######################################## # Heteronuclear T2 relaxation values # ######################################## save_heteronucl_T2_relaxation_1 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_1 _Heteronucl_T2_list.Entry_ID 52175 _Heteronucl_T2_list.ID 1 _Heteronucl_T2_list.Name 'Lac 0.029 mM' _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'no temperature control applied' _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type S(+,-) _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format text _Heteronucl_T2_list.Text_data ; DATA CARRIER_FREQ (MHz) 60.790000 DATA NUCPMG (Hz) @CARRIER_FREQ 1 33.33 33.33 66.67 66.67 100.00 133.33 133.33 166.67 200.00 233.33 266.67 300.00 333.33 400.00 533.33 700.00 966.67 DATA ASSIGNMENTS 1 144 2 147 3 155 4 174 5 176 6 183 7 184 8 187 DATA R2 (s-1) @CARRIER_FREQ 1 1 13.3721 13.3058 13.0567 13.3336 13.1423 12.8597 12.9946 12.7965 12.7063 12.6789 12.7960 12.8892 12.8004 12.4074 12.3925 12.1851 12.2414 2 14.2698 14.2599 13.5933 13.5656 13.3831 13.9716 14.0894 13.6582 13.4313 13.4494 13.4114 13.4159 13.1067 12.9834 13.2629 12.4858 12.7486 3 14.2830 14.2705 13.8582 14.2790 13.8824 13.8056 13.7779 13.7826 13.6887 13.8597 13.3808 13.7681 13.4163 13.0658 13.2045 13.3200 12.9799 4 16.4074 15.9739 15.8560 15.3473 15.3031 16.0194 15.4401 14.7620 14.7445 14.5345 14.7914 14.1952 14.3491 13.4573 13.0262 13.1621 12.8111 5 14.2406 13.9686 14.1288 14.1158 13.6094 14.1059 13.5892 13.8544 13.6187 13.8255 13.5775 13.8047 13.5092 13.3003 13.3095 13.3518 13.0595 6 21.0792 21.4633 20.8500 20.8236 20.3158 20.2053 20.7980 19.7372 20.0209 19.6188 19.3907 18.8411 18.7921 18.4268 17.9066 18.5371 17.3507 7 17.7137 17.5793 17.1971 17.2926 17.0312 16.0714 16.1086 16.2166 15.1849 15.2002 15.1146 14.2365 14.1382 13.7452 13.1893 13.0277 12.5717 8 13.8429 13.4378 13.1869 13.6250 13.5380 13.1688 13.2862 13.1176 13.0265 12.6457 12.9372 12.8047 12.7672 12.7026 12.8808 12.1894 12.3161 DATA R2ERRORS (s-1) @CARRIER_FREQ 1 1 0.1189 0.1185 0.1171 0.1187 0.1176 0.1159 0.1167 0.1156 0.1150 0.1149 0.1156 0.1161 0.1156 0.1134 0.1133 0.1121 0.1125 2 0.0836 0.0836 0.0808 0.0807 0.0799 0.0823 0.0828 0.0811 0.0801 0.0802 0.0801 0.0801 0.0789 0.0784 0.0795 0.0765 0.0775 3 0.1679 0.1678 0.1643 0.1678 0.1645 0.1639 0.1636 0.1637 0.1629 0.1643 0.1604 0.1636 0.1607 0.1579 0.1590 0.1599 0.1572 4 0.3635 0.3553 0.3531 0.3439 0.3431 0.3562 0.3456 0.3337 0.3334 0.3298 0.3342 0.3242 0.3267 0.3123 0.3057 0.3078 0.3025 5 0.1828 0.1803 0.1818 0.1817 0.1771 0.1816 0.1769 0.1793 0.1772 0.1790 0.1768 0.1788 0.1762 0.1744 0.1744 0.1748 0.1723 6 0.1975 0.2018 0.1950 0.1947 0.1893 0.1882 0.1944 0.1834 0.1863 0.1822 0.1799 0.1746 0.1742 0.1708 0.1660 0.1718 0.1612 7 0.0841 0.0835 0.0818 0.0822 0.0811 0.0771 0.0772 0.0777 0.0736 0.0737 0.0734 0.0701 0.0698 0.0684 0.0665 0.0660 0.0645 8 0.2803 0.2747 0.2712 0.2772 0.2760 0.2710 0.2726 0.2703 0.2691 0.2641 0.2679 0.2661 0.2657 0.2648 0.2671 0.2582 0.2598 ; loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '1H-15N CPMG' . . . 