1 53 53 TYR N N 15 1.040 0.052 . . . . . 4267 2 42 . 1 1 54 54 ALA N N 15 1.008 0.027 . . . . . 4267 2 43 . 1 1 55 55 THR N N 15 1.052 0.039 . . . . . 4267 2 44 . 1 1 56 56 ILE N N 15 1.030 0.052 . . . . . 4267 2 45 . 1 1 57 57 TYR N N 15 1.133 0.043 . . . . . 4267 2 46 . 1 1 58 58 GLU N N 15 1.060 0.052 . . . . . 4267 2 47 . 1 1 60 60 LYS N N 15 0.934 0.032 . . . . . 4267 2 48 . 1 1 61 61 GLU N N 15 0.965 0.019 . . . . . 4267 2 49 . 1 1 62 62 ASP N N 15 1.102 0.022 . . . . . 4267 2 50 . 1 1 63 63 LYS N N 15 0.999 0.044 . . . . . 4267 2 51 . 1 1 64 64 SER N N 15 0.999 0.044 . . . . . 4267 2 52 . 1 1 65 65 TYR N N 15 1.080 0.039 . . . . . 4267 2 53 . 1 1 66 66 ASN N N 15 1.055 0.038 . . . . . 4267 2 54 . 1 1 67 67 VAL N N 15 1.011 0.029 . . . . . 4267 2 55 . 1 1 68 68 THR N N 15 1.033 0.035 . . . . . 4267 2 56 . 1 1 69 69 SER N N 15 1.039 0.038 . . . . . 4267 2 57 . 1 1 71 71 LEU N N 15 1.030 0.039 . . . . . 4267 2 58 . 1 1 73 73 ARG N N 15 1.002 0.029 . . . . . 4267 2 59 . 1 1 74 74 LYS N N 15 0.980 0.043 . . . . . 4267 2 60 . 1 1 75 75 LYS N N 15 0.900 0.030 . . . . . 4267 2 61 . 1 1 76 76 LYS N N 15 0.983 0.020 . . . . . 4267 2 62 . 1 1 77 77 CYS N N 15 1.142 0.027 . . . . . 4267 2 63 . 1 1 78 78 ASP N N 15 1.099 0.039 . . . . . 4267 2 64 . 1 1 79 79 TYR N N 15 1.100 0.032 . . . . . 4267 2 65 . 1 1 80 80 TRP N N 15 1.100 0.055 . . . . . 4267 2 66 . 1 1 82 82 ARG N N 15 1.050 0.051 . . . . . 4267 2 67 . 1 1 83 83 THR N N 15 1.133 0.038 . . . . . 4267 2 68 . 1 1 84 84 PHE N N 15 1.105 0.037 . . . . . 4267 2 69 . 1 1 87 87 GLY N N 15 1.029 0.038 . . . . . 4267 2 70 . 1 1 88 88 CYS N N 15 1.033 0.031 . . . . . 4267 2 71 . 1 1 89 89 GLN N N 15 1.004 0.020 . . . . . 4267 2 72 . 1 1 92 92 GLU N N 15 0.994 0.020 . . . . . 4267 2 73 . 1 1 93 93 PHE N N 15 0.973 0.022 . . . . . 4267 2 74 . 1 1 94 94 THR N N 15 1.051 0.032 . . . . . 4267 2 75 . 1 1 95 95 LEU N N 15 1.020 0.036 . . . . . 4267 2 76 . 1 1 96 96 GLY N N 15 1.003 0.048 . . . . . 4267 2 77 . 1 1 97 97 ASN N N 15 0.915 0.023 . . . . . 4267 2 78 . 1 1 98 98 ILE N N 15 1.057 0.032 . . . . . 4267 2 79 . 1 1 99 99 LYS N N 15 0.993 0.020 . . . . . 4267 2 80 . 1 1 100 100 SER N N 15 1.018 0.027 . . . . . 4267 2 81 . 1 1 101 101 TYR N N 15 1.047 0.023 . . . . . 4267 2 82 . 1 1 103 103 GLY N N 15 1.016 0.051 . . . . . 4267 2 83 . 1 1 104 104 LEU N N 15 1.013 0.020 . . . . . 4267 2 84 . 1 1 105 105 THR N N 15 1.103 0.032 . . . . . 4267 2 85 . 1 1 106 106 SER N N 15 1.043 0.025 . . . . . 