data_52778 ####################### # Entry information # ####################### save_entry_information_1 _Entry.Sf_category entry_information _Entry.Sf_framecode entry_information_1 _Entry.ID 52778 _Entry.Title ; USP7 (G392D mutant) relaxation dispersions ; _Entry.Type macromolecule _Entry.Version_type original _Entry.Submission_date 2024-12-20 _Entry.Accession_date 2024-12-20 _Entry.Last_release_date 2024-12-20 _Entry.Original_release_date 2024-12-20 _Entry.Origination author _Entry.Format_name . _Entry.NMR_STAR_version 3.2.14.0 _Entry.NMR_STAR_dict_location . _Entry.Original_NMR_STAR_version 3.1 _Entry.Experimental_method NMR _Entry.Experimental_method_subtype solution _Entry.Source_data_format . _Entry.Source_data_format_version . _Entry.Generated_software_name . _Entry.Generated_software_version . _Entry.Generated_software_ID . _Entry.Generated_software_label . _Entry.Generated_date . _Entry.DOI . _Entry.UUID . _Entry.Related_coordinate_file_name . _Entry.Details ; All files contain R2 effective rates (with errors) vs CPMG frequency. Data include amide 15N single quantum, methyl 13C single quantum, methyl 13C/1H multiple quantum, methyl 1H triple quantum, and methyl 1H single quantum CPMGs. ; _Entry.BMRB_internal_directory_name . loop_ _Entry_author.Ordinal _Entry_author.Given_name _Entry_author.Family_name _Entry_author.First_initial _Entry_author.Middle_initials _Entry_author.Family_title _Entry_author.ORCID _Entry_author.Entry_ID 1 Gabrielle Valles . J. . 0000-0002-1666-3939 52778 2 Emilie Korchak . J. . . 52778 3 Dmitry Korzhnev . M. . 0000-0002-3556-2447 52778 4 Irina Bezsonova . . . 0000-0002-8629-0349 52778 stop_ loop_ _Release.Release_number _Release.Format_type _Release.Format_version _Release.Date _Release.Submission_date _Release.Type _Release.Author _Release.Detail _Release.Entry_ID 1 . . 2025-05-08 . original BMRB . 52778 stop_ loop_ _Related_entries.Database_name _Related_entries.Database_accession_code _Related_entries.Relationship _Related_entries.Entry_ID BMRB 52777 'USP7 relaxation dispersions' 52778 stop_ save_ ############### # Citations # ############### save_citations_1 _Citation.Sf_category citations _Citation.Sf_framecode citations_1 _Citation.Entry_ID 52778 _Citation.ID 1 _Citation.Name . _Citation.Class 'entry citation' _Citation.CAS_abstract_code . _Citation.MEDLINE_UI_code . _Citation.PubMed_ID . _Citation.DOI . _Citation.Full_citation . _Citation.Title ; Activation Dynamics of Ubiquitin-Specific Protease 7 ; _Citation.Status 'in preparation' _Citation.Type journal _Citation.Journal_abbrev 'Not known' _Citation.Journal_name_full . _Citation.Journal_volume . _Citation.Journal_issue . _Citation.Journal_ASTM . _Citation.Journal_ISSN . _Citation.Journal_CSD . _Citation.Book_title . _Citation.Book_chapter_title . _Citation.Book_volume . _Citation.Book_series . _Citation.Book_publisher . _Citation.Book_publisher_city . _Citation.Book_ISBN . _Citation.Conference_title . _Citation.Conference_site . _Citation.Conference_state_province . _Citation.Conference_country . _Citation.Conference_start_date . _Citation.Conference_end_date . _Citation.Conference_abstract_number . _Citation.Thesis_institution . _Citation.Thesis_institution_city . _Citation.Thesis_institution_country . _Citation.WWW_URL . _Citation.Page_first . _Citation.Page_last . _Citation.Year . _Citation.Details . loop_ _Citation_author.Ordinal _Citation_author.Given_name _Citation_author.Family_name _Citation_author.First_initial _Citation_author.Middle_initials _Citation_author.Family_title _Citation_author.ORCID _Citation_author.Entry_ID _Citation_author.Citation_ID 1 Gabrielle Valles . J. . . 52778 1 2 Emilie Korchak . J. . . 52778 1 3 Nancy Jaiswal . . . . 52778 1 4 Dmitry Korzhnev . M. . . 52778 1 5 Irina Bezsonova . . . . 