######################## # Kinetic parameters # ######################## ############################# # Hydrogen exchange rates # ############################# save_H_exch_rates_1 _H_exch_rate_list.Sf_category H_exch_rates _H_exch_rate_list.Sf_framecode H_exch_rates_1 _H_exch_rate_list.Entry_ID 50115 _H_exch_rate_list.ID 1 _H_exch_rate_list.Name . _H_exch_rate_list.Sample_condition_list_ID 1 _H_exch_rate_list.Sample_condition_list_label $sample_conditions_1 _H_exch_rate_list.Val_units s-1 _H_exch_rate_list.Details ; Bruker pulse sequence used: fhsqccxf3gpph. Spin lock times used: 10 ms, 15 ms, 20 ms, 25 ms, 30 ms, 40 ms, 50 ms, 75 ms, and 100 ms. relaxation delay of 3 s was used. ; _H_exch_rate_list.Text_data_format . _H_exch_rate_list.Text_data . loop_ _H_exch_rate_experiment.Experiment_ID _H_exch_rate_experiment.Experiment_name _H_exch_rate_experiment.Sample_ID _H_exch_rate_experiment.Sample_label _H_exch_rate_experiment.Sample_state _H_exch_rate_experiment.Entry_ID _H_exch_rate_experiment.H_exch_rate_list_ID 9 'CLEANEX-PM (15N-HSQC)' . . . 50115 1 stop_ loop_ _H_exch_rate.ID _H_exch_rate.Assembly_atom_ID _H_exch_rate.Entity_assembly_ID _H_exch_rate.Entity_ID _H_exch_rate.Comp_index_ID _H_exch_rate.Seq_ID _H_exch_rate.Comp_ID _H_exch_rate.Atom_ID _H_exch_rate.Atom_type _H_exch_rate.Atom_isotope_number _H_exch_rate.Val _H_exch_rate.Val_min _H_exch_rate.Val_max _H_exch_rate.Val_err _H_exch_rate.Resonance_ID _H_exch_rate.Auth_entity_assembly_ID _H_exch_rate.Auth_seq_ID _H_exch_rate.Auth_comp_ID _H_exch_rate.Auth_atom_ID _H_exch_rate.Entry_ID _H_exch_rate.H_exch_rate_list_ID 1 . 1 1 3 3 ALA H H 1 14.24 . . 0.31 . . 0 ALA H 50115 1 2 . 1 1 4 4 MET H H 1 9.98 . . 0.14 . . 1 MET H 50115 1 3 . 1 1 5 5 THR H H 1 3.33 . . 0.06 . . 2 THR H 50115 1 4 . 1 1 7 7 VAL H H 1 0.64 . . 0.02 . . 4 VAL H 50115 1 5 . 1 1 8 8 ARG H H 1 1.17 . . 0.03 . . 5 ARG H 50115 1 6 . 1 1 12 12 THR H H 1 8.8 . . 0.26 . . 9 THR H 50115 1 7 . 1 1 14 14 ASP H H 1 2.41 . . 0.04 . . 11 ASP H 50115 1 8 . 1 1 16 16 LEU H H 1 0.75 . . 0.03 . . 13 LEU H 50115 1 9 . 1 1 17 17 ASN H H 1 2.43 . . 0.03 . . 14 ASN H 50115 1 10 . 1 1 18 18 LEU H H 1 3.06 . . 0.08 . . 15 LEU H 50115 1 11 . 1 1 19 19 ARG H H 1 2.06 . . 0.03 . . 16 ARG H 50115 1 12 . 1 1 20 20 GLY H H 1 8.34 . . 0.16 . . 17 GLY H 50115 1 13 . 