52175 1 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 52175 1 2 $software_2 . . 52175 1 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_heteronucl_T2_relaxation_2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_2 _Heteronucl_T2_list.Entry_ID 52175 _Heteronucl_T2_list.ID 2 _Heteronucl_T2_list.Name 'Lac 0.058 mM' _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'no temperature control applied' _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type S(+,-) _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format text _Heteronucl_T2_list.Text_data ; DATA CARRIER_FREQ (MHz) 60.790000 DATA NUCPMG (Hz) @CARRIER_FREQ 1 33.33 33.33 66.67 66.67 100.00 133.33 133.33 166.67 200.00 233.33 266.67 300.00 333.33 400.00 533.33 700.00 966.67 DATA ASSIGNMENTS 1 144 2 147 3 155 4 174 5 176 6 183 7 184 8 187 DATA R2 (s-1) @CARRIER_FREQ 1 1 13.1306 13.2403 12.9123 12.9520 12.5521 12.8380 12.7395 13.0221 12.6983 12.5292 12.8615 12.6871 12.9557 12.2518 12.5178 12.5277 11.8962 2 14.4176 14.4831 14.2122 14.1974 13.5508 13.6360 13.8789 13.7192 13.6501 13.7975 13.1986 13.5768 13.0290 12.8892 13.2410 13.2359 12.9117 3 14.6596 14.0432 14.0150 14.1044 13.6791 14.1415 13.5886 13.8367 14.0171 13.6886 13.2647 13.8818 13.7912 13.4610 13.3371 13.2489 12.7447 4 16.0150 15.8044 15.7769 15.3496 15.2505 15.2926 15.0244 14.5664 14.3332 14.3501 14.0439 13.8703 13.6079 13.3846 12.9189 13.6838 12.6753 5 14.1491 14.2710 14.4807 13.8755 12.9492 14.4073 14.2217 13.6777 13.3540 13.0793 13.5097 13.4482 12.8898 13.0480 12.9722 13.3931 12.8219 6 21.1256 21.0614 20.9130 21.4656 20.6525 19.7811 20.4494 19.3001 19.4196 19.8632 18.8461 18.9871 18.4104 18.3242 18.4255 18.4643 17.5319 7 18.4842 17.5528 17.3524 17.0655 17.1276 16.0673 16.9779 15.5055 15.8947 15.2993 15.5889 14.9572 14.5880 14.1144 13.4153 12.9580 12.2440 8 13.7024 13.6132 13.5117 13.5408 13.3005 13.0867 12.7489 13.0587 13.1721 12.8658 12.8485 12.6429 12.7101 12.9414 12.2077 12.1622 11.8952 DATA R2ERRORS (s-1) @CARRIER_FREQ 1 1 0.0848 0.0853 0.0839 0.0841 0.0824 0.0836 0.0832 0.0844 0.0830 0.0823 0.0837 0.0830 0.0841 0.0812 0.0823 0.0823 0.0798 2 0.0954 0.0957 0.0944 0.0943 0.0913 0.0917 0.0928 0.0921 0.0917 0.0924 0.0897 0.0914 0.0889 0.0883 0.0899 0.0899 0.0884 3 0.3862 0.3743 0.3738 0.3754 0.3675 0.3762 0.3658 0.3704 0.3738 0.3676 0.3599 0.3712 0.3696 0.3635 0.3612 0.3596 0.3508 4 0.0796 0.0788 0.0786 0.0769 0.0765 0.0767 0.0756 0.0739 0.0730 0.0731 0.0719 0.0713 0.0704 0.0696 0.0680 0.0706 0.0672 5 0.2288 0.2303 0.2327 0.2257 0.2155 0.2319 0.2297 0.2235 0.2199 0.2169 0.2216 0.2209 0.2148 0.2165 0.2157 0.2203 0.2141 6 0.5049 0.5031 0.4989 0.5145 0.4918 0.4687 0.4863 0.4565 0.4595 0.4708 0.4454 0.4488 0.4350 0.4330 0.4354 0.4363 0.4149 7 0.6817 0.6484 0.6415 0.6317 0.6338 0.5993 0.6288 0.5820 0.5939 0.5758 0.5845 0.5658 0.5551 0.5419 0.5232 0.5114 0.4938 8 0.2120 0.2110 0.2100 0.2103 0.2078 0.2056 0.2022 0.2053 0.2064 0.2033 0.2032 0.2011 0.2018 0.2041 0.1969 0.1964 0.1939 ; loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '1H-15N CPMG' . . . 