52778 1 stop_ save_ ############################################# # Molecular system (assembly) description # ############################################# save_assembly_1 _Assembly.Sf_category assembly _Assembly.Sf_framecode assembly_1 _Assembly.Entry_ID 52778 _Assembly.ID 1 _Assembly.Name 'USP7 (G392D mutant)' _Assembly.BMRB_code . _Assembly.Number_of_components 1 _Assembly.Organic_ligands 0 _Assembly.Metal_ions 0 _Assembly.Non_standard_bonds no _Assembly.Ambiguous_conformational_states no _Assembly.Ambiguous_chem_comp_sites . _Assembly.Molecules_in_chemical_exchange no _Assembly.Paramagnetic no _Assembly.Thiol_state . _Assembly.Molecular_mass . _Assembly.Enzyme_commission_number . _Assembly.Details . _Assembly.DB_query_date . _Assembly.DB_query_revised_last_date . loop_ _Entity_assembly.ID _Entity_assembly.Entity_assembly_name _Entity_assembly.Entity_ID _Entity_assembly.Entity_label _Entity_assembly.Asym_ID _Entity_assembly.PDB_chain_ID _Entity_assembly.Experimental_data_reported _Entity_assembly.Physical_state _Entity_assembly.Conformational_isomer _Entity_assembly.Chemical_exchange_state _Entity_assembly.Magnetic_equivalence_group_code _Entity_assembly.Role _Entity_assembly.Details _Entity_assembly.Entry_ID _Entity_assembly.Assembly_ID 1 USP7 1 $entity_1 . . yes native no no . . . 52778 1 stop_ save_ #################################### # Biological polymers and ligands # #################################### save_entity_1 _Entity.Sf_category entity _Entity.Sf_framecode entity_1 _Entity.Entry_ID 52778 _Entity.ID 1 _Entity.BMRB_code . _Entity.Name entity_1 _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polypeptide(L) _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; GSSKKHTGYVGLKNQGATCY MNSLLQTLFFTNQLRKAVYM MPTEGDDSSKSVPLALQRVF YELQHSDKPVGTKKLTKSFG WETLDSFMQHDVQELCRVLL DNVENKMKGTCVEGTIPKLF RGKMVSYIQCKEVDYRSDRR EDYYDIQLSIKGKKNIFESF VDYVAVEQLDGDNKYDAGEH GLQEAEKDVKFLTLPPVLHL QLMRFMYDPQTDQNIKINDR FEFPEQLPLDEFLQKTDPKD PANYILHAVLVHSGDNHGGH YVVYLNPKGDGKWCKFDDDV VSRCTKEEAIEHNYGGHDDD LSVRHCTNAYMLVYIRESKL SEVLQAVTDHDIPQQLVERL QEEKRIEAQKRKERQE ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states yes _Entity.Ambiguous_chem_comp_sites no _Entity.Nstd_monomer no _Entity.Nstd_chirality no _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 356 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'all free' _Entity.Src_method . _Entity.Parent_entity_ID 1 _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight . _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 . GLY . 52778 1 2 . SER . 52778 1 3 . SER . 52778 1 4 . LYS . 52778 1 5 . LYS . 52778 1 6 . HIS . 52778 1 7 . THR . 52778 1 8 . GLY . 52778 1 9 . TYR . 52778 1 10 . VAL . 52778 1 11 . GLY . 52778 1 12 . LEU . 52778 1 13 . LYS . 52778 1 14 . ASN . 52778 1 15 . GLN . 52778 1 16 . GLY . 52778 1 17 . ALA . 52778 1 18 . THR . 52778 1 19 . CYS . 52778 1 20 . TYR . 52778 1 21 . MET . 52778 1 22 . ASN . 52778 1 23 . SER . 52778 1 24 . LEU . 52778 1 25 . LEU . 52778 1 26 . GLN . 52778 1 27 . THR . 52778 1 28 . LEU . 52778 1 29 . PHE . 52778 1 30 . PHE . 52778 1 31 . THR . 52778 1 32 . ASN . 52778 1 33 . GLN . 52778 1 34 . LEU . 52778 1 35 . ARG . 52778 1 36 . LYS . 52778 1 37 . ALA . 52778 1 38 . VAL . 52778 1 39 . TYR . 52778 1 40 . MET . 52778 1 41 . MET . 52778 1 42 . PRO . 52778 1 43 . THR . 52778 1 44 . GLU . 52778 1 45 . GLY . 52778 1 46 . ASP . 52778 1 47 . ASP . 52778 1 48 . SER . 52778 1 49 . SER . 52778 1 50 . LYS . 52778 1 51 . SER . 52778 1 52 . VAL . 52778 1 53 . PRO . 52778 1 54 . LEU . 52778 1 55 . ALA . 52778 1 56 . LEU . 52778 1 57 . GLN . 52778 1 58 . ARG . 52778 1 59 . VAL . 52778 1 60 . PHE . 52778 1 61 . TYR . 52778 1 62 . GLU . 52778 1 63 . LEU . 52778 1 64 . GLN . 52778 1 65 . HIS . 52778 1 66 . SER . 52778 1 67 . ASP . 52778 1 68 . LYS . 52778 1 69 . PRO . 52778 1 70 . VAL . 52778 1 71 . GLY . 52778 1 72 . THR . 52778 1 73 . LYS . 52778 1 74 . LYS . 52778 1 75 . LEU . 52778 1 76 . THR . 52778 1 77 . LYS . 52778 1 78 . SER . 52778 1 79 . PHE . 52778 1 80 . GLY . 52778 1 81 . TRP . 52778 1 82 . GLU . 52778 1 83 . THR . 52778 1 84 . LEU . 52778 1 85 . ASP . 52778 1 86 . SER . 52778 1 87 . PHE . 52778 1 88 . MET . 52778 1 89 . GLN . 52778 1 90 . HIS . 52778 1 91 . ASP . 52778 1 92 . VAL . 52778 1 93 . GLN . 52778 1 94 . GLU . 52778 1 95 . LEU . 52778 1 96 . CYS . 52778 1 97 . ARG . 52778 1 98 . VAL . 52778 1 99 . LEU . 52778 1 100 . LEU . 52778 1 101 . ASP . 52778 1 102 . ASN . 52778 1 103 . VAL . 52778 1 104 . GLU . 52778 1 105 . ASN . 52778 1 106 . LYS . 52778 1 107 . MET . 52778 1 108 . LYS . 52778 1 109 . GLY . 52778 1 110 . THR . 52778 1 111 . CYS . 52778 1 112 . VAL . 52778 1 113 . GLU . 52778 1 114 . GLY . 52778 1 115 . THR . 52778 1 116 . ILE . 52778 1 117 . PRO . 52778 1 118 . LYS . 52778 1 119 . LEU . 52778 1 120 . PHE . 52778 1 121 . ARG . 52778 1 122 . GLY . 52778 1 123 . LYS . 52778 1 124 . MET . 52778 1 125 . VAL . 52778 1 126 . SER . 52778 1 127 . TYR . 52778 1 128 . ILE . 52778 1 129 . GLN . 52778 1 130 . CYS . 52778 1 131 . LYS . 52778 1 132 . GLU . 52778 1 133 . VAL . 