1 1 22 22 LEU H H 1 1.31 . . 0.01 . . 19 LEU H 50115 1 14 . 1 1 23 23 ASP H H 1 1.11 . . 0.02 . . 20 ASP H 50115 1 15 . 1 1 24 24 GLY H H 1 0.83 . . 0.02 . . 21 GLY H 50115 1 16 . 1 1 26 26 ARG H H 1 5.92 . . 0.1 . . 23 ARG H 50115 1 17 . 1 1 27 27 TRP H H 1 2.29 . . 0.11 . . 24 TRP H 50115 1 18 . 1 1 28 28 ARG H H 1 3.2 . . 0.08 . . 25 ARG H 50115 1 19 . 1 1 29 29 ARG H H 1 4.37 . . 0.05 . . 26 ARG H 50115 1 20 . 1 1 30 30 ALA H H 1 3.39 . . 0.04 . . 27 ALA H 50115 1 21 . 1 1 31 31 GLU H H 1 1.37 . . 0.01 . . 28 GLU H 50115 1 22 . 1 1 33 33 ALA H H 1 3.58 . . 0.07 . . 30 ALA H 50115 1 23 . 1 1 34 34 GLN H H 1 7.25 . . 0.12 . . 31 GLN H 50115 1 24 . 1 1 35 35 SER H H 1 16.41 . . 0.22 . . 32 SER H 50115 1 25 . 1 1 36 36 ARG H H 1 12.54 . . 0.31 . . 33 ARG H 50115 1 26 . 1 1 37 37 ARG H H 1 8 . . 0.11 . . 34 ARG H 50115 1 27 . 1 1 39 39 GLY H H 1 10.82 . . 0.18 . . 36 GLY H 50115 1 28 . 1 1 40 40 ARG H H 1 13.9 . . 0.24 . . 37 ARG H 50115 1 29 . 1 1 41 41 SER H H 1 22.3 . . 0.87 . . 38 SER H 50115 1 30 . 1 1 42 42 ARG H H 1 9.34 . . 0.16 . . 39 ARG H 50115 1 31 . 1 1 44 44 GLY H H 1 12.24 . . 0.24 . . 41 GLY H 50115 1 32 . 1 1 45 45 GLY H H 1 9.5 . . 0.15 . . 42 GLY H 50115 1 33 . 1 1 46 46 ALA H H 1 3.47 . . 0.06 . . 43 ALA H 50115 1 34 . 1 1 48 48 LEU H H 1 1.04 . . 0.03 . . 45 LEU H 50115 1 35 . 1 1 49 49 ARG H H 1 4.46 . . 0.07 . . 46 ARG H 50115 1 36 . 1 1 50 50 TYR H H 1 4.9 . . 0.05 . . 47 TYR H 50115 1 37 . 1 1 51 51 HIS H H 1 19.33 . . 0.49 . . 48 HIS H 50115 1 38 . 1 1 52 52 ARG H H 1 21.49 . . 0.51 . . 49 ARG H 50115 1 39 . 1 1 53 53 THR H H 1 12.22 . . 0.21 . . 50 THR H 50115 1 40 . 1 1 54 54 GLY H H 1 16.64 . . 0.14 . . 51 GLY H 50115 1 41 . 1 1 55 55 VAL H H 1 4.45 . . 0.05 . . 52 VAL H 50115 1 42 . 1 1 56 56 GLY H H 1 7.18 . . 0.14 . . 53 GLY H 50115 1 43 . 1 1 57 57 MET H H 1 9.31 . . 0.17 . . 54 MET H 50115 1 44 . 1 1 58 58 SER H H 1 19.5 . . 0.32 . . 55 SER H 50115 1 45 . 1 1 59 59 ARG H H 1 23.06 . . 1.04 . . 56 ARG H 50115 1 46 . 1 1 60 60 THR H H 1 12.95 . . 0.3 . . 57 THR H 50115 1 47 . 1 1 61 61 GLY H H 1 17.9 . . 0.23 . . 58 GLY H 50115 1 48 . 1 1 63 63 GLY H H 1 25.55 . . 1.01 . . 60 GLY H 50115 1 49 . 1 1 64 64 SER H H 1 15.58 . . 0.51 . . 61 SER H 50115 1 50 . 1 1 65 65 ARG H H 1 4.2 . . 0.03 . . 62 ARG H 50115 1 stop_ save_