######################################## # Heteronuclear T2 relaxation values # ######################################## save_15N_T2_chain_1_500_pH6 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 15N_T2_chain_1_500_pH6 _Heteronucl_T2_list.Entry_ID 5520 _Heteronucl_T2_list.ID 1 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $condition_1 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 500 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units s _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID . . 1 $Sample_1 . 5520 1 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 2 2 ALA N . . 0.398 0.029 . . . . . . . 5520 1 2 . 1 1 3 3 ALA N . . 0.454 0.032 . . . . . . . 5520 1 3 . 1 1 4 4 VAL N . . 0.458 0.039 . . . . . . . 5520 1 4 . 1 1 5 5 SER N . . 0.308 0.022 . . . . . . . 5520 1 5 . 1 1 6 6 VAL N . . 0.255 0.018 . . . . . . . 5520 1 6 . 1 1 7 7 ASP N . . 0.182 0.016 . . . . . . . 5520 1 7 . 1 1 8 8 CYS N . . 0.186 0.013 . . . . . . . 5520 1 8 . 1 1 9 9 SER N . . 0.178 0.012 . . . . . . . 5520 1 9 . 1 1 10 10 GLU N . . 0.139 0.009 . . . . . . . 5520 1 10 . 1 1 11 11 TYR N . . 0.183 0.012 . . . . . . . 5520 1 11 . 1 1 13 13 LYS N . . 0.207 0.014 . . . . . . . 5520 1 12 . 1 1 15 15 ALA N . . 0.160 0.016 . . . . . . . 5520 1 13 . 1 1 16 16 CYS N . . 0.337 0.040 . . . . . . . 5520 1 14 . 1 1 17 17 THR N . . 0.250 0.024 . . . . . . . 5520 1 15 . 1 1 18 18 LEU N . . 0.431 0.050 . . . . . . . 5520 1 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_15N_T2_chain_2_500_pH6 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 15N_T2_chain_2_500_pH6 _Heteronucl_T2_list.Entry_ID 5520 _Heteronucl_T2_list.ID 2 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $condition_1 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 500 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units s _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID . . 1 $Sample_1 . 5520 2 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 2 2 2 2 TYR N . . 0.224 0.032 . . . . . . . 5520 2 2 . 2 2 3 3 ARG N . . 0.230 0.016 . . . . . . . 5520 2 3 . 2 2 5 5 LEU N . . 0.187 0.013 . . . . . . . 5520 2 4 . 2 2 6 6 CYS N . . 0.195 0.013 . . . . . . . 5520 2 5 . 2 2 7 7 GLY N . . 0.186 0.013 . . . . . . . 5520 2 6 . 2 2 8 8 SER N . . 0.179 0.012 . . . . . . . 5520 2 7 . 2 2 9 9 ASP N . . 0.173 0.012 . . . . . . . 5520 2 8 . 2 2 10 10 ASN N . . 0.191 0.013 . . . . . . . 5520 2 9 . 2 2 11 11 LYS N . . 0.199 0.013 . . . . . . . 5520 2 10 . 2 2 12 12 THR N . . 0.206 0.014 . . . . . . . 5520 2 11 . 2 2 13 13 TYR N . . 0.202 0.014 . . . . . . . 5520 2 12 . 2 2 14 14 GLY N . . 0.189 0.013 . . . . . . . 5520 2 13 . 2 2 15 15 ASN N . . 0.193 0.013 . . . . . . . 5520 2 14 . 2 2 16 16 LYS N . . 0.174 0.012 . . . . . . . 5520 2 15 . 2 2 17 17 CYS N . . 0.194 0.013 . . . . . . . 