######################################## # Heteronuclear T1 relaxation values # ######################################## save_283_600_free_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 283_600_free_t1 _Heteronucl_T1_list.Entry_ID 5995 _Heteronucl_T1_list.ID 1 _Heteronucl_T1_list.Sample_condition_list_ID 1 _Heteronucl_T1_list.Sample_condition_list_label $283K _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5995 1 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 4 4 SER N N 15 964.99 51.89 . . . . . 5995 1 2 . 1 1 6 6 THR N N 15 845.49 67.59 . . . . . 5995 1 3 . 1 1 7 7 GLY N N 15 864.40 30.67 . . . . . 5995 1 4 . 1 1 11 11 ASN N N 15 902.21 27.08 . . . . . 5995 1 5 . 1 1 12 12 VAL N N 15 1050.7 20.74 . . . . . 5995 1 6 . 1 1 13 13 GLU N N 15 1055.8 33.58 . . . . . 5995 1 7 . 1 1 15 15 ILE N N 15 1042.9 21.53 . . . . . 5995 1 8 . 1 1 16 16 ASN N N 15 1042.9 32.33 . . . . . 5995 1 9 . 1 1 17 17 GLY N N 15 1038.9 38.36 . . . . . 5995 1 10 . 1 1 22 22 ILE N N 15 958.37 39.94 . . . . . 5995 1 11 . 1 1 23 23 ILE N N 15 1045.2 31.69 . . . . . 5995 1 12 . 1 1 26 26 SER N N 15 1046.9 27.14 . . . . . 5995 1 13 . 1 1 28 28 LYS N N 15 993.97 19.01 . . . . . 5995 1 14 . 1 1 30 30 GLU N N 15 891.38 32.23 . . . . . 5995 1 15 . 1 1 31 31 LYS N N 15 963.94 34.67 . . . . . 5995 1 16 . 1 1 32 32 ILE N N 15 956.89 42.70 . . . . . 5995 1 17 . 1 1 33 33 GLU N N 15 970.01 37.11 . . . . . 5995 1 18 . 1 1 36 36 GLY N N 15 913.30 19.86 . . . . . 5995 1 19 . 1 1 37 37 ASN N N 15 830.80 60.93 . . . . . 5995 1 20 . 1 1 39 39 ARG N N 15 977.28 33.34 . . . . . 5995 1 21 . 1 1 48 48 LEU N N 15 990.00 23.89 . . . . . 5995 1 22 . 1 1 51 51 SER N N 15 897.50 32.90 . . . . . 5995 1 23 . 1 1 54 54 LEU N N 15 1008.0 26.44 . . . . . 5995 1 24 . 1 1 61 61 ASP N N 15 889.94 73.26 . . . . . 5995 1 25 . 1 1 71 71 ALA N N 15 1013.9 34.91 . . . . . 5995 1 26 . 1 1 74 74 THR N N 15 907.06 24.94 . . . . . 5995 1 27 . 1 1 79 79 GLU N N 15 917.54 21.81 . . . . . 5995 1 28 . 1 1 81 81 SER N N 15 984.77 41.84 . . . . . 5995 1 29 . 1 1 84 84 TYR N N 15 1003.3 43.82 . . . . . 5995 1 30 . 1 1 85 85 ASP N N 15 889.19 71.06 . . . . . 5995 1 31 . 1 1 86 86 GLY N N 15 1002.2 24.37 . . . . . 5995 1 32 . 1 1 89 89 THR N N 15 964.39 24.66 . . . . . 5995 1 33 . 1 1 91 91 THR N N 15 1133.9 40.17 . . . . . 5995 1 34 . 1 1 92 92 ILE N N 15 1017.8 56.77 . . . . . 5995 1 35 . 1 1 94 94 LYS N N 15 1065.3 34.91 . . . . . 5995 1 36 . 1 1 96 96 ASP N N 15 1070.4 45.70 . . . . . 5995 1 37 . 1 1 97 97 TYR N N 15 1029.5 15.84 . . . . . 5995 1 38 . 1 1 100 100 PHE N N 15 1105.0 34.08 . . . . . 5995 1 39 . 1 1 101 101 LEU N N 15 1083.0 27.43 . . . . . 5995 1 40 . 1 1 103 103 ALA N N 15 1086.8 35.75 . . . . . 5995 1 41 . 1 1 105 105 LEU N N 15 1041.4 50.46 . . . . . 5995 1 42 . 1 1 107 107 ASN N N 15 954.94 31.14 . . . . . 5995 1 43 . 1 1 111 111 GLY N N 15 906.94 65.49 . . . . . 5995 1 44 . 1 1 115 115 GLN N N 15 1026.6 29.61 . . . . . 5995 1 45 . 1 1 116 116 LEU N N 15 1049.2 39.63 . . . . . 5995 1 46 . 1 1 117 117 MET N N 15 1091.5 54.07 . . . . . 5995 1 47 . 1 1 118 118 GLY N N 15 1044.4 35.00 . . . . . 5995 1 48 . 1 1 119 119 LEU N N 15 1033.4 25.50 . . . . . 5995 1 49 . 1 1 120 120 TYR N N 15 1076.6 19.75 . . . . . 5995 1 50 . 1 1 121 121 GLY N N 15 979.98 30.71 . . . . . 5995 1 51 . 1 1 125 125 ASP N N 15 1004.9 40.68 . . . . . 5995 1 52 . 1 1 126 126 LEU N N 15 1025.4 38.84 . . . . . 5995 1 53 . 1 1 127 127 SER N N 15 959.45 49.60 . . . . . 5995 1 54 . 1 1 130 130 ILE N N 15 937.98 29.23 . . . . . 5995 1 55 . 1 1 131 131 LYS N N 15 975.99 19.84 . . . . . 5995 1 56 . 1 1 133 133 ARG N N 15 983.31 19.71 . . . . . 5995 1 57 . 1 1 135 135 ALA N N 15 993.81 26.11 . . . . . 5995 1 58 . 1 1 136 136 GLN N N 15 1014.2 27.05 . . . . . 5995 1 59 . 1 1 137 137 LEU N N 15 1014.7 35.86 . . . . . 5995 1 60 . 1 1 138 138 CYS N N 15 1018.6 34.36 . . . . . 5995 1 61 . 1 1 140 140 LYS N N 15 1023.1 30.36 . . . . . 5995 1 62 . 1 1 141 141 HIS N N 15 1066.4 31.35 . . . . . 5995 1 63 . 1 1 142 142 GLY N N 15 997.53 31.09 . . . . . 5995 1 64 . 1 1 144 144 LEU N N 15 1048.1 28.83 . . . . . 5995 1 65 . 1 1 148 148 ILE N N 15 988.60 32.98 . . . . . 5995 1 66 . 1 1 151 151 LEU N N 15 1016.3 64.05 . . . . . 5995 1 67 . 1 1 160 160 ALA N N 15 678.35 22.73 . . . . . 5995 1 68 . 1 1 162 162 GLU N N 15 697.88 18.80 . . . . . 