52778 1 134 . ASP . 52778 1 135 . TYR . 52778 1 136 . ARG . 52778 1 137 . SER . 52778 1 138 . ASP . 52778 1 139 . ARG . 52778 1 140 . ARG . 52778 1 141 . GLU . 52778 1 142 . ASP . 52778 1 143 . TYR . 52778 1 144 . TYR . 52778 1 145 . ASP . 52778 1 146 . ILE . 52778 1 147 . GLN . 52778 1 148 . LEU . 52778 1 149 . SER . 52778 1 150 . ILE . 52778 1 151 . LYS . 52778 1 152 . GLY . 52778 1 153 . LYS . 52778 1 154 . LYS . 52778 1 155 . ASN . 52778 1 156 . ILE . 52778 1 157 . PHE . 52778 1 158 . GLU . 52778 1 159 . SER . 52778 1 160 . PHE . 52778 1 161 . VAL . 52778 1 162 . ASP . 52778 1 163 . TYR . 52778 1 164 . VAL . 52778 1 165 . ALA . 52778 1 166 . VAL . 52778 1 167 . GLU . 52778 1 168 . GLN . 52778 1 169 . LEU . 52778 1 170 . ASP . 52778 1 171 . GLY . 52778 1 172 . ASP . 52778 1 173 . ASN . 52778 1 174 . LYS . 52778 1 175 . TYR . 52778 1 176 . ASP . 52778 1 177 . ALA . 52778 1 178 . GLY . 52778 1 179 . GLU . 52778 1 180 . HIS . 52778 1 181 . GLY . 52778 1 182 . LEU . 52778 1 183 . GLN . 52778 1 184 . GLU . 52778 1 185 . ALA . 52778 1 186 . GLU . 52778 1 187 . LYS . 52778 1 188 . ASP . 52778 1 189 . VAL . 52778 1 190 . LYS . 52778 1 191 . PHE . 52778 1 192 . LEU . 52778 1 193 . THR . 52778 1 194 . LEU . 52778 1 195 . PRO . 52778 1 196 . PRO . 52778 1 197 . VAL . 52778 1 198 . LEU . 52778 1 199 . HIS . 52778 1 200 . LEU . 52778 1 201 . GLN . 52778 1 202 . LEU . 52778 1 203 . MET . 52778 1 204 . ARG . 52778 1 205 . PHE . 52778 1 206 . MET . 52778 1 207 . TYR . 52778 1 208 . ASP . 52778 1 209 . PRO . 52778 1 210 . GLN . 52778 1 211 . THR . 52778 1 212 . ASP . 52778 1 213 . GLN . 52778 1 214 . ASN . 52778 1 215 . ILE . 52778 1 216 . LYS . 52778 1 217 . ILE . 52778 1 218 . ASN . 52778 1 219 . ASP . 52778 1 220 . ARG . 52778 1 221 . PHE . 52778 1 222 . GLU . 52778 1 223 . PHE . 52778 1 224 . PRO . 52778 1 225 . GLU . 52778 1 226 . GLN . 52778 1 227 . LEU . 52778 1 228 . PRO . 52778 1 229 . LEU . 52778 1 230 . ASP . 52778 1 231 . GLU . 52778 1 232 . PHE . 52778 1 233 . LEU . 52778 1 234 . GLN . 52778 1 235 . LYS . 52778 1 236 . THR . 52778 1 237 . ASP . 52778 1 238 . PRO . 52778 1 239 . LYS . 52778 1 240 . ASP . 52778 1 241 . PRO . 52778 1 242 . ALA . 52778 1 243 . ASN . 52778 1 244 . TYR . 52778 1 245 . ILE . 52778 1 246 . LEU . 52778 1 247 . HIS . 52778 1 248 . ALA . 52778 1 249 . VAL . 52778 1 250 . LEU . 52778 1 251 . VAL . 52778 1 252 . HIS . 52778 1 253 . SER . 52778 1 254 . GLY . 52778 1 255 . ASP . 52778 1 256 . ASN . 52778 1 257 . HIS . 52778 1 258 . GLY . 52778 1 259 . GLY . 52778 1 260 . HIS . 52778 1 261 . TYR . 52778 1 262 . VAL . 52778 1 263 . VAL . 52778 1 264 . TYR . 52778 1 265 . LEU . 52778 1 266 . ASN . 52778 1 267 . PRO . 52778 1 268 . LYS . 52778 1 269 . GLY . 52778 1 270 . ASP . 52778 1 271 . GLY . 52778 1 272 . LYS . 52778 1 273 . TRP . 52778 1 274 . CYS . 52778 1 275 . LYS . 52778 1 276 . PHE . 52778 1 277 . ASP . 52778 1 278 . ASP . 52778 1 279 . ASP . 52778 1 280 . VAL . 52778 1 281 . VAL . 52778 1 282 . SER . 52778 1 283 . ARG . 52778 1 284 . CYS . 52778 1 285 . THR . 52778 1 286 . LYS . 52778 1 287 . GLU . 52778 1 288 . GLU . 52778 1 289 . ALA . 52778 1 290 . ILE . 52778 1 291 . GLU . 52778 1 292 . HIS . 52778 1 293 . ASN . 52778 1 294 . TYR . 52778 1 295 . GLY . 52778 1 296 . GLY . 52778 1 297 . HIS . 52778 1 298 . ASP . 52778 1 299 . ASP . 52778 1 300 . ASP . 52778 1 301 . LEU . 52778 1 302 . SER . 52778 1 303 . VAL . 52778 1 304 . ARG . 52778 1 305 . HIS . 52778 1 306 . CYS . 52778 1 307 . THR . 52778 1 308 . ASN . 52778 1 309 . ALA . 52778 1 310 . TYR . 52778 1 311 . MET . 52778 1 312 . LEU . 52778 1 313 . VAL . 52778 1 314 . TYR . 52778 1 315 . ILE . 52778 1 316 . ARG . 52778 1 317 . GLU . 52778 1 318 . SER . 52778 1 319 . LYS . 52778 1 320 . LEU . 52778 1 321 . SER . 52778 1 322 . GLU . 52778 1 323 . VAL . 52778 1 324 . LEU . 52778 1 325 . GLN . 52778 1 326 . ALA . 52778 1 327 . VAL . 52778 1 328 . THR . 52778 1 329 . ASP . 52778 1 330 . HIS . 52778 1 331 . ASP . 52778 1 332 . ILE . 52778 1 333 . PRO . 52778 1 334 . GLN . 52778 1 335 . GLN . 52778 1 336 . LEU . 52778 1 337 . VAL . 52778 1 338 . GLU . 52778 1 339 . ARG . 52778 1 340 . LEU . 52778 1 341 . GLN . 52778 1 342 . GLU . 52778 1 343 . GLU . 52778 1 344 . LYS . 52778 1 345 . ARG . 52778 1 346 . ILE . 52778 1 347 . GLU . 52778 1 348 . ALA . 52778 1 349 . GLN . 52778 1 350 . LYS . 52778 1 351 . ARG . 52778 1 352 . LYS . 52778 1 353 . GLU . 52778 1 354 . ARG . 52778 1 355 . GLN . 