52175 2 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 52175 2 2 $software_2 . . 52175 2 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_heteronucl_T2_relaxation_3 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_3 _Heteronucl_T2_list.Entry_ID 52175 _Heteronucl_T2_list.ID 3 _Heteronucl_T2_list.Name 'Lac 0.086 mM' _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'no temperature control applied' _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type S(+,-) _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format text _Heteronucl_T2_list.Text_data ; DATA CARRIER_FREQ (MHz) 60.790000 DATA NUCPMG (Hz) @CARRIER_FREQ 1 33.33 33.33 66.67 100.00 133.33 133.33 166.67 200.00 233.33 266.67 300.00 333.33 400.00 533.33 700.00 966.67 DATA ASSIGNMENTS 1 144 2 147 3 155 3 174 5 176 6 183 7 184 8 187 DATA R2 (s-1) @CARRIER_FREQ 1 1 13.4038 13.5768 12.9488 12.8104 12.7792 13.0232 12.8922 12.6581 12.7251 12.8680 12.5756 12.3690 12.4636 12.4677 12.3122 12.0358 2 14.5270 14.1685 14.1477 14.5895 14.3950 14.0164 13.7418 13.5395 13.6785 13.8068 13.7807 13.6271 13.4463 13.0570 13.2562 13.0156 3 13.9559 14.2620 13.9549 13.8004 13.8307 13.9895 13.4499 13.7841 13.7656 13.5142 13.2882 13.2700 13.1822 13.1438 13.2886 12.8375 4 16.2763 16.1888 15.6882 15.4156 15.3181 15.0721 15.3041 15.1142 14.5900 14.0976 13.8477 14.3599 14.1428 13.0825 13.2059 12.6701 5 14.3562 14.3472 14.0132 14.3310 13.1846 13.8586 13.8947 13.2469 13.3031 13.2549 13.3576 13.2830 13.4125 12.8766 12.8987 12.3736 6 21.2650 21.6255 21.5746 19.9467 20.7788 20.4498 19.6092 19.5883 18.9497 18.9885 19.2185 19.1419 18.2425 17.6728 17.8008 17.1359 7 18.1929 18.6019 17.6558 17.2892 16.5382 16.6753 16.7238 15.5606 15.3650 15.1891 15.1600 15.0164 14.1506 13.3844 13.2730 12.4853 8 13.8652 13.5997 13.7446 13.2455 13.3473 13.1218 13.4039 13.3973 12.8959 12.9410 12.9448 12.6248 12.4093 12.5221 12.2934 12.4167 DATA R2ERRORS (s-1) @CARRIER_FREQ 1 1 0.0734 0.0741 0.0718 0.0713 0.0712 0.0721 0.0716 0.0708 0.0710 0.0715 0.0705 0.0698 0.0701 0.0701 0.0696 0.0686 2 0.3315 0.3255 0.3251 0.3325 0.3292 0.3230 0.3185 0.3153 0.3175 0.3196 0.3192 0.3167 0.3138 0.3078 0.3109 0.3072 3 0.2522 0.2562 0.2522 0.2503 0.2506 0.2527 0.2459 0.2501 0.2498 0.2467 0.2439 0.2437 0.2426 0.2422 0.2439 0.2385 4 0.1972 0.1963 0.1912 0.1885 0.1876 0.1852 0.1875 0.1856 0.1807 0.1762 0.1740 0.1786 0.1766 0.1675 0.1685 0.1641 5 0.4603 0.4601 0.4523 0.4597 0.4339 0.4488 0.4496 0.4353 0.4365 0.4354 0.4377 0.4360 0.4389 0.4273 0.4278 0.4169 6 0.3052 0.3114 0.3106 0.2838 0.2971 0.2917 0.2786 0.2782 0.2687 0.2693 0.2727 0.2715 0.2586 0.2508 0.2525 0.2437 7 0.2672 0.2731 0.2596 0.2545 0.2446 0.2464 0.2470 0.2324 0.2300 0.2280 0.2276 0.2259 0.2162 0.2080 0.2068 0.1989 8 0.3148 0.3106 0.3129 0.3052 0.3067 0.3033 0.3076 0.3075 0.2999 0.3006 0.3007 0.2959 0.2928 0.2945 0.2912 0.2929 ; loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '1H-15N CPMG' . . . 