4267 2 86 . 1 1 107 107 TYR N N 15 1.059 0.031 . . . . . 4267 2 87 . 1 1 108 108 LEU N N 15 1.066 0.035 . . . . . 4267 2 88 . 1 1 109 109 VAL N N 15 1.059 0.021 . . . . . 4267 2 89 . 1 1 110 110 ARG N N 15 1.018 0.026 . . . . . 4267 2 90 . 1 1 112 112 VAL N N 15 1.001 0.035 . . . . . 4267 2 91 . 1 1 113 113 SER N N 15 1.068 0.025 . . . . . 4267 2 92 . 1 1 115 115 ASN N N 15 1.060 0.045 . . . . . 4267 2 93 . 1 1 116 116 TYR N N 15 1.000 0.050 . . . . . 4267 2 94 . 1 1 117 117 ASN N N 15 1.106 0.035 . . . . . 4267 2 95 . 1 1 118 118 GLN N N 15 0.955 0.028 . . . . . 4267 2 96 . 1 1 119 119 HIS N N 15 1.056 0.043 . . . . . 4267 2 97 . 1 1 120 120 ALA N N 15 1.047 0.033 . . . . . 4267 2 98 . 1 1 122 122 VAL N N 15 1.122 0.043 . . . . . 4267 2 99 . 1 1 123 123 PHE N N 15 1.064 0.038 . . . . . 4267 2 100 . 1 1 124 124 PHE N N 15 1.054 0.029 . . . . . 4267 2 101 . 1 1 125 125 LYS N N 15 1.047 0.030 . . . . . 4267 2 102 . 1 1 127 127 VAL N N 15 1.041 0.030 . . . . . 4267 2 103 . 1 1 128 128 SER N N 15 1.034 0.034 . . . . . 4267 2 104 . 1 1 129 129 GLN N N 15 1.000 0.034 . . . . . 4267 2 105 . 1 1 130 130 ASN N N 15 1.026 0.024 . . . . . 4267 2 106 . 1 1 131 131 ARG N N 15 1.034 0.029 . . . . . 4267 2 107 . 1 1 132 132 GLU N N 15 1.079 0.022 . . . . . 4267 2 108 . 1 1 133 133 TYR N N 15 1.087 0.041 . . . . . 4267 2 109 . 1 1 134 134 PHE N N 15 1.036 0.021 . . . . . 4267 2 110 . 1 1 135 135 LYS N N 15 1.070 0.028 . . . . . 4267 2 111 . 1 1 136 136 ILE N N 15 1.099 0.031 . . . . . 4267 2 112 . 1 1 137 137 THR N N 15 1.043 0.049 . . . . . 4267 2 113 . 1 1 138 138 LEU N N 15 1.071 0.047 . . . . . 4267 2 114 . 1 1 139 139 TYR N N 15 1.024 0.045 . . . . . 4267 2 115 . 1 1 140 140 GLY N N 15 1.090 0.036 . . . . . 4267 2 116 . 1 1 141 141 ARG N N 15 1.059 0.021 . . . . . 4267 2 117 . 1 1 142 142 THR N N 15 1.040 0.030 . . . . . 4267 2 118 . 1 1 143 143 LYS N N 15 1.056 0.034 . . . . . 4267 2 119 . 1 1 144 144 GLU N N 15 1.167 0.050 . . . . . 4267 2 120 . 1 1 145 145 LEU N N 15 1.112 0.040 . . . . . 4267 2 121 . 1 1 146 146 THR N N 15 1.227 0.042 . . . . . 4267 2 122 . 1 1 147 147 SER N N 15 0.985 0.041 . . . . . 4267 2 123 . 1 1 148 148 GLU N N 15 0.949 0.024 . . . . . 4267 2 124 . 1 1 150 150 LYS N N 15 1.041 0.021 . . . . . 4267 2 125 . 1 1 151 151 GLU N N 15 1.034 0.021 . . . . . 4267 2 126 . 1 1 152 152 ASN N N 15 1.007 0.020 . . . . . 4267 2 127 . 1 1 153 153 PHE N N 15 0.986 0.025 . . . . . 4267 2 128 . 1 1 154 154 ILE N N 15 0.986 0.020 . . . . . 