52778 1 356 . GLU . 52778 1 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . GLY 1 1 52778 1 . SER 2 2 52778 1 . SER 3 3 52778 1 . LYS 4 4 52778 1 . LYS 5 5 52778 1 . HIS 6 6 52778 1 . THR 7 7 52778 1 . GLY 8 8 52778 1 . TYR 9 9 52778 1 . VAL 10 10 52778 1 . GLY 11 11 52778 1 . LEU 12 12 52778 1 . LYS 13 13 52778 1 . ASN 14 14 52778 1 . GLN 15 15 52778 1 . GLY 16 16 52778 1 . ALA 17 17 52778 1 . THR 18 18 52778 1 . CYS 19 19 52778 1 . TYR 20 20 52778 1 . MET 21 21 52778 1 . ASN 22 22 52778 1 . SER 23 23 52778 1 . LEU 24 24 52778 1 . LEU 25 25 52778 1 . GLN 26 26 52778 1 . THR 27 27 52778 1 . LEU 28 28 52778 1 . PHE 29 29 52778 1 . PHE 30 30 52778 1 . THR 31 31 52778 1 . ASN 32 32 52778 1 . GLN 33 33 52778 1 . LEU 34 34 52778 1 . ARG 35 35 52778 1 . LYS 36 36 52778 1 . ALA 37 37 52778 1 . VAL 38 38 52778 1 . TYR 39 39 52778 1 . MET 40 40 52778 1 . MET 41 41 52778 1 . PRO 42 42 52778 1 . THR 43 43 52778 1 . GLU 44 44 52778 1 . GLY 45 45 52778 1 . ASP 46 46 52778 1 . ASP 47 47 52778 1 . SER 48 48 52778 1 . SER 49 49 52778 1 . LYS 50 50 52778 1 . SER 51 51 52778 1 . VAL 52 52 52778 1 . PRO 53 53 52778 1 . LEU 54 54 52778 1 . ALA 55 55 52778 1 . LEU 56 56 52778 1 . GLN 57 57 52778 1 . ARG 58 58 52778 1 . VAL 59 59 52778 1 . PHE 60 60 52778 1 . TYR 61 61 52778 1 . GLU 62 62 52778 1 . LEU 63 63 52778 1 . GLN 64 64 52778 1 . HIS 65 65 52778 1 . SER 66 66 52778 1 . ASP 67 67 52778 1 . LYS 68 68 52778 1 . PRO 69 69 52778 1 . VAL 70 70 52778 1 . GLY 71 71 52778 1 . THR 72 72 52778 1 . LYS 73 73 52778 1 . LYS 74 74 52778 1 . LEU 75 75 52778 1 . THR 76 76 52778 1 . LYS 77 77 52778 1 . SER 78 78 52778 1 . PHE 79 79 52778 1 . GLY 80 80 52778 1 . TRP 81 81 52778 1 . GLU 82 82 52778 1 . THR 83 83 52778 1 . LEU 84 84 52778 1 . ASP 85 85 52778 1 . SER 86 86 52778 1 . PHE 87 87 52778 1 . MET 88 88 52778 1 . GLN 89 89 52778 1 . HIS 90 90 52778 1 . ASP 91 91 52778 1 . VAL 92 92 52778 1 . GLN 93 93 52778 1 . GLU 94 94 52778 1 . LEU 95 95 52778 1 . CYS 96 96 52778 1 . ARG 97 97 52778 1 . VAL 98 98 52778 1 . LEU 99 99 52778 1 . LEU 100 100 52778 1 . ASP 101 101 52778 1 . ASN 102 102 52778 1 . VAL 103 103 52778 1 . GLU 104 104 52778 1 . ASN 105 105 52778 1 . LYS 106 106 52778 1 . MET 107 107 52778 1 . LYS 108 108 52778 1 . GLY 109 109 52778 1 . THR 110 110 52778 1 . CYS 111 111 52778 1 . VAL 112 112 52778 1 . GLU 113 113 52778 1 . GLY 114 114 52778 1 . THR 115 115 52778 1 . ILE 116 116 52778 1 . PRO 117 117 52778 1 . LYS 118 118 52778 1 . LEU 119 119 52778 1 . PHE 120 120 52778 1 . ARG 121 121 52778 1 . GLY 122 122 52778 1 . LYS 123 123 52778 1 . MET 124 124 52778 1 . VAL 125 125 52778 1 . SER 126 126 52778 1 . TYR 127 127 52778 1 . ILE 128 128 52778 1 . GLN 129 129 52778 1 . CYS 130 130 52778 1 . LYS 131 131 52778 1 . GLU 132 132 52778 1 . VAL 133 133 52778 1 . ASP 134 134 52778 1 . TYR 135 135 52778 1 . ARG 136 136 52778 1 . SER 137 137 52778 1 . ASP 138 138 52778 1 . ARG 139 139 52778 1 . ARG 140 140 52778 1 . GLU 141 141 52778 1 . ASP 142 142 52778 1 . TYR 143 143 52778 1 . TYR 144 144 52778 1 . ASP 145 145 52778 1 . ILE 146 146 52778 1 . GLN 147 147 52778 1 . LEU 148 148 52778 1 . SER 149 149 52778 1 . ILE 150 150 52778 1 . LYS 151 151 52778 1 . GLY 152 152 52778 1 . LYS 153 153 52778 1 . LYS 154 154 52778 1 . ASN 155 155 52778 1 . ILE 156 156 52778 1 . PHE 157 157 52778 1 . GLU 158 158 52778 1 . SER 159 159 52778 1 . PHE 160 160 52778 1 . VAL 161 161 52778 1 . ASP 162 162 52778 1 . TYR 163 163 52778 1 . VAL 164 164 52778 1 . ALA 165 165 52778 1 . VAL 166 166 52778 1 . GLU 167 167 52778 1 . GLN 168 168 52778 1 . LEU 169 169 52778 1 . ASP 170 170 52778 1 . GLY 171 171 52778 1 . ASP 172 172 52778 1 . ASN 173 173 52778 1 . LYS 174 174 52778 1 . TYR 175 175 52778 1 . ASP 176 176 52778 1 . ALA 177 177 52778 1 . GLY 178 178 52778 1 . GLU 179 179 52778 1 . HIS 180 180 52778 1 . GLY 181 181 52778 1 . LEU 182 182 52778 1 . GLN 183 183 52778 1 . GLU 184 184 52778 1 . ALA 185 185 52778 1 . GLU 186 186 52778 1 . LYS 187 187 52778 1 . ASP 188 188 52778 1 . VAL 189 189 52778 1 . LYS 190 190 52778 1 . PHE 191 191 52778 1 . LEU 192 192 52778 1 . THR 193 193 52778 1 . LEU 194 194 52778 1 . PRO 195 195 52778 1 . PRO 196 196 52778 1 . VAL 197 197 52778 1 . LEU 198 198 52778 1 . HIS 199 199 52778 1 . LEU 200 200 52778 1 . GLN 201 201 52778 1 . LEU 202 202 52778 1 . MET 203 203 52778 1 . ARG 204 204 52778 1 . PHE 205 205 52778 1 . MET 206 206 52778 1 . TYR 207 207 52778 1 . ASP 