52175 3 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 52175 3 2 $software_2 . . 52175 3 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_heteronucl_T2_relaxation_4 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_4 _Heteronucl_T2_list.Entry_ID 52175 _Heteronucl_T2_list.ID 4 _Heteronucl_T2_list.Name 'Lac 0.166 mM' _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'no temperature control applied' _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type S(+,-) _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format text _Heteronucl_T2_list.Text_data ; DATA CARRIER_FREQ (MHz) 60.790000 DATA NUCPMG (Hz) @CARRIER_FREQ 1 33.33 33.33 66.67 66.67 100.00 133.33 166.67 200.00 300.00 400.00 400.00 600.00 700.00 800.00 800.00 966.67 DATA ASSIGNMENTS 1 144 2 147 3 155 4 174 5 176 6 183 7 184 8 187 DATA R2 (s-1) @CARRIER_FREQ 1 1 13.3744 13.8770 12.8075 13.3499 13.0238 13.0738 12.9183 13.0590 12.7158 13.0035 12.3902 12.3780 12.2969 12.3097 12.0098 11.9450 2 14.4093 14.7090 14.7595 14.1158 13.9466 13.8657 13.8796 13.5745 13.0541 13.4521 13.0305 13.0274 13.1463 11.8923 12.5889 12.8518 3 14.2459 14.8809 15.1248 14.0038 14.5497 14.4046 14.4440 14.1015 13.4645 13.5938 13.8969 13.5250 13.8475 13.4618 13.2634 13.4705 4 17.1364 16.4707 16.1879 16.3238 15.9148 16.1480 15.5466 15.2352 14.7064 14.4643 14.2171 13.6275 13.6425 12.9936 13.4480 13.0228 5 14.3101 14.6241 13.7313 14.2104 14.6345 13.8896 14.2174 13.4098 13.3914 13.3564 12.9430 13.0866 13.1923 12.7340 13.0248 12.8025 6 20.8491 21.9478 20.5635 20.9408 20.9510 20.5399 20.3416 19.8750 19.7521 18.5621 18.9281 18.2988 17.7354 17.5667 17.4512 17.5997 7 19.0856 18.4389 18.3981 18.6995 18.1321 17.2275 17.6258 16.7999 15.6784 14.9771 14.5620 14.0376 13.4124 12.7162 12.8439 12.7551 8 13.5595 14.4162 13.7054 13.3520 13.6202 13.3729 13.7952 13.3031 13.1568 12.7607 13.1954 12.2886 12.8019 12.6014 12.5026 12.8390 DATA R2ERRORS (s-1) @CARRIER_FREQ 1 1 0.4115 0.4220 0.4001 0.4110 0.4044 0.4054 0.4023 0.4051 0.3983 0.4040 0.3919 0.3917 0.3902 0.3904 0.3848 0.3835 2 0.4525 0.4595 0.4606 0.4458 0.4420 0.4402 0.4405 0.4338 0.4227 0.4311 0.4222 0.4221 0.4246 0.3993 0.4131 0.4184 3 0.6948 0.7177 0.7267 0.6863 0.7056 0.7004 0.7018 0.6897 0.6679 0.6723 0.6826 0.6699 0.6809 0.6678 0.6612 0.6681 4 0.3993 0.3854 0.3797 0.3825 0.3743 0.3789 0.3672 0.3614 0.3517 0.3473 0.3430 0.3329 0.3332 0.3226 0.3299 0.3230 5 0.2822 0.2867 0.2740 0.2807 0.2869 0.2762 0.2808 0.2696 0.2694 0.2689 0.2634 0.2653 0.2667 0.2607 0.2645 0.2616 6 0.3151 0.3349 0.3101 0.3167 0.3168 0.3097 0.3063 0.2986 0.2965 0.2779 0.2835 0.2740 0.2658 0.2634 0.2618 0.2639 7 0.3335 0.3220 0.3213 0.3266 0.3167 0.3017 0.3082 0.2950 0.2781 0.2682 0.2625 0.2556 0.2477 0.2393 0.2408 0.2397 8 0.3761 0.3928 0.3789 0.3722 0.3773 0.3726 0.3806 0.3713 0.3686 0.3615 0.3693 0.3532 0.3622 0.3586 0.3569 0.3629 ; loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '1H-15N CPMG' . . . 