4267 2 129 . 1 1 155 155 ARG N N 15 1.003 0.020 . . . . . 4267 2 130 . 1 1 156 156 PHE N N 15 0.999 0.028 . . . . . 4267 2 131 . 1 1 157 157 SER N N 15 1.033 0.021 . . . . . 4267 2 132 . 1 1 158 158 LYS N N 15 1.000 0.020 . . . . . 4267 2 133 . 1 1 159 159 SER N N 15 1.048 0.034 . . . . . 4267 2 134 . 1 1 160 160 LEU N N 15 1.009 0.020 . . . . . 4267 2 135 . 1 1 161 161 GLY N N 15 1.029 0.022 . . . . . 4267 2 136 . 1 1 162 162 LEU N N 15 1.069 0.021 . . . . . 4267 2 137 . 1 1 165 165 ASN N N 15 0.969 0.019 . . . . . 4267 2 138 . 1 1 167 167 ILE N N 15 1.060 0.029 . . . . . 4267 2 139 . 1 1 168 168 VAL N N 15 1.040 0.025 . . . . . 4267 2 140 . 1 1 169 169 PHE N N 15 1.088 0.040 . . . . . 4267 2 141 . 1 1 171 171 VAL N N 15 1.031 0.030 . . . . . 4267 2 142 . 1 1 173 173 ILE N N 15 1.142 0.057 . . . . . 4267 2 143 . 1 1 175 175 GLN N N 15 1.152 0.030 . . . . . 4267 2 144 . 1 1 176 176 CYS N N 15 1.022 0.051 . . . . . 4267 2 145 . 1 1 178 178 ASP N N 15 1.025 0.032 . . . . . 4267 2 146 . 1 1 179 179 GLY N N 15 0.984 0.021 . . . . . 4267 2 147 . 1 1 32 32 TRP NE1 N 15 1.223 0.048 . . . . . 4267 2 148 . 1 1 80 80 TRP NE1 N 15 0.918 0.037 . . . . . 4267 2 149 . 1 1 110 110 ARG NE N 15 1.470 0.074 . . . . . 4267 2 150 . 1 1 141 141 ARG NE N 15 1.129 0.056 . . . . . 4267 2 151 . 1 1 155 155 ARG NE N 15 1.745 0.087 . . . . . 4267 2 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_T1_relaxation_500 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode T1_relaxation_500 _Heteronucl_T1_list.Entry_ID 4267 _Heteronucl_T1_list.ID 3 _Heteronucl_T1_list.Sample_condition_list_ID 1 _Heteronucl_T1_list.Sample_condition_list_label $sample_conditions_all _Heteronucl_T1_list.Spectrometer_frequency_1H 500 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units s _Heteronucl_T1_list.Details ; N15 T1 relaxation data with decoupling of CSA/DD cross-relaxation, water flipback. Interleaved acquisition mode. 500 MHz. ; _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 4 4 SER N N 15 0.940 0.362 . . . . . 4267 3 2 . 1 1 5 5 THR N N 15 0.893 0.114 . . . . . 4267 3 3 . 1 1 6 6 SER N N 15 0.837 0.099 . . . . . 4267 3 4 . 1 1 7 7 ASP N N 15 0.704 0.052 . . . . . 4267 3 5 . 1 1 8 8 LEU N N 15 0.710 0.021 . . . . . 4267 3 6 . 1 1 9 9 ILE N N 15 0.790 0.033 . . . . . 4267 3 7 . 1 1 11 11 ALA N N 15 0.799 0.024 . . . . . 4267 3 8 . 1 1 14 14 LEU N N 15 0.785 0.024 . . . . . 4267 3 9 . 1 1 15 15 SER N N 15 0.798 0.052 . . . . . 4267 3 10 . 