5995 1 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_288_600_free_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 288_600_free_t1 _Heteronucl_T1_list.Entry_ID 5995 _Heteronucl_T1_list.ID 2 _Heteronucl_T1_list.Sample_condition_list_ID 2 _Heteronucl_T1_list.Sample_condition_list_label $288K _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5995 2 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 ALA N N 15 901.18 29.93 . . . . . 5995 2 2 . 1 1 4 4 SER N N 15 913.94 41.60 . . . . . 5995 2 3 . 1 1 6 6 THR N N 15 785.19 42.00 . . . . . 5995 2 4 . 1 1 10 10 PHE N N 15 919.79 44.36 . . . . . 5995 2 5 . 1 1 11 11 ASN N N 15 864.18 35.43 . . . . . 5995 2 6 . 1 1 12 12 VAL N N 15 1008.8 26.53 . . . . . 5995 2 7 . 1 1 13 13 GLU N N 15 947.04 17.93 . . . . . 5995 2 8 . 1 1 16 16 ASN N N 15 954.55 24.81 . . . . . 5995 2 9 . 1 1 17 17 GLY N N 15 953.75 24.66 . . . . . 5995 2 10 . 1 1 22 22 ILE N N 15 954.51 26.37 . . . . . 5995 2 11 . 1 1 23 23 ILE N N 15 988.22 16.85 . . . . . 5995 2 12 . 1 1 24 24 LEU N N 15 967.27 23.88 . . . . . 5995 2 13 . 1 1 26 26 SER N N 15 965.41 18.26 . . . . . 5995 2 14 . 1 1 28 28 LYS N N 15 974.58 27.90 . . . . . 5995 2 15 . 1 1 30 30 GLU N N 15 850.14 20.94 . . . . . 5995 2 16 . 1 1 31 31 LYS N N 15 917.18 14.87 . . . . . 5995 2 17 . 1 1 32 32 ILE N N 15 882.21 19.86 . . . . . 5995 2 18 . 1 1 33 33 GLU N N 15 917.53 26.08 . . . . . 5995 2 19 . 1 1 35 35 ASN N N 15 968.10 20.76 . . . . . 5995 2 20 . 1 1 36 36 GLY N N 15 828.53 22.59 . . . . . 5995 2 21 . 1 1 37 37 ASN N N 15 833.18 29.01 . . . . . 5995 2 22 . 1 1 38 38 PHE N N 15 871.92 19.55 . . . . . 5995 2 23 . 1 1 39 39 ARG N N 15 942.60 32.82 . . . . . 5995 2 24 . 1 1 40 40 LEU N N 15 988.58 23.27 . . . . . 5995 2 25 . 1 1 46 46 HIS N N 15 949.54 16.66 . . . . . 5995 2 26 . 1 1 48 48 LEU N N 15 944.17 26.64 . . . . . 5995 2 27 . 1 1 51 51 SER N N 15 842.34 23.36 . . . . . 5995 2 28 . 1 1 53 53 VAL N N 15 1010.4 12.11 . . . . . 5995 2 29 . 1 1 54 54 LEU N N 15 959.97 21.16 . . . . . 5995 2 30 . 1 1 55 55 LYS N N 15 973.34 16.53 . . . . . 5995 2 31 . 1 1 58 58 THR N N 15 898.92 21.00 . . . . . 5995 2 32 . 1 1 60 60 ARG N N 15 904.37 25.17 . . . . . 5995 2 33 . 1 1 61 61 ASP N N 15 861.89 45.18 . . . . . 5995 2 34 . 1 1 62 62 GLU N N 15 860.53 22.63 . . . . . 5995 2 35 . 1 1 64 64 CYS N N 15 927.25 51.04 . . . . . 5995 2 36 . 1 1 66 66 GLU N N 15 872.46 29.34 . . . . . 5995 2 37 . 1 1 68 68 SER N N 15 945.88 21.66 . . . . . 5995 2 38 . 1 1 69 69 MET N N 15 974.01 20.53 . . . . . 5995 2 39 . 1 1 71 71 ALA N N 15 937.92 26.34 . . . . . 5995 2 40 . 1 1 72 72 ASP N N 15 1037.7 36.37 . . . . . 5995 2 41 . 1 1 74 74 THR N N 15 877.45 23.71 . . . . . 5995 2 42 . 1 1 75 75 GLU N N 15 872.33 54.33 . . . . . 5995 2 43 . 1 1 76 76 LYS N N 15 956.42 27.34 . . . . . 5995 2 44 . 1 1 77 77 ALA N N 15 939.33 101.4 . . . . . 5995 2 45 . 1 1 79 79 GLU N N 15 870.85 25.37 . . . . . 5995 2 46 . 1 1 80 80 TYR N N 15 910.63 14.33 . . . . . 5995 2 47 . 1 1 81 81 SER N N 15 950.37 25.3 . . . . . 5995 2 48 . 1 1 82 82 VAL N N 15 916.86 29.25 . . . . . 5995 2 49 . 1 1 84 84 TYR N N 15 980.29 18.51 . . . . . 5995 2 50 . 1 1 85 85 ASP N N 15 852.94 39.54 . . . . . 5995 2 51 . 1 1 86 86 GLY N N 15 921.54 20.87 . . . . . 5995 2 52 . 1 1 88 88 ASN N N 15 977.53 18.92 . . . . . 5995 2 53 . 1 1 89 89 THR N N 15 923.25 25.18 . . . . . 5995 2 54 . 1 1 91 91 THR N N 15 891.44 41.66 . . . . . 5995 2 55 . 1 1 92 92 ILE N N 15 937.66 32.53 . . . . . 5995 2 56 . 1 1 94 94 LYS N N 15 970.63 30.49 . . . . . 5995 2 57 . 1 1 95 95 THR N N 15 979.12 31.15 . . . . . 5995 2 58 . 1 1 96 96 ASP N N 15 947.53 20.55 . . . . . 5995 2 59 . 1 1 97 97 TYR N N 15 928.12 45.36 . . . . . 5995 2 60 . 1 1 99 99 ASN N N 15 857.21 53.45 . . . . . 5995 2 61 . 1 1 100 100 PHE N N 15 1014.1 12.83 . . . . . 5995 2 62 . 1 1 101 101 LEU N N 15 991.55 21.21 . . . . . 5995 2 63 . 1 1 102 102 MET N N 15 982.05 22.61 . . . . . 5995 2 64 . 1 1 103 103 ALA N N 15 996.75 17.16 . . . . . 5995 2 65 . 1 1 105 105 LEU N N 15 944.55 23.79 . . . . . 5995 2 66 . 1 1 107 107 ASN N N 15 911.95 26.21 . . . . . 5995 2 67 . 1 1 108 108 GLU N N 15 929.41 20.59 . . . . . 5995 2 68 . 1 1 111 111 GLY N N 15 822.93 46.74 . . . . . 5995 2 69 . 1 1 113 113 THR N N 15 883.08 27.35 . . . . . 5995 2 70 . 1 1 115 115 GLN N N 15 924.15 23.10 . . . . . 5995 2 71 . 1 1 116 116 LEU N N 15 965.39 24.42 . . . . . 5995 2 72 . 1 1 117 117 MET N N 15 979.25 30.60 . . . . . 5995 2 73 . 1 1 118 118 GLY N N 15 987.33 15.52 . . . . . 5995 2 74 . 1 1 119 119 LEU N N 15 981.57 16.25 . . . . . 5995 2 75 . 1 1 120 120 TYR N N 15 987.07 13.57 . . . . . 5995 2 76 . 