52175 4 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 52175 4 2 $software_2 . . 52175 4 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_heteronucl_T2_relaxation_5 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_5 _Heteronucl_T2_list.Entry_ID 52175 _Heteronucl_T2_list.ID 5 _Heteronucl_T2_list.Name 'Lac 0.217 mM' _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'no temperature control applied' _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type S(+,-) _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format text _Heteronucl_T2_list.Text_data ; DATA CARRIER_FREQ (MHz) 60.790000 DATA NUCPMG (Hz) @CARRIER_FREQ 1 33.33 33.33 66.67 66.67 100.00 133.33 166.67 200.00 300.00 400.00 400.00 600.00 700.00 800.00 800.00 966.67 DATA ASSIGNMENTS 1 144 2 147 3 155 4 174 5 176 6 183 7 184 8 187 DATA R2 (s-1) @CARRIER_FREQ 1 1 13.2846 13.1193 12.7761 13.0436 12.3934 12.7438 12.6485 12.2912 12.6567 12.4317 12.2872 11.8510 12.4502 12.2929 11.9368 11.7933 2 14.2120 14.5592 13.8591 14.3299 13.7288 14.1806 13.8037 13.8279 13.8910 13.7056 13.3649 12.7436 12.9477 12.6756 13.3708 12.7126 3 13.7300 14.0759 13.9475 13.6228 13.8858 13.5269 14.0177 13.6151 13.4198 13.0068 13.1055 13.3730 12.6532 12.7857 12.9477 13.0654 4 16.5306 16.2891 15.6767 15.5781 15.8237 15.3901 15.5326 14.3774 14.9543 14.1415 13.9536 13.5493 13.4883 13.0877 12.4220 12.9292 5 13.5975 14.2718 14.2322 13.7441 14.1439 13.6118 13.3087 13.0896 13.2435 13.1390 13.1858 13.0277 12.8445 12.3786 12.9864 12.5605 6 20.9113 21.1915 20.6541 20.1486 19.7565 19.9286 19.2523 19.1795 18.5295 18.6257 17.8178 17.2137 17.4359 17.0688 17.1052 17.2653 7 18.0813 18.7231 17.8281 17.9564 17.3594 17.1538 17.0291 16.3195 15.4442 14.8248 14.6859 13.7809 13.4443 13.0997 12.7750 12.7557 8 13.7541 13.7880 13.2369 13.7841 13.4697 13.3380 13.3088 13.0244 12.9112 12.7136 12.4461 12.6031 12.5601 12.3012 12.3107 11.7870 DATA R2ERRORS (s-1) @CARRIER_FREQ 1 1 0.2416 0.2396 0.2356 0.2387 0.2312 0.2352 0.2341 0.2300 0.2342 0.2316 0.2300 0.2252 0.2318 0.2301 0.2261 0.2246 2 0.3146 0.3202 0.3090 0.3165 0.3070 0.3141 0.3082 0.3085 0.3095 0.3067 0.3015 0.2923 0.2953 0.2913 0.3016 0.2919 3 0.2486 0.2530 0.2513 0.2473 0.2506 0.2461 0.2522 0.2472 0.2448 0.2398 0.2410 0.2442 0.2356 0.2372 0.2391 0.2405 4 0.2201 0.2173 0.2105 0.2094 0.2121 0.2074 0.2089 0.1968 0.2027 0.1945 0.1927 0.1888 0.1882 0.1845 0.1785 0.1830 5 0.4078 0.4219 0.4211 0.4108 0.4192 0.4081 0.4020 0.3976 0.4007 0.3986 0.3995 0.3964 