5520 2 16 . 2 2 18 18 ASN N . . 0.185 0.013 . . . . . . . 5520 2 17 . 2 2 19 19 PHE N . . 0.182 0.012 . . . . . . . 5520 2 18 . 2 2 20 20 CYS N . . 0.179 0.012 . . . . . . . 5520 2 19 . 2 2 21 21 ASN N . . 0.199 0.013 . . . . . . . 5520 2 20 . 2 2 22 22 ALA N . . 0.198 0.013 . . . . . . . 5520 2 21 . 2 2 23 23 VAL N . . 0.190 0.013 . . . . . . . 5520 2 22 . 2 2 24 24 VAL N . . 0.179 0.013 . . . . . . . 5520 2 23 . 2 2 25 25 GLU N . . 0.196 0.013 . . . . . . . 5520 2 24 . 2 2 26 26 SER N . . 0.203 0.014 . . . . . . . 5520 2 25 . 2 2 27 27 ASN N . . 0.193 0.013 . . . . . . . 5520 2 26 . 2 2 28 28 GLY N . . 0.207 0.014 . . . . . . . 5520 2 27 . 2 2 29 29 THR N . . 0.212 0.014 . . . . . . . 5520 2 28 . 2 2 30 30 LEU N . . 0.2 0.014 . . . . . . . 5520 2 29 . 2 2 31 31 THR N . . 0.191 0.013 . . . . . . . 5520 2 30 . 2 2 32 32 LEU N . . 0.200 0.014 . . . . . . . 5520 2 31 . 2 2 33 33 SER N . . 0.187 0.013 . . . . . . . 5520 2 32 . 2 2 34 34 HIS N . . 0.181 0.012 . . . . . . . 5520 2 33 . 2 2 35 35 PHE N . . 0.189 0.013 . . . . . . . 5520 2 34 . 2 2 36 36 GLY N . . 0.189 0.013 . . . . . . . 5520 2 35 . 2 2 37 37 LYS N . . 0.205 0.014 . . . . . . . 5520 2 36 . 2 2 38 38 CYS N . . 0.180 0.012 . . . . . . . 5520 2 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_15N_T2_chain_1_600_pH6 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 15N_T2_chain_1_600_pH6 _Heteronucl_T2_list.Entry_ID 5520 _Heteronucl_T2_list.ID 3 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $condition_1 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units s _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID . . 1 $Sample_1 . 5520 3 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 2 2 ALA N . . 0.305 0.081 . . . . . . . 5520 3 2 . 1 1 3 3 ALA N . . 0.434 0.030 . . . . . . . 5520 3 3 . 1 1 4 4 VAL N . . 0.485 0.038 . . . . . . . 5520 3 4 . 1 1 5 5 SER N . . 0.294 0.020 . . . . . . . 5520 3 5 . 1 1 6 6 VAL N . . 0.260 0.018 . . . . . . . 5520 3 6 . 1 1 7 7 ASP N . . 0.185 0.016 . . . . . . . 5520 3 7 . 1 1 8 8 CYS N . . 0.178 0.012 . . . . . . . 5520 3 8 . 1 1 9 9 SER N . . 0.181 0.012 . . . . . . . 5520 3 9 . 1 1 10 10 GLU N . . 0.133 0.009 . . . . . . . 5520 3 10 . 1 1 11 11 TYR N . . 0.176 0.012 . . . . . . . 5520 3 11 . 1 1 13 13 LYS N . . 0.204 0.014 . . . . . . . 5520 3 12 . 1 1 15 15 ALA N . . 0.137 0.013 . . . . . . . 5520 3 13 . 1 1 16 16 CYS N . . 0.207 0.014 . . . . . . . 5520 3 14 . 1 1 17 17 THR N . . 0.235 0.022 . . . . . . . 5520 3 15 . 1 1 18 18 LEU N . . 0.427 0.048 . . . . . . . 5520 3 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_15N_T2_chain_2_600_pH6 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 15N_T2_chain_2_600_pH6 _Heteronucl_T2_list.Entry_ID 5520 _Heteronucl_T2_list.ID 4 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $condition_1 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units s _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID . . 1 $Sample_1 . 5520 4 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 2 2 2 2 TYR N . . 0.207 0.056 . . . . . . . 5520 4 2 . 2 2 3 3 ARG N . . 0.247 0.017 . . . . . . . 5520 4 3 . 2 2 5 5 LEU N . . 0.213 0.014 . . . . . . . 5520 4 4 . 2 2 6 6 CYS N . . 0.205 0.014 . . . . . . . 5520 4 5 . 2 2 7 7 GLY N . . 0.165 0.011 . . . . . . . 5520 4 6 . 2 2 8 8 SER N . . 0.199 0.013 . . . . . . . 5520 4 7 . 2 2 9 9 ASP N . . 0.162 0.011 . . . . . . . 5520 4 8 . 2 2 10 10 ASN N . . 0.180 0.012 . . . . . . . 5520 4 9 . 2 2 11 11 LYS N . . 0.209 0.014 . . . . . . . 5520 4 10 . 2 2 12 12 THR N . . 0.213 0.014 . . . . . . . 5520 4 11 . 2 2 13 13 TYR N . . 0.194 0.013 . . . . . . . 5520 4 12 . 2 2 14 14 GLY N . . 0.185 0.013 . . . . . . . 5520 4 13 . 2 2 15 15 ASN N . . 0.196 0.013 . . . . . . . 5520 4 14 . 2 2 16 16 LYS N . . 0.175 0.012 . . . . . . . 5520 4 15 . 2 2 17 17 CYS N . . 0.172 0.012 . . . . . . . 5520 4 16 . 2 2 18 18 ASN N . . 0.179 0.012 . . . . . . . 5520 4 17 . 2 2 19 19 PHE N . . 0.189 0.013 . . . . . . . 5520 4 18 . 2 2 20 20 CYS N . . 0.186 0.013 . . . . . . . 5520 4 19 . 2 2 21 21 ASN N . . 0.179 0.012 . . . . . . . 5520 4 20 . 2 2 22 22 ALA N . . 0.169 0.011 . . . . . . . 5520 4 21 . 2 2 23 23 VAL N . . 0.195 0.013 . . . . . . . 5520 4 22 . 2 2 24 24 VAL N . . 0.183 0.012 . . . . . . . 5520 4 23 . 2 2 25 25 GLU N . . 0.158 0.011 . . . . . . . 5520 4 24 . 2 2 26 26 SER N . . 0.189 0.013 . . . . . . . 5520 4 25 . 2 2 27 27 ASN N . . 0.177 0.012 . . . . . . . 5520 4 26 . 2 2 28 28 GLY N . . 0.190 0.013 . . . . . . . 5520 4 27 . 2 2 29 29 THR N . . 0.218 0.015 . . . . . . . 5520 4 28 . 2 2 30 30 LEU N . . 0.203 0.014 . . . . . . . 5520 4 29 . 2 2 31 31 THR N . . 0.200 0.014 . . . . . . . 5520 4 30 . 2 2 32 32 LEU N . . 0.212 0.014 . . . . . . . 5520 4 31 . 2 2 33 33 SER N . . 0.178 0.012 . . . . . . . 5520 4 32 . 2 2 34 34 HIS N . . 0.138 0.009 . . . . . . . 5520 4 33 . 2 2 35 35 PHE N . . 0.184 0.012 . . . . . . . 5520 4 34 . 2 2 36 36 GLY N . . 0.176 0.012 . . . . . . . 5520 4 35 . 2 2 37 37 LYS N . . 0.228 0.015 . . . . . . . 5520 4 36 . 2 2 38 38 CYS N . . 0.199 0.013 . . . . . . . 5520 4 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_15N_T2_chain_1_600_pH39 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 15N_T2_chain_1_600_pH39 _Heteronucl_T2_list.Entry_ID 5520 _Heteronucl_T2_list.ID 5 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $condition_1 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units s _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID . . 1 $Sample_1 . 5520 5 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 2 2 ALA N . . 0.826 0.057 . . . . . . . 5520 5 2 . 1 1 3 3 ALA N . . 0.763 0.053 . . . . . . . 