1 1 16 16 LYS N N 15 0.792 0.034 . . . . . 4267 3 11 . 1 1 17 17 VAL N N 15 0.844 0.025 . . . . . 4267 3 12 . 1 1 19 19 LEU N N 15 0.841 0.025 . . . . . 4267 3 13 . 1 1 20 20 GLN N N 15 0.799 0.031 . . . . . 4267 3 14 . 1 1 21 21 GLN N N 15 0.799 0.024 . . . . . 4267 3 15 . 1 1 23 23 PHE N N 15 0.872 0.032 . . . . . 4267 3 16 . 1 1 24 24 GLN N N 15 0.914 0.049 . . . . . 4267 3 17 . 1 1 25 25 ASP N N 15 0.904 0.033 . . . . . 4267 3 18 . 1 1 26 26 ASN N N 15 0.846 0.042 . . . . . 4267 3 19 . 1 1 27 27 GLN N N 15 0.854 0.026 . . . . . 4267 3 20 . 1 1 28 28 PHE N N 15 0.862 0.034 . . . . . 4267 3 21 . 1 1 29 29 GLN N N 15 0.831 0.027 . . . . . 4267 3 22 . 1 1 30 30 GLY N N 15 0.786 0.033 . . . . . 4267 3 23 . 1 1 31 31 LYS N N 15 0.832 0.028 . . . . . 4267 3 24 . 1 1 32 32 TRP N N 15 0.750 0.034 . . . . . 4267 3 25 . 1 1 33 33 TYR N N 15 0.832 0.042 . . . . . 4267 3 26 . 1 1 34 34 VAL N N 15 0.867 0.040 . . . . . 4267 3 27 . 1 1 35 35 VAL N N 15 0.839 0.045 . . . . . 4267 3 28 . 1 1 36 36 GLY N N 15 0.795 0.034 . . . . . 4267 3 29 . 1 1 37 37 LEU N N 15 0.769 0.023 . . . . . 4267 3 30 . 1 1 38 38 ALA N N 15 0.771 0.033 . . . . . 4267 3 31 . 1 1 39 39 GLY N N 15 0.859 0.044 . . . . . 4267 3 32 . 1 1 40 40 ASN N N 15 0.921 0.054 . . . . . 4267 3 33 . 1 1 41 41 ALA N N 15 0.823 0.077 . . . . . 4267 3 34 . 1 1 43 43 LEU N N 15 0.732 0.047 . . . . . 4267 3 35 . 1 1 46 46 ASP N N 15 0.771 0.166 . . . . . 4267 3 36 . 1 1 48 48 ASP N N 15 0.803 0.038 . . . . . 4267 3 37 . 1 1 52 52 MET N N 15 0.818 0.066 . . . . . 4267 3 38 . 1 1 53 53 TYR N N 15 0.874 0.204 . . . . . 4267 3 39 . 1 1 54 54 ALA N N 15 0.883 0.040 . . . . . 4267 3 40 . 1 1 55 55 THR N N 15 0.871 0.042 . . . . . 4267 3 41 . 1 1 56 56 ILE N N 15 0.855 0.056 . . . . . 4267 3 42 . 1 1 57 57 TYR N N 15 0.829 0.039 . . . . . 4267 3 43 . 1 1 58 58 GLU N N 15 0.855 0.029 . . . . . 4267 3 44 . 1 1 60 60 LYS N N 15 0.793 0.025 . . . . . 4267 3 45 . 1 1 61 61 GLU N N 15 0.899 0.108 . . . . . 4267 3 46 . 1 1 62 62 ASP N N 15 0.854 0.032 . . . . . 4267 3 47 . 1 1 63 63 LYS N N 15 0.805 0.024 . . . . . 4267 3 48 . 1 1 64 64 SER N N 15 0.834 0.025 . . . . . 4267 3 49 . 1 1 65 65 TYR N N 15 0.820 0.034 . . . . . 4267 3 50 . 1 1 66 66 ASN N N 15 0.777 0.025 . . . . . 4267 3 51 . 1 1 67 67 VAL N N 15 0.854 0.041 . . . . . 4267 3 52 . 1 1 68 68 THR N N 15 0.840 0.040 . . . . . 4267 3 53 . 1 1 69 69 SER N N 15 0.905 0.070 . . . . . 4267 3 54 . 1 1 71 71 LEU N N 15 0.901 0.038 . . . . . 4267 3 55 . 