1 1 121 121 GLY N N 15 949.24 15.50 . . . . . 5995 2 77 . 1 1 125 125 ASP N N 15 908.58 19.28 . . . . . 5995 2 78 . 1 1 126 126 LEU N N 15 966.15 14.52 . . . . . 5995 2 79 . 1 1 127 127 SER N N 15 904.95 31.29 . . . . . 5995 2 80 . 1 1 130 130 ILE N N 15 907.98 27.62 . . . . . 5995 2 81 . 1 1 131 131 LYS N N 15 893.79 23.19 . . . . . 5995 2 82 . 1 1 133 133 ARG N N 15 927.38 28.12 . . . . . 5995 2 83 . 1 1 135 135 ALA N N 15 901.67 24.20 . . . . . 5995 2 84 . 1 1 136 136 GLN N N 15 934.39 21.44 . . . . . 5995 2 85 . 1 1 137 137 LEU N N 15 936.71 23.43 . . . . . 5995 2 86 . 1 1 138 138 CYS N N 15 929.29 18.69 . . . . . 5995 2 87 . 1 1 140 140 LYS N N 15 947.99 25.22 . . . . . 5995 2 88 . 1 1 141 141 HIS N N 15 956.48 10.48 . . . . . 5995 2 89 . 1 1 142 142 GLY N N 15 939.07 22.06 . . . . . 5995 2 90 . 1 1 144 144 LEU N N 15 993.16 19.69 . . . . . 5995 2 91 . 1 1 145 145 ARG N N 15 959.39 20.79 . . . . . 5995 2 92 . 1 1 146 146 GLU N N 15 863.24 38.48 . . . . . 5995 2 93 . 1 1 148 148 ILE N N 15 939.94 22.82 . . . . . 5995 2 94 . 1 1 151 151 LEU N N 15 979.48 31.60 . . . . . 5995 2 95 . 1 1 155 155 ASN N N 15 961.72 22.88 . . . . . 5995 2 96 . 1 1 157 157 CYS N N 15 979.33 26.60 . . . . . 5995 2 97 . 1 1 158 158 LEU N N 15 970.03 15.26 . . . . . 5995 2 98 . 1 1 162 162 GLU N N 15 688.37 15.70 . . . . . 5995 2 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_298_600_free_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 298_600_free_t1 _Heteronucl_T1_list.Entry_ID 5995 _Heteronucl_T1_list.ID 3 _Heteronucl_T1_list.Sample_condition_list_ID 4 _Heteronucl_T1_list.Sample_condition_list_label $298K _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5995 3 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 ALA N N 15 736.03 13.27 . . . . . 5995 3 2 . 1 1 4 4 SER N N 15 674.35 41.11 . . . . . 5995 3 3 . 1 1 11 11 ASN N N 15 651.68 34.69 . . . . . 5995 3 4 . 1 1 12 12 VAL N N 15 759.17 22.32 . . . . . 5995 3 5 . 1 1 13 13 GLU N N 15 753.74 13.09 . . . . . 5995 3 6 . 1 1 16 16 ASN N N 15 756.46 7.279 . . . . . 5995 3 7 . 1 1 17 17 GLY N N 15 746.54 11.82 . . . . . 5995 3 8 . 1 1 18 18 GLU N N 15 798.67 35.61 . . . . . 5995 3 9 . 1 1 19 19 TRP N N 15 731.97 19.00 . . . . . 5995 3 10 . 1 1 20 20 HIS N N 15 720.22 12.10 . . . . . 5995 3 11 . 1 1 22 22 ILE N N 15 745.39 13.87 . . . . . 5995 3 12 . 1 1 23 23 ILE N N 15 772.34 9.415 . . . . . 5995 3 13 . 1 1 24 24 LEU N N 15 766.44 9.429 . . . . . 5995 3 14 . 1 1 26 26 SER N N 15 755.65 7.373 . . . . . 5995 3 15 . 1 1 27 27 ASP N N 15 734.82 14.62 . . . . . 5995 3 16 . 1 1 28 28 LYS N N 15 747.91 12.08 . . . . . 5995 3 17 . 1 1 30 30 GLU N N 15 620.98 25.04 . . . . . 5995 3 18 . 1 1 31 31 LYS N N 15 683.17 10.15 . . . . . 5995 3 19 . 1 1 32 32 ILE N N 15 706.68 11.31 . . . . . 5995 3 20 . 1 1 33 33 GLU N N 15 720.84 11.79 . . . . . 5995 3 21 . 1 1 36 36 GLY N N 15 648.01 19.03 . . . . . 5995 3 22 . 1 1 37 37 ASN N N 15 726.10 20.93 . . . . . 5995 3 23 . 1 1 38 38 PHE N N 15 696.68 15.81 . . . . . 5995 3 24 . 1 1 39 39 ARG N N 15 701.33 14.53 . . . . . 5995 3 25 . 1 1 40 40 LEU N N 15 760.03 18.49 . . . . . 5995 3 26 . 1 1 41 41 PHE N N 15 732.28 16.63 . . . . . 5995 3 27 . 1 1 48 48 LEU N N 15 751.53 16.45 . . . . . 5995 3 28 . 1 1 51 51 SER N N 15 627.33 20.09 . . . . . 5995 3 29 . 1 1 53 53 VAL N N 15 798.01 7.482 . . . . . 5995 3 30 . 1 1 54 54 LEU N N 15 772.15 13.66 . . . . . 5995 3 31 . 1 1 55 55 LYS N N 15 754.74 12.78 . . . . . 5995 3 32 . 1 1 57 57 HIS N N 15 735.43 17.22 . . . . . 5995 3 33 . 1 1 58 58 THR N N 15 769.52 23.73 . . . . . 5995 3 34 . 1 1 60 60 ARG N N 15 682.87 11.77 . . . . . 5995 3 35 . 1 1 62 62 GLU N N 15 669.51 22.49 . . . . . 5995 3 36 . 1 1 64 64 CYS N N 15 727.66 16.19 . . . . . 5995 3 37 . 1 1 66 66 GLU N N 15 678.88 32.27 . . . . . 5995 3 38 . 1 1 68 68 SER N N 15 682.53 28.74 . . . . . 5995 3 39 . 1 1 69 69 MET N N 15 787.15 10.93 . . . . . 5995 3 40 . 1 1 70 70 VAL N N 15 681.70 38.08 . . . . . 5995 3 41 . 1 1 71 71 ALA N N 15 756.05 20.04 . . . . . 5995 3 42 . 1 1 72 72 ASP N N 15 768.90 10.90 . . . . . 5995 3 43 . 1 1 74 74 THR N N 15 649.59 22.00 . . . . . 5995 3 44 . 1 1 75 75 GLU N N 15 657.87 28.80 . . . . . 5995 3 45 . 1 1 76 76 LYS N N 15 721.45 15.28 . . . . . 5995 3 46 . 1 1 79 79 GLU N N 15 675.73 9.531 . . . . . 5995 3 47 . 1 1 81 81 SER N N 15 726.80 11.42 . . . . . 5995 3 48 . 1 1 82 82 VAL N N 15 719.82 20.37 . . . . . 5995 3 49 . 1 1 84 84 TYR N N 15 751.74 12.70 . . . . . 5995 3 50 . 1 1 85 85 ASP N N 15 696.72 23.24 . . . . . 