5520 5 3 . 1 1 4 4 VAL N . . 0.571 0.040 . . . . . . . 5520 5 4 . 1 1 5 5 SER N . . 0.346 0.024 . . . . . . . 5520 5 5 . 1 1 6 6 VAL N . . 0.259 0.018 . . . . . . . 5520 5 6 . 1 1 7 7 ASP N . . 0.238 0.016 . . . . . . . 5520 5 7 . 1 1 8 8 CYS N . . 0.208 0.014 . . . . . . . 5520 5 8 . 1 1 9 9 SER N . . 0.122 0.008 . . . . . . . 5520 5 9 . 1 1 10 10 GLU N . . 0.192 0.013 . . . . . . . 5520 5 10 . 1 1 11 11 TYR N . . 0.188 0.013 . . . . . . . 5520 5 11 . 1 1 13 13 LYS N . . 0.211 0.014 . . . . . . . 5520 5 12 . 1 1 15 15 ALA N . . 0.122 0.008 . . . . . . . 5520 5 13 . 1 1 16 16 CYS N . . 0.248 0.017 . . . . . . . 5520 5 14 . 1 1 17 17 THR N . . 0.310 0.021 . . . . . . . 5520 5 15 . 1 1 18 18 LEU N . . 0.497 0.034 . . . . . . . 5520 5 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_15N_T2_chain_2_600_pH39 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 15N_T2_chain_2_600_pH39 _Heteronucl_T2_list.Entry_ID 5520 _Heteronucl_T2_list.ID 6 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $condition_1 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units s _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID . . 1 $Sample_1 . 5520 6 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 2 2 2 2 TYR N . . 0.301 0.030 . . . . . . . 5520 6 2 . 2 2 3 3 ARG N . . 0.245 0.012 . . . . . . . 5520 6 3 . 2 2 5 5 LEU N . . 0.172 0.012 . . . . . . . 5520 6 4 . 2 2 6 6 CYS N . . 0.189 0.013 . . . . . . . 5520 6 5 . 2 2 7 7 GLY N . . 0.208 0.014 . . . . . . . 5520 6 6 . 2 2 8 8 SER N . . 0.185 0.013 . . . . . . . 5520 6 7 . 2 2 9 9 ASP N . . 0.174 0.012 . . . . . . . 5520 6 8 . 2 2 10 10 ASN N . . 0.183 0.012 . . . . . . . 5520 6 9 . 2 2 11 11 LYS N . . 0.186 0.013 . . . . . . . 5520 6 10 . 2 2 12 12 THR N . . 0.205 0.014 . . . . . . . 5520 6 11 . 2 2 13 13 TYR N . . 0.194 0.013 . . . . . . . 5520 6 12 . 2 2 14 14 GLY N . . 0.209 0.014 . . . . . . . 5520 6 13 . 2 2 15 15 ASN N . . 0.195 0.013 . . . . . . . 5520 6 14 . 2 2 16 16 LYS N . . 0.189 0.013 . . . . . . . 5520 6 15 . 2 2 17 17 CYS N . . 0.219 0.015 . . . . . . . 5520 6 16 . 2 2 18 18 ASN N . . 0.205 0.014 . . . . . . . 5520 6 17 . 2 2 19 19 PHE N . . 0.174 0.012 . . . . . . . 5520 6 18 . 2 2 20 20 CYS N . . 0.207 0.014 . . . . . . . 5520 6 19 . 2 2 21 21 ASN N . . 0.181 0.012 . . . . . . . 5520 6 20 . 2 2 22 22 ALA N . . 0.174 0.012 . . . . . . . 5520 6 21 . 2 2 23 23 VAL N . . 0.193 0.013 . . . . . . . 5520 6 22 . 2 2 24 24 VAL N . . 0.157 0.011 . . . . . . . 5520 6 23 . 2 2 25 25 GLU N . . 0.189 0.013 . . . . . . . 5520 6 24 . 2 2 26 26 SER N . . 0.201 0.014 . . . . . . . 5520 6 25 . 2 2 27 27 ASN N . . 0.202 0.014 . . . . . . . 5520 6 26 . 2 2 28 28 GLY N . . 0.217 0.015 . . . . . . . 5520 6 27 . 2 2 29 29 THR N . . 0.211 0.014 . . . . . . . 5520 6 28 . 2 2 30 30 LEU N . . 0.199 0.013 . . . . . . . 