######################################## # Heteronuclear T1 relaxation values # ######################################## save_T1_c_domain _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode T1_c_domain _Heteronucl_T1_list.Entry_ID 4801 _Heteronucl_T1_list.ID 1 _Heteronucl_T1_list.Sample_condition_list_ID 1 _Heteronucl_T1_list.Sample_condition_list_label $Cond_1 _Heteronucl_T1_list.Spectrometer_frequency_1H 500 _Heteronucl_T1_list.T1_coherence_type 1H _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details ; T1 values for some hyperfine shifted protons as measured in standard inversion-recovery experiments ; _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID . . 1 $sample_1 . 4801 1 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 69 69 HIS HD1 . . 1 10 . . . . . 4801 1 2 . 1 1 69 69 HIS HE1 . . 3 5 . . . . . 4801 1 3 . 1 1 106 106 MET HB2 . . 7 5 . . . . . 4801 1 4 . 1 1 106 106 MET HG3 . . 14 5 . . . . . 4801 1 5 . 1 1 106 106 MET HE . . 4 5 . . . . . 4801 1 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_T1_heme _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode T1_heme _Heteronucl_T1_list.Entry_ID 4801 _Heteronucl_T1_list.ID 2 _Heteronucl_T1_list.Sample_condition_list_ID 1 _Heteronucl_T1_list.Sample_condition_list_label $Cond_1 _Heteronucl_T1_list.Spectrometer_frequency_1H 500 _Heteronucl_T1_list.T1_coherence_type 1H _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details ; T1 values for some hyperfine shifted protons as measured in standard inversion-recovery experiments ; _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID . . 1 $sample_1 . 4801 2 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 2 2 1 1 HEC 1HMC . . 73 5 . . . . . 4801 2 2 . 2 2 1 1 HEC 2HMC . . 73 5 . . . . . 4801 2 3 . 2 2 1 1 HEC 3HMC . . 73 5 . . . . . 4801 2 4 . 2 2 1 1 HEC 1HMD . . 101 5 . . . . . 4801 2 5 . 2 2 1 1 HEC 2HMD . . 101 5 . . . . . 4801 2 6 . 2 2 1 1 HEC 3HMD . . 101 5 . . . . . 4801 2 7 . 2 2 1 1 HEC 1HMA . . 130 5 . . . . . 4801 2 8 . 2 2 1 1 HEC 2HMA . . 130 5 . . . . . 4801 2 9 . 2 2 1 1 HEC 3HMA . . 130 5 . . . . . 4801 2 stop_ save_