5995 3 51 . 1 1 86 86 GLY N N 15 712.04 14.52 . . . . . 5995 3 52 . 1 1 88 88 ASN N N 15 784.50 9.011 . . . . . 5995 3 53 . 1 1 89 89 THR N N 15 722.28 18.64 . . . . . 5995 3 54 . 1 1 91 91 THR N N 15 743.76 36.05 . . . . . 5995 3 55 . 1 1 92 92 ILE N N 15 743.85 27.33 . . . . . 5995 3 56 . 1 1 94 94 LYS N N 15 775.56 12.71 . . . . . 5995 3 57 . 1 1 96 96 ASP N N 15 751.25 16.00 . . . . . 5995 3 58 . 1 1 97 97 TYR N N 15 723.57 17.35 . . . . . 5995 3 59 . 1 1 100 100 PHE N N 15 827.86 21.74 . . . . . 5995 3 60 . 1 1 101 101 LEU N N 15 784.81 17.52 . . . . . 5995 3 61 . 1 1 103 103 ALA N N 15 793.94 29.08 . . . . . 5995 3 62 . 1 1 104 104 HIS N N 15 780.79 9.724 . . . . . 5995 3 63 . 1 1 105 105 LEU N N 15 752.35 17.82 . . . . . 5995 3 64 . 1 1 106 106 ILE N N 15 790.22 17.26 . . . . . 5995 3 65 . 1 1 107 107 ASN N N 15 731.97 16.15 . . . . . 5995 3 66 . 1 1 111 111 GLY N N 15 647.65 37.49 . . . . . 5995 3 67 . 1 1 113 113 THR N N 15 746.05 21.35 . . . . . 5995 3 68 . 1 1 114 114 PHE N N 15 743.98 9.151 . . . . . 5995 3 69 . 1 1 115 115 GLN N N 15 753.26 16.01 . . . . . 5995 3 70 . 1 1 116 116 LEU N N 15 768.75 12.98 . . . . . 5995 3 71 . 1 1 117 117 MET N N 15 795.66 16.78 . . . . . 5995 3 72 . 1 1 118 118 GLY N N 15 763.21 17.53 . . . . . 5995 3 73 . 1 1 119 119 LEU N N 15 771.38 11.51 . . . . . 5995 3 74 . 1 1 120 120 TYR N N 15 802.90 21.64 . . . . . 5995 3 75 . 1 1 121 121 GLY N N 15 756.73 16.37 . . . . . 5995 3 76 . 1 1 123 123 GLU N N 15 794.18 17.22 . . . . . 5995 3 77 . 1 1 125 125 ASP N N 15 717.87 18.22 . . . . . 5995 3 78 . 1 1 126 126 LEU N N 15 755.65 12.88 . . . . . 5995 3 79 . 1 1 127 127 SER N N 15 681.84 33.04 . . . . . 5995 3 80 . 1 1 128 128 SER N N 15 656.19 16.85 . . . . . 5995 3 81 . 1 1 129 129 ASP N N 15 828.27 8.724 . . . . . 5995 3 82 . 1 1 130 130 ILE N N 15 681.92 16.09 . . . . . 5995 3 83 . 1 1 131 131 LYS N N 15 713.62 15.03 . . . . . 5995 3 84 . 1 1 133 133 ARG N N 15 735.36 9.642 . . . . . 5995 3 85 . 1 1 134 134 PHE N N 15 719.19 12.33 . . . . . 5995 3 86 . 1 1 135 135 ALA N N 15 710.16 11.92 . . . . . 5995 3 87 . 1 1 136 136 GLN N N 15 751.75 9.767 . . . . . 5995 3 88 . 1 1 137 137 LEU N N 15 758.25 10.08 . . . . . 5995 3 89 . 1 1 138 138 CYS N N 15 735.38 8.301 . . . . . 5995 3 90 . 1 1 140 140 LYS N N 15 757.20 11.13 . . . . . 5995 3 91 . 1 1 141 141 HIS N N 15 793.54 9.562 . . . . . 5995 3 92 . 1 1 142 142 GLY N N 15 701.77 13.18 . . . . . 5995 3 93 . 1 1 143 143 ILE N N 15 684.93 20.87 . . . . . 5995 3 94 . 1 1 144 144 LEU N N 15 796.12 10.80 . . . . . 5995 3 95 . 1 1 145 145 ARG N N 15 713.77 19.30 . . . . . 5995 3 96 . 1 1 146 146 GLU N N 15 641.91 40.11 . . . . . 5995 3 97 . 1 1 148 148 ILE N N 15 751.66 11.91 . . . . . 5995 3 98 . 1 1 151 151 LEU N N 15 786.38 20.09 . . . . . 5995 3 99 . 1 1 158 158 LEU N N 15 741.72 16.73 . . . . . 5995 3 100 . 1 1 162 162 GLU N N 15 672.26 11.25 . . . . . 5995 3 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_303_600_free_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 303_600_free_t1 _Heteronucl_T1_list.Entry_ID 5995 _Heteronucl_T1_list.ID 4 _Heteronucl_T1_list.Sample_condition_list_ID 5 _Heteronucl_T1_list.Sample_condition_list_label $303K _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5995 4 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 ALA N N 15 693.16 15.60 . . . . . 5995 4 2 . 1 1 4 4 SER N N 15 626.41 41.09 . . . . . 5995 4 3 . 1 1 6 6 THR N N 15 572.46 33.45 . . . . . 5995 4 4 . 1 1 11 11 ASN N N 15 636.37 19.08 . . . . . 5995 4 5 . 1 1 12 12 VAL N N 15 734.34 5.511 . . . . . 5995 4 6 . 1 1 13 13 GLU N N 15 689.13 8.133 . . . . . 5995 4 7 . 1 1 16 16 ASN N N 15 708.41 8.800 . . . . . 5995 4 8 . 1 1 17 17 GLY N N 15 706.99 13.62 . . . . . 5995 4 9 . 1 1 19 19 TRP N N 15 696.41 8.728 . . . . . 5995 4 10 . 1 1 20 20 HIS N N 15 724.85 15.99 . . . . . 5995 4 11 . 1 1 21 21 THR N N 15 631.23 23.39 . . . . . 5995 4 12 . 1 1 22 22 ILE N N 15 693.06 4.859 . . . . . 5995 4 13 . 1 1 23 23 ILE N N 15 710.53 10.67 . . . . . 5995 4 14 . 1 1 24 24 LEU N N 15 704.78 8.992 . . . . . 5995 4 15 . 1 1 26 26 SER N N 15 701.72 12.22 . . . . . 5995 4 16 . 1 1 27 27 ASP N N 15 653.87 13.38 . . . . . 5995 4 17 . 1 1 28 28 LYS N N 15 760.60 11.51 . . . . . 5995 4 18 . 1 1 30 30 GLU N N 15 586.56 9.525 . . . . . 5995 4 19 . 1 1 31 31 LYS N N 15 650.87 6.777 . . . . . 5995 4 20 . 1 1 32 32 ILE N N 15 639.04 5.560 . . . . . 5995 4 21 . 1 1 33 33 GLU N N 15 650.32 10.64 . . . . . 5995 4 22 . 