208 208 52778 1 . PRO 209 209 52778 1 . GLN 210 210 52778 1 . THR 211 211 52778 1 . ASP 212 212 52778 1 . GLN 213 213 52778 1 . ASN 214 214 52778 1 . ILE 215 215 52778 1 . LYS 216 216 52778 1 . ILE 217 217 52778 1 . ASN 218 218 52778 1 . ASP 219 219 52778 1 . ARG 220 220 52778 1 . PHE 221 221 52778 1 . GLU 222 222 52778 1 . PHE 223 223 52778 1 . PRO 224 224 52778 1 . GLU 225 225 52778 1 . GLN 226 226 52778 1 . LEU 227 227 52778 1 . PRO 228 228 52778 1 . LEU 229 229 52778 1 . ASP 230 230 52778 1 . GLU 231 231 52778 1 . PHE 232 232 52778 1 . LEU 233 233 52778 1 . GLN 234 234 52778 1 . LYS 235 235 52778 1 . THR 236 236 52778 1 . ASP 237 237 52778 1 . PRO 238 238 52778 1 . LYS 239 239 52778 1 . ASP 240 240 52778 1 . PRO 241 241 52778 1 . ALA 242 242 52778 1 . ASN 243 243 52778 1 . TYR 244 244 52778 1 . ILE 245 245 52778 1 . LEU 246 246 52778 1 . HIS 247 247 52778 1 . ALA 248 248 52778 1 . VAL 249 249 52778 1 . LEU 250 250 52778 1 . VAL 251 251 52778 1 . HIS 252 252 52778 1 . SER 253 253 52778 1 . GLY 254 254 52778 1 . ASP 255 255 52778 1 . ASN 256 256 52778 1 . HIS 257 257 52778 1 . GLY 258 258 52778 1 . GLY 259 259 52778 1 . HIS 260 260 52778 1 . TYR 261 261 52778 1 . VAL 262 262 52778 1 . VAL 263 263 52778 1 . TYR 264 264 52778 1 . LEU 265 265 52778 1 . ASN 266 266 52778 1 . PRO 267 267 52778 1 . LYS 268 268 52778 1 . GLY 269 269 52778 1 . ASP 270 270 52778 1 . GLY 271 271 52778 1 . LYS 272 272 52778 1 . TRP 273 273 52778 1 . CYS 274 274 52778 1 . LYS 275 275 52778 1 . PHE 276 276 52778 1 . ASP 277 277 52778 1 . ASP 278 278 52778 1 . ASP 279 279 52778 1 . VAL 280 280 52778 1 . VAL 281 281 52778 1 . SER 282 282 52778 1 . ARG 283 283 52778 1 . CYS 284 284 52778 1 . THR 285 285 52778 1 . LYS 286 286 52778 1 . GLU 287 287 52778 1 . GLU 288 288 52778 1 . ALA 289 289 52778 1 . ILE 290 290 52778 1 . GLU 291 291 52778 1 . HIS 292 292 52778 1 . ASN 293 293 52778 1 . TYR 294 294 52778 1 . GLY 295 295 52778 1 . GLY 296 296 52778 1 . HIS 297 297 52778 1 . ASP 298 298 52778 1 . ASP 299 299 52778 1 . ASP 300 300 52778 1 . LEU 301 301 52778 1 . SER 302 302 52778 1 . VAL 303 303 52778 1 . ARG 304 304 52778 1 . HIS 305 305 52778 1 . CYS 306 306 52778 1 . THR 307 307 52778 1 . ASN 308 308 52778 1 . ALA 309 309 52778 1 . TYR 310 310 52778 1 . MET 311 311 52778 1 . LEU 312 312 52778 1 . VAL 313 313 52778 1 . TYR 314 314 52778 1 . ILE 315 315 52778 1 . ARG 316 316 52778 1 . GLU 317 317 52778 1 . SER 318 318 52778 1 . LYS 319 319 52778 1 . LEU 320 320 52778 1 . SER 321 321 52778 1 . GLU 322 322 52778 1 . VAL 323 323 52778 1 . LEU 324 324 52778 1 . GLN 325 325 52778 1 . ALA 326 326 52778 1 . VAL 327 327 52778 1 . THR 328 328 52778 1 . ASP 329 329 52778 1 . HIS 330 330 52778 1 . ASP 331 331 52778 1 . ILE 332 332 52778 1 . PRO 333 333 52778 1 . GLN 334 334 52778 1 . GLN 335 335 52778 1 . LEU 336 336 52778 1 . VAL 337 337 52778 1 . GLU 338 338 52778 1 . ARG 339 339 52778 1 . LEU 340 340 52778 1 . GLN 341 341 52778 1 . GLU 342 342 52778 1 . GLU 343 343 52778 1 . LYS 344 344 52778 1 . ARG 345 345 52778 1 . ILE 346 346 52778 1 . GLU 347 347 52778 1 . ALA 348 348 52778 1 . GLN 349 349 52778 1 . LYS 350 350 52778 1 . ARG 351 351 52778 1 . LYS 352 352 52778 1 . GLU 353 353 52778 1 . ARG 354 354 52778 1 . GLN 355 355 52778 1 . GLU 356 356 52778 1 stop_ save_ #################### # Natural source # #################### save_natural_source_1 _Entity_natural_src_list.Sf_category natural_source _Entity_natural_src_list.Sf_framecode natural_source_1 _Entity_natural_src_list.Entry_ID 52778 _Entity_natural_src_list.ID 1 loop_ _Entity_natural_src.ID _Entity_natural_src.Entity_ID _Entity_natural_src.Entity_label _Entity_natural_src.Entity_chimera_segment_ID _Entity_natural_src.NCBI_taxonomy_ID _Entity_natural_src.Type _Entity_natural_src.Common _Entity_natural_src.Organism_name_scientific _Entity_natural_src.Organism_name_common _Entity_natural_src.Organism_acronym _Entity_natural_src.ICTVdb_decimal_code _Entity_natural_src.Superkingdom _Entity_natural_src.Kingdom _Entity_natural_src.Genus _Entity_natural_src.Species _Entity_natural_src.Strain _Entity_natural_src.Variant _Entity_natural_src.Organ _Entity_natural_src.Tissue _Entity_natural_src.Tissue_fraction _Entity_natural_src.Cell_line _Entity_natural_src.Cell_type _Entity_natural_src.ATCC_number _Entity_natural_src.Organelle _Entity_natural_src.Secretion _Entity_natural_src.Plasmid _Entity_natural_src.Gene_mnemonic _Entity_natural_src.Details _Entity_natural_src.Entry_ID _Entity_natural_src.Entity_natural_src_list_ID 1 1 $entity_1 . 