0.3928 0.3839 0.3956 0.3874 6 0.3593 0.3650 0.3542 0.3445 0.3371 0.3403 0.3280 0.3267 0.3153 0.3170 0.3035 0.2938 0.2973 0.2916 0.2921 0.2946 7 0.3599 0.3726 0.3551 0.3575 0.3463 0.3425 0.3402 0.3277 0.3131 0.3032 0.3011 0.2875 0.2827 0.2779 0.2735 0.2732 8 0.2506 0.2510 0.2442 0.2510 0.2471 0.2454 0.2451 0.2416 0.2403 0.2379 0.2348 0.2367 0.2362 0.2332 0.2333 0.2274 ; loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '1H-15N CPMG' . . . 52175 5 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 52175 5 2 $software_2 . . 52175 5 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_heteronucl_T2_relaxation_6 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_6 _Heteronucl_T2_list.Entry_ID 52175 _Heteronucl_T2_list.ID 6 _Heteronucl_T2_list.Name 'Lac 0.248 mM' _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'no temperature control applied' _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type S(+,-) _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format text _Heteronucl_T2_list.Text_data ; DATA CARRIER_FREQ (MHz) 60.790000 DATA NUCPMG (Hz) @CARRIER_FREQ 1 33.33 33.33 66.67 66.67 100.00 133.33 166.67 200.00 300.00 400.00 400.00 600.00 700.00 800.00 800.00 966.67 DATA ASSIGNMENTS 1 144 2 147 3 155 4 174 5 176 6 183 7 184 8 187 DATA R2 (s-1) @CARRIER_FREQ 1 1 13.5897 13.3192 13.0384 13.1394 13.1737 13.0413 13.1877 12.9655 13.0431 12.8562 12.7606 12.7537 12.4380 12.4876 12.4617 12.3418 2 14.2052 13.9959 13.9904 14.0510 14.0899 13.7294 13.9132 13.4866 13.5784 13.6994 13.3100 12.9863 13.5934 13.1316 13.1609 13.0412 3 14.2480 14.2026 14.0892 13.9290 14.3632 14.2585 13.8001 13.8660 13.6095 13.3311 13.5212 13.2182 13.1254 13.0568 13.0172 12.7915 4 15.9642 15.9954 15.5841 15.5307 15.2748 15.6275 15.4911 14.8923 14.8616 14.9432 14.6621 13.6309 13.6876 13.4308 13.4897 13.0678 5 14.3104 14.1412 14.0718 13.9818 14.2268 13.6370 13.9588 13.6268 13.7880 13.6883 13.4821 13.4411 13.6208 13.6241 13.3741 13.3497 6 20.5711 20.0321 20.2080 19.7327 19.6794 19.5057 19.4320 19.0783 18.8081 18.3871 17.9638 18.1854 17.8805 17.5692 17.9028 17.0906 7 17.0704 17.2853 16.8965 16.7949 16.6877 16.6556 16.5020 15.8303 15.7062 15.1732 14.9326 14.2052 14.2580 13.7758 13.8738 13.2909 8 13.8245 13.5541 13.3481 13.7344 13.4713 13.3047 13.2672 13.1396 13.0034 12.7487 12.7200 12.4664 12.3007 12.3712 12.3162 12.2061 DATA R2ERRORS (s-1) @CARRIER_FREQ 1 1 0.1113 0.1098 0.1083 0.1089 0.1091 0.1083 0.1091 0.1079 0.1083 0.1074 0.1068 0.1068 0.1052 0.1054 0.1053 0.1047 2 0.1979 0.1959 0.1958 0.1964 0.1968 0.1932 0.1950 0.1909 0.1918 0.1929 0.1892 0.1862 0.1919 0.1875 0.1878 0.1867 3 0.1547 0.1544 0.1535 0.1522 0.1556 0.1548 0.1513 0.1518 0.1498 0.1477 0.1492 0.1469 0.1462 0.1457 0.1455 0.1438 4 0.2947 0.2952 0.2889 0.2881 0.2843 0.2895 0.2875 0.2787 0.2783 0.2795 0.2755 0.2614 0.2622 0.2588 0.2596 0.2542 5 0.1317 0.1306 0.1302 0.1296 0.1312 