1 1 35 35 ASN N N 15 707.41 14.79 . . . . . 5995 4 23 . 1 1 36 36 GLY N N 15 628.19 3.859 . . . . . 5995 4 24 . 1 1 38 38 PHE N N 15 631.38 6.642 . . . . . 5995 4 25 . 1 1 39 39 ARG N N 15 664.39 7.511 . . . . . 5995 4 26 . 1 1 40 40 LEU N N 15 710.90 9.957 . . . . . 5995 4 27 . 1 1 42 42 LEU N N 15 701.77 8.900 . . . . . 5995 4 28 . 1 1 46 46 HIS N N 15 711.37 7.089 . . . . . 5995 4 29 . 1 1 48 48 LEU N N 15 693.20 10.85 . . . . . 5995 4 30 . 1 1 51 51 SER N N 15 608.07 6.784 . . . . . 5995 4 31 . 1 1 52 52 LEU N N 15 701.95 12.98 . . . . . 5995 4 32 . 1 1 53 53 VAL N N 15 745.17 11.89 . . . . . 5995 4 33 . 1 1 54 54 LEU N N 15 717.70 5.001 . . . . . 5995 4 34 . 1 1 55 55 LYS N N 15 693.21 11.08 . . . . . 5995 4 35 . 1 1 57 57 HIS N N 15 662.92 12.74 . . . . . 5995 4 36 . 1 1 58 58 THR N N 15 665.44 6.330 . . . . . 5995 4 37 . 1 1 60 60 ARG N N 15 720.52 4.747 . . . . . 5995 4 38 . 1 1 62 62 GLU N N 15 642.69 7.138 . . . . . 5995 4 39 . 1 1 64 64 CYS N N 15 678.44 11.10 . . . . . 5995 4 40 . 1 1 67 67 LEU N N 15 674.75 8.381 . . . . . 5995 4 41 . 1 1 68 68 SER N N 15 673.68 14.94 . . . . . 5995 4 42 . 1 1 69 69 MET N N 15 732.87 8.362 . . . . . 5995 4 43 . 1 1 70 70 VAL N N 15 651.95 25.00 . . . . . 5995 4 44 . 1 1 71 71 ALA N N 15 702.74 13.04 . . . . . 5995 4 45 . 1 1 72 72 ASP N N 15 723.77 11.66 . . . . . 5995 4 46 . 1 1 74 74 THR N N 15 652.93 8.470 . . . . . 5995 4 47 . 1 1 76 76 LYS N N 15 702.56 7.116 . . . . . 5995 4 48 . 1 1 77 77 ALA N N 15 733.56 33.59 . . . . . 5995 4 49 . 1 1 79 79 GLU N N 15 625.58 7.597 . . . . . 5995 4 50 . 1 1 81 81 SER N N 15 704.73 9.472 . . . . . 5995 4 51 . 1 1 84 84 TYR N N 15 741.87 6.212 . . . . . 5995 4 52 . 1 1 86 86 GLY N N 15 683.81 4.781 . . . . . 5995 4 53 . 1 1 88 88 ASN N N 15 733.62 9.969 . . . . . 5995 4 54 . 1 1 89 89 THR N N 15 681.94 11.99 . . . . . 5995 4 55 . 1 1 92 92 ILE N N 15 707.91 7.377 . . . . . 5995 4 56 . 1 1 94 94 LYS N N 15 698.04 10.19 . . . . . 5995 4 57 . 1 1 95 95 THR N N 15 716.00 8.562 . . . . . 5995 4 58 . 1 1 96 96 ASP N N 15 716.21 10.51 . . . . . 5995 4 59 . 1 1 97 97 TYR N N 15 673.24 9.319 . . . . . 5995 4 60 . 1 1 98 98 ASP N N 15 771.47 16.05 . . . . . 5995 4 61 . 1 1 99 99 ASN N N 15 731.53 5.300 . . . . . 5995 4 62 . 1 1 101 101 LEU N N 15 723.75 8.378 . . . . . 5995 4 63 . 1 1 102 102 MET N N 15 736.05 12.52 . . . . . 5995 4 64 . 1 1 103 103 ALA N N 15 743.35 11.43 . . . . . 5995 4 65 . 1 1 104 104 HIS N N 15 715.56 6.722 . . . . . 5995 4 66 . 1 1 105 105 LEU N N 15 710.57 12.86 . . . . . 5995 4 67 . 1 1 106 106 ILE N N 15 750.07 14.37 . . . . . 5995 4 68 . 1 1 107 107 ASN N N 15 673.99 8.740 . . . . . 5995 4 69 . 1 1 108 108 GLU N N 15 700.36 12.57 . . . . . 5995 4 70 . 1 1 110 110 ASP N N 15 744.22 11.16 . . . . . 5995 4 71 . 1 1 111 111 GLY N N 15 624.45 25.17 . . . . . 5995 4 72 . 1 1 113 113 THR N N 15 660.39 13.24 . . . . . 5995 4 73 . 1 1 114 114 PHE N N 15 702.85 5.705 . . . . . 5995 4 74 . 1 1 115 115 GLN N N 15 687.02 13.84 . . . . . 5995 4 75 . 1 1 116 116 LEU N N 15 720.69 11.74 . . . . . 5995 4 76 . 1 1 117 117 MET N N 15 734.83 13.66 . . . . . 5995 4 77 . 1 1 118 118 GLY N N 15 733.56 5.058 . . . . . 5995 4 78 . 1 1 119 119 LEU N N 15 775.64 21.80 . . . . . 5995 4 79 . 1 1 120 120 TYR N N 15 735.00 14.50 . . . . . 5995 4 80 . 1 1 121 121 GLY N N 15 714.40 12.04 . . . . . 5995 4 81 . 1 1 123 123 GLU N N 15 729.45 6.006 . . . . . 5995 4 82 . 1 1 125 125 ASP N N 15 687.20 8.610 . . . . . 5995 4 83 . 1 1 126 126 LEU N N 15 717.66 10.81 . . . . . 5995 4 84 . 1 1 127 127 SER N N 15 657.59 19.01 . . . . . 5995 4 85 . 1 1 128 128 SER N N 15 620.60 9.998 . . . . . 5995 4 86 . 1 1 129 129 ASP N N 15 787.13 5.809 . . . . . 5995 4 87 . 1 1 130 130 ILE N N 15 651.85 6.650 . . . . . 5995 4 88 . 1 1 131 131 LYS N N 15 672.06 7.273 . . . . . 5995 4 89 . 1 1 133 133 ARG N N 15 696.57 3.732 . . . . . 5995 4 90 . 1 1 135 135 ALA N N 15 647.70 8.966 . . . . . 5995 4 91 . 1 1 136 136 GLN N N 15 677.39 9.179 . . . . . 5995 4 92 . 1 1 137 137 LEU N N 15 697.81 12.97 . . . . . 5995 4 93 . 1 1 138 138 CYS N N 15 669.76 8.708 . . . . . 5995 4 94 . 1 1 140 140 LYS N N 15 697.30 10.09 . . . . . 5995 4 95 . 1 1 141 141 HIS N N 15 714.96 13.68 . . . . . 5995 4 96 . 1 1 142 142 GLY N N 15 674.15 9.983 . . . . . 5995 4 97 . 1 1 143 143 ILE N N 15 708.38 5.978 . . . . . 5995 4 98 . 1 1 144 144 LEU N N 15 737.35 12.70 . . . . . 5995 4 99 . 1 1 145 145 ARG N N 15 702.88 8.019 . . . . . 5995 4 100 . 1 1 146 146 GLU N N 15 643.91 22.75 . . . . . 5995 4 101 . 