9606 organism . 'Homo sapiens' Human . . Eukaryota Metazoa Homo sapiens . . . . . . . . . . . . . 52778 1 stop_ save_ ######################### # Experimental source # ######################### save_experimental_source_1 _Entity_experimental_src_list.Sf_category experimental_source _Entity_experimental_src_list.Sf_framecode experimental_source_1 _Entity_experimental_src_list.Entry_ID 52778 _Entity_experimental_src_list.ID 1 loop_ _Entity_experimental_src.ID _Entity_experimental_src.Entity_ID _Entity_experimental_src.Entity_label _Entity_experimental_src.Entity_chimera_segment_ID _Entity_experimental_src.Production_method _Entity_experimental_src.Host_org_scientific_name _Entity_experimental_src.Host_org_name_common _Entity_experimental_src.Host_org_details _Entity_experimental_src.Host_org_NCBI_taxonomy_ID _Entity_experimental_src.Host_org_genus _Entity_experimental_src.Host_org_species _Entity_experimental_src.Host_org_strain _Entity_experimental_src.Host_org_variant _Entity_experimental_src.Host_org_ATCC_number _Entity_experimental_src.Vector_type _Entity_experimental_src.PDBview_host_org_vector_name _Entity_experimental_src.PDBview_plasmid_name _Entity_experimental_src.Vector_name _Entity_experimental_src.Vector_details _Entity_experimental_src.Vendor_name _Entity_experimental_src.Details _Entity_experimental_src.Entry_ID _Entity_experimental_src.Entity_experimental_src_list_ID 1 1 $entity_1 . 'recombinant technology' 'Escherichia coli' . . . Escherichia coli . . . plasmid . . pET28a-LIC . . . 52778 1 stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Sample.Sf_category sample _Sample.Sf_framecode sample_1 _Sample.Entry_ID 52778 _Sample.ID 1 _Sample.Name 'USP7 (G392D mutant)' _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number 1 _Sample.Solvent_system '90% H2O/10% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'USP7 (G392D mutant)' '[U-100% 15N], [U-12C/2H, methyl-13CH3]' . . 1 $entity_1 . . 1.0 . . mM . . . . 52778 1 2 Tris 'natural abundance' . . . . . . 20 . . mM . . . . 52778 1 3 NaCl 'natural abundance' . . . . . . 100 . . mM . . . . 52778 1 4 DTT 'natural abundance' . . . . . . 10 . . mM . . . . 52778 1 stop_ save_ ####################### # Sample conditions # ####################### save_sample_conditions_1 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode sample_conditions_1 _Sample_condition_list.Entry_ID 52778 _Sample_condition_list.ID 1 _Sample_condition_list.Name 1 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID 'ionic strength' 100 . mM 52778 1 pH 7.4 . pH 52778 1 pressure 1 . atm 52778 1 temperature 303 . K 52778 1 stop_ save_ ############################ # Computer software used # ############################ save_software_1 _Software.Sf_category software _Software.Sf_framecode software_1 _Software.Entry_ID 52778 _Software.ID 1 _Software.Type . _Software.Name NMRPipe _Software.Version . _Software.DOI . _Software.Details . loop_ _Task.Task _Task.Software_module _Task.Entry_ID _Task.Software_ID processing . 52778 1 stop_ save_ save_software_2 _Software.Sf_category software _Software.Sf_framecode software_2 _Software.Entry_ID 52778 _Software.ID 2 _Software.Type . _Software.Name SPARKY _Software.Version . _Software.DOI . _Software.Details . loop_ _Task.Task _Task.Software_module _Task.Entry_ID _Task.Software_ID 'data analysis' . 52778 2 stop_ save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_NMR_spectrometer_1 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode NMR_spectrometer_1 _NMR_spectrometer.Entry_ID 52778 _NMR_spectrometer.ID 1 _NMR_spectrometer.Name 800 _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model 'AVANCE NEO' _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 800 save_ ############################# # NMR applied experiments # ############################# save_experiment_list_1 _Experiment_list.Sf_category experiment_list _Experiment_list.Sf_framecode experiment_list_1 _Experiment_list.Entry_ID 52778 _Experiment_list.ID 1 _Experiment_list.Details . loop_ _Experiment.ID _Experiment.Name _Experiment.Raw_data_flag _Experiment.NUS_flag _Experiment.Interleaved_flag _Experiment.NMR_spec_expt_ID _Experiment.NMR_spec_expt_label _Experiment.MS_expt_ID _Experiment.MS_expt_label _Experiment.SAXS_expt_ID _Experiment.SAXS_expt_label _Experiment.FRET_expt_ID _Experiment.FRET_expt_label _Experiment.EMR_expt_ID _Experiment.EMR_expt_label _Experiment.Sample_ID _Experiment.Sample_label _Experiment.Sample_state _Experiment.Sample_volume _Experiment.Sample_volume_units _Experiment.Sample_condition_list_ID _Experiment.Sample_condition_list_label _Experiment.Sample_spinning_rate _Experiment.Sample_angle _Experiment.NMR_tube_type _Experiment.NMR_spectrometer_ID _Experiment.NMR_spectrometer_label _Experiment.NMR_spectrometer_probe_ID _Experiment.NMR_spectrometer_probe_label _Experiment.NMR_spectral_processing_ID _Experiment.NMR_spectral_processing_label _Experiment.Mass_spectrometer_ID _Experiment.Mass_spectrometer_label _Experiment.Xray_instrument_ID _Experiment.Xray_instrument_label _Experiment.Fluorescence_instrument_ID _Experiment.Fluorescence_instrument_label _Experiment.EMR_instrument_ID _Experiment.EMR_instrument_label _Experiment.Chromatographic_system_ID _Experiment.Chromatographic_system_label _Experiment.Chromatographic_column_ID _Experiment.Chromatographic_column_label _Experiment.Details _Experiment.Entry_ID _Experiment.Experiment_list_ID 1 '15N TROSY CPMG' no . . . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 52778 1 2 'methyl 1H triple-quantum' no . . . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 52778 1 3 'methyl 13C single quantum' no . . . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 52778 1 4 'methyl 13C/1H multiple quantum' no . . . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 52778 1 5 'methyl 1H single quantum' no . . . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 52778 1 stop_ loop_ _Experiment_file.Experiment_ID _Experiment_file.Experiment_name _Experiment_file.Name _Experiment_file.Type _Experiment_file.Content _Experiment_file.Directory_path _Experiment_file.Details _Experiment_file.Entry_ID _Experiment_file.Experiment_list_ID 1 '15N TROSY CPMG' G392D-1H-SQ-with-fits.xlsx . 'Other kinds of data' . . 52778 1 2 'methyl 1H triple-quantum' G392D-1H-TQ-with-fits.xlsx . 'Other kinds of data' . . 52778 1 3 'methyl 13C single quantum' G392D-13C1H-MQ-with-fits.xlsx . 'Other kinds of data' . . 52778 1 4 'methyl 13C/1H multiple quantum' G392D-13C-SQ-with-fits.xlsx . 'Other kinds of data' . . 52778 1 5 'methyl 1H single quantum' G392D-15N-SQ-with-fits.xlsx . 'Other kinds of data' . . 52778 1 stop_ save_ ######################### # Other kinds of data # ######################### save_other_data_types_1 _Other_data_type_list.Sf_category other_data_types _Other_data_type_list.Sf_framecode other_data_types_1 _Other_data_type_list.Entry_ID 52778 _Other_data_type_list.ID 1 _Other_data_type_list.Name 'methyl 1H triple quantum R2 effective rates' _Other_data_type_list.Definition 'R2 effective rates' _Other_data_type_list.Sample_condition_list_ID 1 _Other_data_type_list.Sample_condition_list_label $sample_conditions_1 _Other_data_type_list.Chem_shift_reference_ID . _Other_data_type_list.Chem_shift_reference_label . _Other_data_type_list.Details 'R2 effective rates (with errors) vs CPMG frequency' _Other_data_type_list.Text_data_format . _Other_data_type_list.Text_data . loop_ _Other_data_experiment.Experiment_ID _Other_data_experiment.Experiment_name _Other_data_experiment.Sample_ID _Other_data_experiment.Sample_label _Other_data_experiment.Sample_state _Other_data_experiment.Entry_ID _Other_data_experiment.Other_data_type_list_ID 2 'methyl 1H triple-quantum' . . . 52778 1 stop_ loop_ _Other_data_software.Software_ID _Other_data_software.Software_label _Other_data_software.Method_ID _Other_data_software.Method_label _Other_data_software.Entry_ID _Other_data_software.Other_data_type_list_ID 1 $software_1 . . 52778 1 2 $software_2 . . 52778 1 stop_ save_ save_other_data_types_2 _Other_data_type_list.Sf_category other_data_types _Other_data_type_list.Sf_framecode other_data_types_2 _Other_data_type_list.Entry_ID 52778 _Other_data_type_list.ID 2 _Other_data_type_list.Name 'methyl 13C/1H multiple quantum R2 effective rates' _Other_data_type_list.Definition 'R2 effective rates' _Other_data_type_list.Sample_condition_list_ID 1 _Other_data_type_list.Sample_condition_list_label $sample_conditions_1 _Other_data_type_list.Chem_shift_reference_ID . _Other_data_type_list.Chem_shift_reference_label . _Other_data_type_list.Details 'R2 effective rates (with errors) vs CPMG frequency' _Other_data_type_list.Text_data_format . _Other_data_type_list.Text_data . loop_ _Other_data_experiment.Experiment_ID _Other_data_experiment.Experiment_name _Other_data_experiment.Sample_ID _Other_data_experiment.Sample_label _Other_data_experiment.Sample_state _Other_data_experiment.Entry_ID _Other_data_experiment.Other_data_type_list_ID 4 'methyl 13C/1H multiple quantum' . . . 