5520 6 29 . 2 2 31 31 THR N . . 0.200 0.014 . . . . . . . 5520 6 30 . 2 2 32 32 LEU N . . 0.202 0.014 . . . . . . . 5520 6 31 . 2 2 33 33 SER N . . 0.178 0.012 . . . . . . . 5520 6 32 . 2 2 34 34 HIS N . . 0.207 0.014 . . . . . . . 5520 6 33 . 2 2 35 35 PHE N . . 0.211 0.014 . . . . . . . 5520 6 34 . 2 2 36 36 GLY N . . 0.191 0.013 . . . . . . . 5520 6 35 . 2 2 37 37 LYS N . . 0.235 0.016 . . . . . . . 5520 6 36 . 2 2 38 38 CYS N . . 0.188 0.013 . . . . . . . 5520 6 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_15N_T2_chain_1_750_pH6 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 15N_T2_chain_1_750_pH6 _Heteronucl_T2_list.Entry_ID 5520 _Heteronucl_T2_list.ID 7 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $condition_1 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 750 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units s _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID . . 1 $Sample_1 . 5520 7 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 2 2 ALA N . . 0.185 0.012 . . . . . . . 5520 7 2 . 1 1 3 3 ALA N . . 0.246 0.017 . . . . . . . 5520 7 3 . 1 1 4 4 VAL N . . 0.303 0.030 . . . . . . . 5520 7 4 . 1 1 5 5 SER N . . 0.189 0.013 . . . . . . . 5520 7 5 . 1 1 6 6 VAL N . . 0.184 0.019 . . . . . . . 5520 7 6 . 1 1 7 7 ASP N . . 0.114 0.010 . . . . . . . 5520 7 7 . 1 1 8 8 CYS N . . 0.125 0.008 . . . . . . . 5520 7 8 . 1 1 9 9 SER N . . 0.123 0.008 . . . . . . . 5520 7 9 . 1 1 10 10 GLU N . . 0.092 0.006 . . . . . . . 5520 7 10 . 1 1 11 11 TYR N . . 0.137 0.009 . . . . . . . 5520 7 11 . 1 1 13 13 LYS N . . 0.169 0.011 . . . . . . . 5520 7 12 . 1 1 15 15 ALA N . . 0.099 0.011 . . . . . . . 5520 7 13 . 1 1 16 16 CYS N . . 0.130 0.009 . . . . . . . 5520 7 14 . 1 1 17 17 THR N . . 0.142 0.014 . . . . . . . 5520 7 15 . 1 1 18 18 LEU N . . 0.308 0.031 . . . . . . . 5520 7 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_15N_T2_chain_2_750_pH6 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 15N_T2_chain_2_750_pH6 _Heteronucl_T2_list.Entry_ID 5520 _Heteronucl_T2_list.ID 8 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $condition_1 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 750 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units s _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID . . 1 $Sample_1 . 5520 8 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 2 2 2 2 TYR N . . 0.152 0.017 . . . . . . . 5520 8 2 . 2 2 3 3 ARG N . . 0.163 0.011 . . . . . . . 5520 8 3 . 2 2 5 5 LEU N . . 0.162 0.011 . . . . . . . 5520 8 4 . 2 2 6 6 CYS N . . 0.168 0.011 . . . . . . . 5520 8 5 . 2 2 7 7 GLY N . . 0.148 0.010 . . . . . . . 5520 8 6 . 2 2 8 8 SER N . . 0.143 0.010 . . . . . . . 5520 8 7 . 2 2 9 9 ASP N . . 0.149 0.010 . . . . . . . 5520 8 8 . 2 2 10 10 ASN N . . 0.164 0.011 . . . . . . . 5520 8 9 . 