1 1 148 148 ILE N N 15 688.03 8.541 . . . . . 5995 4 102 . 1 1 151 151 LEU N N 15 748.67 10.82 . . . . . 5995 4 103 . 1 1 152 152 SER N N 15 730.77 13.45 . . . . . 5995 4 104 . 1 1 153 153 ASN N N 15 618.03 12.30 . . . . . 5995 4 105 . 1 1 157 157 CYS N N 15 696.53 9.016 . . . . . 5995 4 106 . 1 1 158 158 LEU N N 15 704.14 16.25 . . . . . 5995 4 107 . 1 1 162 162 GLU N N 15 724.13 7.893 . . . . . 5995 4 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_308_600_free_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 308_600_free_t1 _Heteronucl_T1_list.Entry_ID 5995 _Heteronucl_T1_list.ID 5 _Heteronucl_T1_list.Sample_condition_list_ID 6 _Heteronucl_T1_list.Sample_condition_list_label $308K _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5995 5 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 4 4 SER N N 15 552.20 34.06 . . . . . 5995 5 2 . 1 1 13 13 GLU N N 15 631.74 2.738 . . . . . 5995 5 3 . 1 1 16 16 ASN N N 15 631.40 12.54 . . . . . 5995 5 4 . 1 1 17 17 GLY N N 15 636.25 5.679 . . . . . 5995 5 5 . 1 1 19 19 TRP N N 15 617.86 11.95 . . . . . 5995 5 6 . 1 1 22 22 ILE N N 15 620.38 15.04 . . . . . 5995 5 7 . 1 1 23 23 ILE N N 15 654.20 5.380 . . . . . 5995 5 8 . 1 1 26 26 SER N N 15 657.86 6.680 . . . . . 5995 5 9 . 1 1 30 30 GLU N N 15 531.74 24.25 . . . . . 5995 5 10 . 1 1 31 31 LYS N N 15 602.49 6.573 . . . . . 5995 5 11 . 1 1 32 32 ILE N N 15 604.25 4.094 . . . . . 5995 5 12 . 1 1 33 33 GLU N N 15 612.20 23.86 . . . . . 5995 5 13 . 1 1 36 36 GLY N N 15 562.89 8.659 . . . . . 5995 5 14 . 1 1 38 38 PHE N N 15 587.17 14.64 . . . . . 5995 5 15 . 1 1 39 39 ARG N N 15 594.73 13.39 . . . . . 5995 5 16 . 1 1 40 40 LEU N N 15 652.35 14.56 . . . . . 5995 5 17 . 1 1 48 48 LEU N N 15 647.13 4.022 . . . . . 5995 5 18 . 1 1 51 51 SER N N 15 539.86 17.36 . . . . . 5995 5 19 . 1 1 53 53 VAL N N 15 665.19 3.095 . . . . . 5995 5 20 . 1 1 54 54 LEU N N 15 637.25 14.75 . . . . . 5995 5 21 . 1 1 57 57 HIS N N 15 655.29 12.64 . . . . . 5995 5 22 . 1 1 60 60 ARG N N 15 576.43 22.80 . . . . . 5995 5 23 . 1 1 68 68 SER N N 15 567.41 32.79 . . . . . 5995 5 24 . 1 1 69 69 MET N N 15 663.33 21.72 . . . . . 5995 5 25 . 1 1 71 71 ALA N N 15 646.56 9.557 . . . . . 5995 5 26 . 1 1 74 74 THR N N 15 543.97 31.12 . . . . . 5995 5 27 . 1 1 79 79 GLU N N 15 552.79 13.52 . . . . . 5995 5 28 . 1 1 81 81 SER N N 15 606.03 7.765 . . . . . 5995 5 29 . 1 1 86 86 GLY N N 15 599.62 19.56 . . . . . 5995 5 30 . 1 1 89 89 THR N N 15 647.57 8.290 . . . . . 5995 5 31 . 1 1 92 92 ILE N N 15 632.77 10.86 . . . . . 5995 5 32 . 1 1 94 94 LYS N N 15 640.85 4.608 . . . . . 5995 5 33 . 1 1 96 96 ASP N N 15 642.56 5.491 . . . . . 5995 5 34 . 1 1 100 100 PHE N N 15 685.38 21.29 . . . . . 5995 5 35 . 1 1 101 101 LEU N N 15 664.76 8.433 . . . . . 5995 5 36 . 1 1 103 103 ALA N N 15 687.78 9.088 . . . . . 5995 5 37 . 1 1 105 105 LEU N N 15 645.20 12.88 . . . . . 5995 5 38 . 1 1 107 107 ASN N N 15 608.87 11.56 . . . . . 5995 5 39 . 1 1 111 111 GLY N N 15 567.71 41.93 . . . . . 5995 5 40 . 1 1 115 115 GLN N N 15 627.71 7.097 . . . . . 5995 5 41 . 1 1 116 116 LEU N N 15 646.29 6.840 . . . . . 5995 5 42 . 1 1 117 117 MET N N 15 668.43 8.982 . . . . . 5995 5 43 . 1 1 118 118 GLY N N 15 658.04 20.02 . . . . . 5995 5 44 . 1 1 120 120 TYR N N 15 658.24 11.38 . . . . . 5995 5 45 . 1 1 121 121 GLY N N 15 632.90 25.80 . . . . . 5995 5 46 . 1 1 123 123 GLU N N 15 538.07 35.47 . . . . . 5995 5 47 . 1 1 125 125 ASP N N 15 636.08 17.74 . . . . . 5995 5 48 . 1 1 126 126 LEU N N 15 644.99 20.80 . . . . . 5995 5 49 . 1 1 127 127 SER N N 15 593.21 34.71 . . . . . 5995 5 50 . 1 1 130 130 ILE N N 15 575.07 10.72 . . . . . 5995 5 51 . 1 1 133 133 ARG N N 15 629.27 17.04 . . . . . 5995 5 52 . 1 1 136 136 GLN N N 15 639.00 3.991 . . . . . 5995 5 53 . 1 1 137 137 LEU N N 15 641.37 6.181 . . . . . 5995 5 54 . 1 1 138 138 CYS N N 15 643.60 12.51 . . . . . 5995 5 55 . 1 1 140 140 LYS N N 15 634.60 7.735 . . . . . 5995 5 56 . 1 1 141 141 HIS N N 15 670.61 4.806 . . . . . 5995 5 57 . 1 1 142 142 GLY N N 15 565.94 21.62 . . . . . 5995 5 58 . 1 1 144 144 LEU N N 15 681.82 4.879 . . . . . 5995 5 59 . 1 1 145 145 ARG N N 15 596.62 17.93 . . . . . 5995 5 60 . 1 1 148 148 ILE N N 15 641.37 7.472 . . . . . 5995 5 61 . 1 1 151 151 LEU N N 15 651.38 18.40 . . . . . 5995 5 62 . 1 1 162 162 GLU N N 15 693.89 12.36 . . . . . 