1 1 73 73 ARG N N 15 0.818 0.026 . . . . . 4267 3 56 . 1 1 76 76 LYS N N 15 0.796 0.029 . . . . . 4267 3 57 . 1 1 77 77 CYS N N 15 0.832 0.039 . . . . . 4267 3 58 . 1 1 78 78 ASP N N 15 0.850 0.042 . . . . . 4267 3 59 . 1 1 79 79 TYR N N 15 0.923 0.031 . . . . . 4267 3 60 . 1 1 80 80 TRP N N 15 0.823 0.034 . . . . . 4267 3 61 . 1 1 82 82 ARG N N 15 0.913 0.062 . . . . . 4267 3 62 . 1 1 83 83 THR N N 15 0.878 0.029 . . . . . 4267 3 63 . 1 1 84 84 PHE N N 15 0.806 0.056 . . . . . 4267 3 64 . 1 1 87 87 GLY N N 15 0.865 0.061 . . . . . 4267 3 65 . 1 1 88 88 CYS N N 15 0.812 0.029 . . . . . 4267 3 66 . 1 1 89 89 GLN N N 15 0.815 0.027 . . . . . 4267 3 67 . 1 1 92 92 GLU N N 15 0.781 0.023 . . . . . 4267 3 68 . 1 1 93 93 PHE N N 15 0.834 0.040 . . . . . 4267 3 69 . 1 1 94 94 THR N N 15 0.809 0.027 . . . . . 4267 3 70 . 1 1 95 95 LEU N N 15 0.868 0.026 . . . . . 4267 3 71 . 1 1 96 96 GLY N N 15 0.816 0.056 . . . . . 4267 3 72 . 1 1 97 97 ASN N N 15 0.827 0.134 . . . . . 4267 3 73 . 1 1 98 98 ILE N N 15 0.840 0.027 . . . . . 4267 3 74 . 1 1 99 99 LYS N N 15 0.786 0.024 . . . . . 4267 3 75 . 1 1 100 100 SER N N 15 0.816 0.029 . . . . . 4267 3 76 . 1 1 101 101 TYR N N 15 0.856 0.028 . . . . . 4267 3 77 . 1 1 104 104 LEU N N 15 0.841 0.027 . . . . . 4267 3 78 . 1 1 105 105 THR N N 15 0.879 0.061 . . . . . 4267 3 79 . 1 1 106 106 SER N N 15 0.851 0.029 . . . . . 4267 3 80 . 1 1 107 107 TYR N N 15 0.828 0.025 . . . . . 4267 3 81 . 1 1 108 108 LEU N N 15 0.790 0.024 . . . . . 4267 3 82 . 1 1 109 109 VAL N N 15 0.859 0.026 . . . . . 4267 3 83 . 1 1 110 110 ARG N N 15 0.809 0.035 . . . . . 4267 3 84 . 1 1 112 112 VAL N N 15 0.759 0.036 . . . . . 4267 3 85 . 1 1 113 113 SER N N 15 0.808 0.024 . . . . . 4267 3 86 . 1 1 115 115 ASN N N 15 0.789 0.047 . . . . . 4267 3 87 . 1 1 116 116 TYR N N 15 0.766 0.024 . . . . . 4267 3 88 . 1 1 117 117 ASN N N 15 0.817 0.028 . . . . . 4267 3 89 . 1 1 118 118 GLN N N 15 0.813 0.028 . . . . . 4267 3 90 . 1 1 119 119 HIS N N 15 0.849 0.037 . . . . . 4267 3 91 . 1 1 120 120 ALA N N 15 0.842 0.032 . . . . . 4267 3 92 . 1 1 122 122 VAL N N 15 0.823 0.056 . . . . . 4267 3 93 . 1 1 123 123 PHE N N 15 0.816 0.026 . . . . . 4267 3 94 . 1 1 124 124 PHE N N 15 0.821 0.025 . . . . . 4267 3 95 . 1 1 125 125 LYS N N 15 0.804 0.024 . . . . . 4267 3 96 . 1 1 127 127 VAL N N 15 0.810 0.026 . . . . . 4267 3 97 . 1 1 128 128 SER N N 15 0.863 0.040 . . . . . 4267 3 98 . 1 1 129 129 GLN N N 15 0.774 0.066 . . . . . 4267 3 99 . 1 1 130 130 ASN N N 15 0.813 0.043 . . . . . 