2 2 11 11 LYS N . . 0.156 0.010 . . . . . . . 5520 8 10 . 2 2 12 12 THR N . . 0.164 0.011 . . . . . . . 5520 8 11 . 2 2 13 13 TYR N . . 0.146 0.010 . . . . . . . 5520 8 12 . 2 2 14 14 GLY N . . 0.141 0.009 . . . . . . . 5520 8 13 . 2 2 15 15 ASN N . . 0.158 0.011 . . . . . . . 5520 8 14 . 2 2 16 16 LYS N . . 0.119 0.008 . . . . . . . 5520 8 15 . 2 2 17 17 CYS N . . 0.147 0.010 . . . . . . . 5520 8 16 . 2 2 18 18 ASN N . . 0.150 0.010 . . . . . . . 5520 8 17 . 2 2 19 19 PHE N . . 0.149 0.010 . . . . . . . 5520 8 18 . 2 2 20 20 CYS N . . 0.154 0.010 . . . . . . . 5520 8 19 . 2 2 21 21 ASN N . . 0.153 0.010 . . . . . . . 5520 8 20 . 2 2 22 22 ALA N . . 0.166 0.011 . . . . . . . 5520 8 21 . 2 2 23 23 VAL N . . 0.162 0.011 . . . . . . . 5520 8 22 . 2 2 24 24 VAL N . . 0.144 0.010 . . . . . . . 5520 8 23 . 2 2 25 25 GLU N . . 0.168 0.011 . . . . . . . 5520 8 24 . 2 2 26 26 SER N . . 0.160 0.011 . . . . . . . 5520 8 25 . 2 2 27 27 ASN N . . 0.141 0.009 . . . . . . . 5520 8 26 . 2 2 28 28 GLY N . . 0.165 0.011 . . . . . . . 5520 8 27 . 2 2 29 29 THR N . . 0.157 0.011 . . . . . . . 5520 8 28 . 2 2 30 30 LEU N . . 0.16 0.011 . . . . . . . 5520 8 29 . 2 2 31 31 THR N . . 0.146 0.010 . . . . . . . 5520 8 30 . 2 2 32 32 LEU N . . 0.167 0.011 . . . . . . . 5520 8 31 . 2 2 33 33 SER N . . 0.154 0.010 . . . . . . . 5520 8 32 . 2 2 34 34 HIS N . . 0.143 0.010 . . . . . . . 5520 8 33 . 2 2 35 35 PHE N . . 0.129 0.009 . . . . . . . 5520 8 34 . 2 2 36 36 GLY N . . 0.158 0.011 . . . . . . . 5520 8 35 . 2 2 37 37 LYS N . . 0.182 0.012 . . . . . . . 5520 8 36 . 2 2 38 38 CYS N . . 0.151 0.010 . . . . . . . 5520 8 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_15N_T2_chain_1_750_pH39 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 15N_T2_chain_1_750_pH39 _Heteronucl_T2_list.Entry_ID 5520 _Heteronucl_T2_list.ID 9 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $condition_1 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 750 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units s _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID . . 1 $Sample_1 . 5520 9 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 2 2 ALA N . . 0.578 0.094 . . . . . . . 5520 9 2 . 1 1 3 3 ALA N . . 0.729 0.112 . . . . . . . 5520 9 3 . 1 1 4 4 VAL N . . 0.436 0.030 . . . . . . . 5520 9 4 . 1 1 5 5 SER N . . 0.300 0.021 . . . . . . . 5520 9 5 . 1 1 6 6 VAL N . . 0.215 0.015 . . . . . . . 5520 9 6 . 1 1 7 7 ASP N . . 0.163 0.019 . . . . . . . 5520 9 7 . 1 1 8 8 CYS N . . 0.150 0.010 . . . . . . . 5520 9 8 . 1 1 9 9 SER N . . 0.092 0.006 . . . . . . . 5520 9 9 . 1 1 10 10 GLU N . . 0.161 0.011 . . . . . . . 5520 9 10 . 1 1 11 11 TYR N . . 0.131 0.009 . . . . . . . 5520 9 11 . 1 1 13 13 LYS N . . 0.152 0.012 . . . . . . . 5520 9 12 . 1 1 15 15 ALA N . . 0.076 0.005 . . . . . . . 5520 9 13 . 