0.1273 0.1294 0.1273 0.1283 0.1277 0.1264 0.1261 0.1272 0.1273 0.1257 0.1255 6 0.3057 0.2968 0.2997 0.2919 0.2911 0.2883 0.2872 0.2817 0.2776 0.2713 0.2652 0.2684 0.2640 0.2596 0.2643 0.2531 7 0.2137 0.2161 0.2117 0.2106 0.2094 0.2090 0.2073 0.2002 0.1989 0.1934 0.1911 0.1841 0.1846 0.1801 0.1810 0.1758 8 0.2001 0.1974 0.1954 0.1992 0.1966 0.1949 0.1946 0.1933 0.1920 0.1896 0.1894 0.1870 0.1855 0.1862 0.1857 0.1847 ; loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '1H-15N CPMG' . . . 52175 6 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 52175 6 2 $software_2 . . 52175 6 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_heteronucl_T2_relaxation_7 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_7 _Heteronucl_T2_list.Entry_ID 52175 _Heteronucl_T2_list.ID 7 _Heteronucl_T2_list.Name 'Lac 0.946 mM' _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'no temperature control applied' _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type S(+,-) _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format text _Heteronucl_T2_list.Text_data ; DATA CARRIER_FREQ (MHz) DATA NUCPMG (Hz) @CARRIER_FREQ 1 33.33 66.67 66.67 100.00 133.33 133.33 166.67 200.00 233.33 300.00 400.00 566.67 700.00 866.67 966.67 DATA ASSIGNMENTS 1 144 2 147 3 155 4 174 5 176 6 183 7 184 8 187 DATA R2 (s-1) @CARRIER_FREQ 1 1 13.43 12.78 12.82 12.51 12.66 12.95 12.80 12.75 13.13 12.72 12.61 12.66 12.51 12.54 12.30 2 13.73 13.49 13.20 13.58 12.89 13.37 13.67 13.31 13.28 13.24 12.95 12.94 12.72 13.06 12.72 3 13.85 13.88 13.59 13.70 13.93 13.85 13.62 13.82 13.45 13.52 13.64 13.71 13.36 13.62 13.87 4 13.76 13.57 13.88 13.72 13.63 13.77 13.63 13.93 13.82 13.52 13.73 13.52 13.50 13.30 13.50 5 14.32 13.65 13.98 14.39 13.91 13.24 14.07 13.76 14.15 13.98 13.29 13.36 13.72 13.20 13.20 6 17.52 17.16 17.19 17.59 17.19 17.36 17.15 17.03 17.53 16.73 17.14 16.92 16.35 16.54 16.45 7 14.11 14.04 14.00 13.68 13.75 13.72 13.80 13.73 13.59 13.84 13.60 13.31 13.29 13.42 13.16 8 13.65 13.47 13.60 13.26 13.28 13.26 13.05 13.06 13.18 13.10 13.14 12.54 12.43 12.62 12.33 DATA R2ERRORS (s-1) @CARRIER_FREQ 1 1 0.25 0.24 0.24 0.24 0.24 0.24 0.24 0.24 0.24 0.24 0.24 0.24 0.24 0.24 0.23 2 0.41 0.40 0.39 0.40 0.39 0.40 0.40 0.40 0.40 0.40 0.39 0.39 0.39 0.39 0.39 3 0.33 0.33 0.33 0.33 0.33 0.33 0.33 0.33 0.33 0.33 0.33 0.33 0.32 0.33 0.33 4 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 5 0.41 0.39 0.40 0.41 0.40 0.39 0.40 0.40 0.40 0.40 0.39 0.39 0.40 0.39 0.39 6 0.09 0.09 0.09 0.09 0.09 0.09 0.09 0.09 0.09 0.09 0.09 0.09 0.09 0.09 0.09 7 0.03 0.03 0.03 0.02 0.03 0.03 0.03 0.03 0.02 0.03 0.02 0.02 0.02 0.02 0.02 8 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.14 0.15 0.14 ; loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '1H-15N CPMG' . . . 52175 7 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 52175 7 2 $software_2 . . 52175 7 stop_ save_