5995 5 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_291_500_free_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 291_500_free_t1 _Heteronucl_T1_list.Entry_ID 5995 _Heteronucl_T1_list.ID 6 _Heteronucl_T1_list.Sample_condition_list_ID 7 _Heteronucl_T1_list.Sample_condition_list_label $291K _Heteronucl_T1_list.Spectrometer_frequency_1H 500 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5995 6 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 4 4 SER N N 15 811.85 54.57 . . . . . 5995 6 2 . 1 1 6 6 THR N N 15 767.55 67.60 . . . . . 5995 6 3 . 1 1 7 7 GLY N N 15 821.77 56.27 . . . . . 5995 6 4 . 1 1 11 11 ASN N N 15 942.45 63.18 . . . . . 5995 6 5 . 1 1 12 12 VAL N N 15 831.62 25.49 . . . . . 5995 6 6 . 1 1 13 13 GLU N N 15 745.23 27.16 . . . . . 5995 6 7 . 1 1 15 15 ILE N N 15 729.62 28.18 . . . . . 5995 6 8 . 1 1 16 16 ASN N N 15 744.16 13.63 . . . . . 5995 6 9 . 1 1 17 17 GLY N N 15 711.84 41.38 . . . . . 5995 6 10 . 1 1 22 22 ILE N N 15 822.83 79.08 . . . . . 5995 6 11 . 1 1 23 23 ILE N N 15 723.82 38.98 . . . . . 5995 6 12 . 1 1 26 26 SER N N 15 738.63 8.208 . . . . . 5995 6 13 . 1 1 27 27 ASP N N 15 804.05 50.74 . . . . . 5995 6 14 . 1 1 30 30 GLU N N 15 712.60 14.09 . . . . . 5995 6 15 . 1 1 31 31 LYS N N 15 712.19 42.29 . . . . . 5995 6 16 . 1 1 32 32 ILE N N 15 704.44 22.03 . . . . . 5995 6 17 . 1 1 33 33 GLU N N 15 766.72 16.48 . . . . . 5995 6 18 . 1 1 36 36 GLY N N 15 805.59 38.74 . . . . . 5995 6 19 . 1 1 37 37 ASN N N 15 716.76 69.80 . . . . . 5995 6 20 . 1 1 39 39 ARG N N 15 755.61 25.32 . . . . . 5995 6 21 . 1 1 40 40 LEU N N 15 829.17 51.40 . . . . . 5995 6 22 . 1 1 47 47 VAL N N 15 739.21 13.56 . . . . . 5995 6 23 . 1 1 48 48 LEU N N 15 733.25 30.34 . . . . . 5995 6 24 . 1 1 51 51 SER N N 15 767.89 23.36 . . . . . 5995 6 25 . 1 1 53 53 VAL N N 15 772.55 11.47 . . . . . 5995 6 26 . 1 1 54 54 LEU N N 15 743.76 18.61 . . . . . 5995 6 27 . 1 1 55 55 LYS N N 15 762.62 23.86 . . . . . 5995 6 28 . 1 1 60 60 ARG N N 15 745.68 16.33 . . . . . 5995 6 29 . 1 1 64 64 CYS N N 15 869.85 116.1 . . . . . 5995 6 30 . 1 1 67 67 LEU N N 15 762.26 32.42 . . . . . 5995 6 31 . 1 1 68 68 SER N N 15 803.23 26.80 . . . . . 5995 6 32 . 1 1 69 69 MET N N 15 781.20 21.51 . . . . . 5995 6 33 . 1 1 71 71 ALA N N 15 734.25 26.22 . . . . . 5995 6 34 . 1 1 72 72 ASP N N 15 788.51 19.89 . . . . . 5995 6 35 . 1 1 74 74 THR N N 15 692.82 30.35 . . . . . 5995 6 36 . 1 1 76 76 LYS N N 15 827.63 24.59 . . . . . 5995 6 37 . 1 1 77 77 ALA N N 15 1149.5 218.1 . . . . . 5995 6 38 . 1 1 79 79 GLU N N 15 781.00 31.94 . . . . . 5995 6 39 . 1 1 80 80 TYR N N 15 752.85 65.51 . . . . . 5995 6 40 . 1 1 81 81 SER N N 15 714.54 20.43 . . . . . 5995 6 41 . 1 1 86 86 GLY N N 15 783.62 20.06 . . . . . 5995 6 42 . 1 1 88 88 ASN N N 15 759.11 17.56 . . . . . 5995 6 43 . 1 1 89 89 THR N N 15 712.96 28.72 . . . . . 5995 6 44 . 1 1 91 91 THR N N 15 630.74 93.85 . . . . . 5995 6 45 . 1 1 92 92 ILE N N 15 925.06 76.43 . . . . . 5995 6 46 . 1 1 94 94 LYS N N 15 765.60 23.15 . . . . . 5995 6 47 . 1 1 96 96 ASP N N 15 736.94 36.81 . . . . . 5995 6 48 . 1 1 97 97 TYR N N 15 711.25 25.78 . . . . . 5995 6 49 . 1 1 98 98 ASP N N 15 751.13 57.83 . . . . . 5995 6 50 . 1 1 100 100 PHE N N 15 804.66 31.37 . . . . . 5995 6 51 . 1 1 101 101 LEU N N 15 804.96 31.38 . . . . . 5995 6 52 . 1 1 102 102 MET N N 15 798.00 31.32 . . . . . 5995 6 53 . 1 1 103 103 ALA N N 15 701.67 30.53 . . . . . 5995 6 54 . 1 1 104 104 HIS N N 15 709.43 12.63 . . . . . 5995 6 55 . 1 1 105 105 LEU N N 15 704.09 50.48 . . . . . 5995 6 56 . 1 1 107 107 ASN N N 15 736.72 32.40 . . . . . 5995 6 57 . 1 1 108 108 GLU N N 15 735.05 24.54 . . . . . 5995 6 58 . 1 1 111 111 GLY N N 15 891.03 42.36 . . . . . 5995 6 59 . 1 1 113 113 THR N N 15 772.34 16.07 . . . . . 5995 6 60 . 1 1 115 115 GLN N N 15 778.00 12.14 . . . . . 5995 6 61 . 1 1 116 116 LEU N N 15 767.50 32.72 . . . . . 5995 6 62 . 1 1 117 117 MET N N 15 766.55 36.88 . . . . . 5995 6 63 . 1 1 118 118 GLY N N 15 761.97 19.09 . . . . . 5995 6 64 . 1 1 121 121 GLY N N 15 775.78 37.22 . . . . . 5995 6 65 . 1 1 123 123 GLU N N 15 723.26 47.33 . . . . . 5995 6 66 . 1 1 125 125 ASP N N 15 756.32 25.58 . . . . . 5995 6 67 . 1 1 126 126 LEU N N 15 823.30 28.05 . . . . . 5995 6 68 . 1 1 127 127 SER N N 15 760.24 28.41 . . . . . 5995 6 69 . 1 1 129 129 ASP N N 15 806.87 32.86 . . . . . 5995 6 70 . 1 1 130 130 ILE N N 15 779.06 22.47 . . . . . 5995 6 71 . 1 1 131 131 LYS N N 15 746.78 29.04 . . . . . 5995 6 72 . 1 1 133 133 ARG N N 15 721.75 16.69 . . . . . 5995 6 73 . 1 1 136 136 GLN N N 15 730.24 11.91 . . . . . 5995 6 74 . 1 1 137 137 LEU N N 15 737.33 15.03 . . . . . 