4267 3 100 . 1 1 131 131 ARG N N 15 0.868 0.026 . . . . . 4267 3 101 . 1 1 132 132 GLU N N 15 0.829 0.025 . . . . . 4267 3 102 . 1 1 133 133 TYR N N 15 0.818 0.033 . . . . . 4267 3 103 . 1 1 134 134 PHE N N 15 0.776 0.023 . . . . . 4267 3 104 . 1 1 135 135 LYS N N 15 0.806 0.024 . . . . . 4267 3 105 . 1 1 136 136 ILE N N 15 0.769 0.023 . . . . . 4267 3 106 . 1 1 137 137 THR N N 15 0.859 0.043 . . . . . 4267 3 107 . 1 1 138 138 LEU N N 15 0.823 0.025 . . . . . 4267 3 108 . 1 1 139 139 TYR N N 15 0.810 0.040 . . . . . 4267 3 109 . 1 1 140 140 GLY N N 15 0.761 0.037 . . . . . 4267 3 110 . 1 1 141 141 ARG N N 15 0.855 0.041 . . . . . 4267 3 111 . 1 1 142 142 THR N N 15 0.821 0.030 . . . . . 4267 3 112 . 1 1 143 143 LYS N N 15 0.900 0.060 . . . . . 4267 3 113 . 1 1 144 144 GLU N N 15 0.899 0.027 . . . . . 4267 3 114 . 1 1 146 146 THR N N 15 0.969 0.042 . . . . . 4267 3 115 . 1 1 148 148 GLU N N 15 0.799 0.050 . . . . . 4267 3 116 . 1 1 150 150 LYS N N 15 0.787 0.024 . . . . . 4267 3 117 . 1 1 151 151 GLU N N 15 0.799 0.024 . . . . . 4267 3 118 . 1 1 152 152 ASN N N 15 0.773 0.023 . . . . . 4267 3 119 . 1 1 153 153 PHE N N 15 0.765 0.057 . . . . . 4267 3 120 . 1 1 154 154 ILE N N 15 0.777 0.023 . . . . . 4267 3 121 . 1 1 155 155 ARG N N 15 0.776 0.023 . . . . . 4267 3 122 . 1 1 156 156 PHE N N 15 0.796 0.024 . . . . . 4267 3 123 . 1 1 157 157 SER N N 15 0.799 0.024 . . . . . 4267 3 124 . 1 1 158 158 LYS N N 15 0.776 0.026 . . . . . 4267 3 125 . 1 1 159 159 SER N N 15 0.865 0.038 . . . . . 4267 3 126 . 1 1 160 160 LEU N N 15 0.820 0.028 . . . . . 4267 3 127 . 1 1 161 161 GLY N N 15 0.787 0.024 . . . . . 4267 3 128 . 1 1 162 162 LEU N N 15 0.806 0.024 . . . . . 4267 3 129 . 1 1 165 165 ASN N N 15 0.742 0.032 . . . . . 4267 3 130 . 1 1 167 167 ILE N N 15 0.831 0.034 . . . . . 4267 3 131 . 1 1 168 168 VAL N N 15 0.821 0.025 . . . . . 4267 3 132 . 1 1 169 169 PHE N N 15 0.921 0.033 . . . . . 4267 3 133 . 1 1 171 171 VAL N N 15 0.808 0.028 . . . . . 4267 3 134 . 1 1 173 173 ILE N N 15 0.832 0.149 . . . . . 4267 3 135 . 1 1 175 175 GLN N N 15 1.052 0.061 . . . . . 4267 3 136 . 1 1 176 176 CYS N N 15 0.949 0.122 . . . . . 4267 3 137 . 1 1 178 178 ASP N N 15 0.871 0.044 . . . . . 4267 3 138 . 1 1 179 179 GLY N N 15 0.910 0.032 . . . . . 4267 3 139 . 1 1 32 32 TRP NE1 N 15 0.924 0.028 . . . . . 4267 3 140 . 1 1 80 80 TRP NE1 N 15 0.694 0.035 . . . . . 4267 3 141 . 1 1 110 110 ARG NE N 15 1.078 0.081 . . . . . 4267 3 stop_ save_