52778 2 stop_ loop_ _Other_data_software.Software_ID _Other_data_software.Software_label _Other_data_software.Method_ID _Other_data_software.Method_label _Other_data_software.Entry_ID _Other_data_software.Other_data_type_list_ID 1 $software_1 . . 52778 2 2 $software_2 . . 52778 2 stop_ save_ save_other_data_types_3 _Other_data_type_list.Sf_category other_data_types _Other_data_type_list.Sf_framecode other_data_types_3 _Other_data_type_list.Entry_ID 52778 _Other_data_type_list.ID 3 _Other_data_type_list.Name 'methyl 13C single quantum R2 effective rates' _Other_data_type_list.Definition 'R2 effective rates' _Other_data_type_list.Sample_condition_list_ID 1 _Other_data_type_list.Sample_condition_list_label $sample_conditions_1 _Other_data_type_list.Chem_shift_reference_ID . _Other_data_type_list.Chem_shift_reference_label . _Other_data_type_list.Details 'R2 effective rates (with errors) vs CPMG frequency' _Other_data_type_list.Text_data_format . _Other_data_type_list.Text_data . loop_ _Other_data_experiment.Experiment_ID _Other_data_experiment.Experiment_name _Other_data_experiment.Sample_ID _Other_data_experiment.Sample_label _Other_data_experiment.Sample_state _Other_data_experiment.Entry_ID _Other_data_experiment.Other_data_type_list_ID 3 'methyl 13C single quantum' . . . 52778 3 stop_ loop_ _Other_data_software.Software_ID _Other_data_software.Software_label _Other_data_software.Method_ID _Other_data_software.Method_label _Other_data_software.Entry_ID _Other_data_software.Other_data_type_list_ID 1 $software_1 . . 52778 3 2 $software_2 . . 52778 3 stop_ save_ save_other_data_types_4 _Other_data_type_list.Sf_category other_data_types _Other_data_type_list.Sf_framecode other_data_types_4 _Other_data_type_list.Entry_ID 52778 _Other_data_type_list.ID 4 _Other_data_type_list.Name 'methyl 1H single quantum R2 effective rates' _Other_data_type_list.Definition 'R2 effective rates' _Other_data_type_list.Sample_condition_list_ID 1 _Other_data_type_list.Sample_condition_list_label $sample_conditions_1 _Other_data_type_list.Chem_shift_reference_ID . _Other_data_type_list.Chem_shift_reference_label . _Other_data_type_list.Details 'R2 effective rates (with errors) vs CPMG frequency' _Other_data_type_list.Text_data_format . _Other_data_type_list.Text_data . loop_ _Other_data_experiment.Experiment_ID _Other_data_experiment.Experiment_name _Other_data_experiment.Sample_ID _Other_data_experiment.Sample_label _Other_data_experiment.Sample_state _Other_data_experiment.Entry_ID _Other_data_experiment.Other_data_type_list_ID 5 'methyl 1H single quantum' . . . 52778 4 stop_ loop_ _Other_data_software.Software_ID _Other_data_software.Software_label _Other_data_software.Method_ID _Other_data_software.Method_label _Other_data_software.Entry_ID _Other_data_software.Other_data_type_list_ID 1 $software_1 . . 52778 4 2 $software_2 . . 52778 4 stop_ save_ save_other_data_types_5 _Other_data_type_list.Sf_category other_data_types _Other_data_type_list.Sf_framecode other_data_types_5 _Other_data_type_list.Entry_ID 52778 _Other_data_type_list.ID 5 _Other_data_type_list.Name 'amide 15N single quantum R2 effective rates' _Other_data_type_list.Definition 'R2 effective rates' _Other_data_type_list.Sample_condition_list_ID 1 _Other_data_type_list.Sample_condition_list_label $sample_conditions_1 _Other_data_type_list.Chem_shift_reference_ID . _Other_data_type_list.Chem_shift_reference_label . _Other_data_type_list.Details 'R2 effective rates (with errors) vs CPMG frequency' _Other_data_type_list.Text_data_format . _Other_data_type_list.Text_data . loop_ _Other_data_experiment.Experiment_ID _Other_data_experiment.Experiment_name _Other_data_experiment.Sample_ID _Other_data_experiment.Sample_label _Other_data_experiment.Sample_state _Other_data_experiment.Entry_ID _Other_data_experiment.Other_data_type_list_ID 1 '15N TROSY CPMG' . . . 52778 5 stop_ loop_ _Other_data_software.Software_ID _Other_data_software.Software_label _Other_data_software.Method_ID _Other_data_software.Method_label _Other_data_software.Entry_ID _Other_data_software.Other_data_type_list_ID 1 $software_1 . . 52778 5 2 $software_2 . . 52778 5 stop_ save_