1 1 16 16 CYS N . . 0.213 0.014 . . . . . . . 5520 9 14 . 1 1 17 17 THR N . . 0.248 0.017 . . . . . . . 5520 9 15 . 1 1 18 18 LEU N . . 0.343 0.024 . . . . . . . 5520 9 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_15N_T2_chain_2_750_pH39 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 15N_T2_chain_2_750_pH39 _Heteronucl_T2_list.Entry_ID 5520 _Heteronucl_T2_list.ID 10 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $condition_1 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 750 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units s _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID . . 1 $Sample_1 . 5520 10 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 2 2 2 2 TYR N . . 0.200 0.018 . . . . . . . 5520 10 2 . 2 2 3 3 ARG N . . 0.224 0.011 . . . . . . . 5520 10 3 . 2 2 5 5 LEU N . . 0.116 0.009 . . . . . . . 5520 10 4 . 2 2 6 6 CYS N . . 0.147 0.011 . . . . . . . 5520 10 5 . 2 2 7 7 GLY N . . 0.140 0.009 . . . . . . . 5520 10 6 . 2 2 8 8 SER N . . 0.135 0.009 . . . . . . . 5520 10 7 . 2 2 9 9 ASP N . . 0.146 0.010 . . . . . . . 5520 10 8 . 2 2 10 10 ASN N . . 0.153 0.010 . . . . . . . 5520 10 9 . 2 2 11 11 LYS N . . 0.146 0.010 . . . . . . . 5520 10 10 . 2 2 12 12 THR N . . 0.157 0.011 . . . . . . . 5520 10 11 . 2 2 13 13 TYR N . . 0.154 0.010 . . . . . . . 5520 10 12 . 2 2 14 14 GLY N . . 0.184 0.012 . . . . . . . 5520 10 13 . 2 2 15 15 ASN N . . 0.183 0.012 . . . . . . . 5520 10 14 . 2 2 16 16 LYS N . . 0.172 0.012 . . . . . . . 5520 10 15 . 2 2 17 17 CYS N . . 0.151 0.015 . . . . . . . 5520 10 16 . 2 2 18 18 ASN N . . 0.16 0.011 . . . . . . . 5520 10 17 . 2 2 19 19 PHE N . . 0.145 0.010 . . . . . . . 5520 10 18 . 2 2 20 20 CYS N . . 0.162 0.011 . . . . . . . 5520 10 19 . 2 2 21 21 ASN N . . 0.169 0.011 . . . . . . . 5520 10 20 . 2 2 22 22 ALA N . . 0.174 0.012 . . . . . . . 5520 10 21 . 2 2 23 23 VAL N . . 0.167 0.011 . . . . . . . 5520 10 22 . 2 2 24 24 VAL N . . 0.123 0.008 . . . . . . . 5520 10 23 . 2 2 25 25 GLU N . . 0.152 0.012 . . . . . . . 5520 10 24 . 2 2 26 26 SER N . . 0.156 0.010 . . . . . . . 5520 10 25 . 2 2 27 27 ASN N . . 0.151 0.010 . . . . . . . 5520 10 26 . 2 2 28 28 GLY N . . 0.166 0.011 . . . . . . . 5520 10 27 . 2 2 29 29 THR N . . 0.139 0.009 . . . . . . . 5520 10 28 . 2 2 30 30 LEU N . . 0.156 0.010 . . . . . . . 5520 10 29 . 2 2 31 31 THR N . . 0.141 0.009 . . . . . . . 5520 10 30 . 2 2 32 32 LEU N . . 0.171 0.011 . . . . . . . 5520 10 31 . 2 2 33 33 SER N . . 0.152 0.017 . . . . . . . 5520 10 32 . 2 2 34 34 HIS N . . 0.151 0.010 . . . . . . . 5520 10 33 . 2 2 35 35 PHE N . . 0.168 0.011 . . . . . . . 5520 10 34 . 2 2 36 36 GLY N . . 0.159 0.011 . . . . . . . 5520 10 35 . 2 2 37 37 LYS N . . 0.178 0.012 . . . . . . . 5520 10 36 . 2 2 38 38 CYS N . . 0.149 0.010 . . . . . . . 5520 10 stop_ save_