5995 6 75 . 1 1 138 138 CYS N N 15 684.57 21.96 . . . . . 5995 6 76 . 1 1 140 140 LYS N N 15 725.02 13.25 . . . . . 5995 6 77 . 1 1 141 141 HIS N N 15 749.84 23.90 . . . . . 5995 6 78 . 1 1 142 142 GLY N N 15 725.01 16.32 . . . . . 5995 6 79 . 1 1 144 144 LEU N N 15 746.46 12.53 . . . . . 5995 6 80 . 1 1 145 145 ARG N N 15 733.20 15.75 . . . . . 5995 6 81 . 1 1 148 148 ILE N N 15 771.80 12.21 . . . . . 5995 6 82 . 1 1 151 151 LEU N N 15 802.69 47.95 . . . . . 5995 6 83 . 1 1 153 153 ASN N N 15 794.19 23.94 . . . . . 5995 6 84 . 1 1 158 158 LEU N N 15 745.11 36.55 . . . . . 5995 6 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_297_500_free_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 297_500_free_t1 _Heteronucl_T1_list.Entry_ID 5995 _Heteronucl_T1_list.ID 7 _Heteronucl_T1_list.Sample_condition_list_ID 8 _Heteronucl_T1_list.Sample_condition_list_label $297K _Heteronucl_T1_list.Spectrometer_frequency_1H 500 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5995 7 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 ALA N N 15 701.34 48.16 . . . . . 5995 7 2 . 1 1 4 4 SER N N 15 699.79 46.31 . . . . . 5995 7 3 . 1 1 6 6 THR N N 15 505.28 40.61 . . . . . 5995 7 4 . 1 1 7 7 GLY N N 15 714.30 30.04 . . . . . 5995 7 5 . 1 1 11 11 ASN N N 15 713.42 85.43 . . . . . 5995 7 6 . 1 1 12 12 VAL N N 15 678.17 11.23 . . . . . 5995 7 7 . 1 1 13 13 GLU N N 15 657.10 11.03 . . . . . 5995 7 8 . 1 1 15 15 ILE N N 15 654.09 10.60 . . . . . 5995 7 9 . 1 1 16 16 ASN N N 15 663.11 13.27 . . . . . 5995 7 10 . 1 1 17 17 GLY N N 15 620.52 25.73 . . . . . 5995 7 11 . 1 1 21 21 THR N N 15 709.89 126.8 . . . . . 5995 7 12 . 1 1 22 22 ILE N N 15 614.52 31.71 . . . . . 5995 7 13 . 1 1 23 23 ILE N N 15 703.28 16.45 . . . . . 5995 7 14 . 1 1 26 26 SER N N 15 653.68 29.57 . . . . . 5995 7 15 . 1 1 27 27 ASP N N 15 684.60 11.51 . . . . . 5995 7 16 . 1 1 30 30 GLU N N 15 646.75 28.48 . . . . . 5995 7 17 . 1 1 31 31 LYS N N 15 639.58 20.43 . . . . . 5995 7 18 . 1 1 32 32 ILE N N 15 628.22 22.21 . . . . . 5995 7 19 . 1 1 33 33 GLU N N 15 683.55 14.05 . . . . . 5995 7 20 . 1 1 36 36 GLY N N 15 671.35 14.14 . . . . . 5995 7 21 . 1 1 37 37 ASN N N 15 673.92 13.40 . . . . . 5995 7 22 . 1 1 39 39 ARG N N 15 704.56 23.95 . . . . . 5995 7 23 . 1 1 40 40 LEU N N 15 730.90 38.04 . . . . . 5995 7 24 . 1 1 42 42 LEU N N 15 710.51 41.79 . . . . . 5995 7 25 . 1 1 47 47 VAL N N 15 652.07 18.00 . . . . . 5995 7 26 . 1 1 48 48 LEU N N 15 636.63 15.08 . . . . . 5995 7 27 . 1 1 51 51 SER N N 15 663.85 13.84 . . . . . 5995 7 28 . 1 1 52 52 LEU N N 15 702.15 27.67 . . . . . 5995 7 29 . 1 1 54 54 LEU N N 15 643.21 7.902 . . . . . 5995 7 30 . 1 1 57 57 HIS N N 15 707.31 40.80 . . . . . 5995 7 31 . 1 1 60 60 ARG N N 15 742.09 21.71 . . . . . 5995 7 32 . 1 1 64 64 CYS N N 15 651.68 15.93 . . . . . 5995 7 33 . 1 1 65 65 SER N N 15 671.60 14.72 . . . . . 5995 7 34 . 1 1 66 66 GLU N N 15 629.70 11.55 . . . . . 5995 7 35 . 1 1 67 67 LEU N N 15 671.21 22.49 . . . . . 5995 7 36 . 1 1 68 68 SER N N 15 702.22 16.11 . . . . . 5995 7 37 . 1 1 69 69 MET N N 15 659.47 10.76 . . . . . 5995 7 38 . 1 1 71 71 ALA N N 15 664.71 11.32 . . . . . 5995 7 39 . 1 1 72 72 ASP N N 15 686.23 27.01 . . . . . 5995 7 40 . 1 1 74 74 THR N N 15 700.49 20.05 . . . . . 5995 7 41 . 1 1 77 77 ALA N N 15 637.43 16.21 . . . . . 5995 7 42 . 1 1 79 79 GLU N N 15 679.25 21.81 . . . . . 5995 7 43 . 1 1 80 80 TYR N N 15 715.94 45.10 . . . . . 5995 7 44 . 1 1 81 81 SER N N 15 688.72 28.25 . . . . . 5995 7 45 . 1 1 86 86 GLY N N 15 658.17 18.83 . . . . . 5995 7 46 . 1 1 88 88 ASN N N 15 663.09 12.48 . . . . . 5995 7 47 . 1 1 89 89 THR N N 15 683.73 26.26 . . . . . 5995 7 48 . 1 1 91 91 THR N N 15 627.62 63.43 . . . . . 5995 7 49 . 1 1 92 92 ILE N N 15 702.46 59.55 . . . . . 5995 7 50 . 1 1 94 94 LYS N N 15 662.17 28.33 . . . . . 5995 7 51 . 1 1 95 95 THR N N 15 704.84 47.93 . . . . . 5995 7 52 . 1 1 96 96 ASP N N 15 648.59 21.70 . . . . . 5995 7 53 . 1 1 97 97 TYR N N 15 648.01 21.22 . . . . . 5995 7 54 . 1 1 100 100 PHE N N 15 668.51 34.68 . . . . . 5995 7 55 . 1 1 101 101 LEU N N 15 675.79 22.13 . . . . . 5995 7 56 . 1 1 102 102 MET N N 15 698.46 7.334 . . . . . 5995 7 57 . 1 1 103 103 ALA N N 15 640.72 35.23 . . . . . 5995 7 58 . 1 1 104 104 HIS N N 15 659.31 15.05 . . . . . 5995 7 59 . 1 1 105 105 LEU N N 15 617.96 27.45 . . . . . 5995 7 60 . 1 1 107 107 ASN N N 15 665.56 14.38 . . . . . 5995 7 61 . 1 1 108 108 GLU N N 15 679.22 40.87 . . . . . 5995 7 62 . 1 1 111 111 GLY N N 15 769.13 48.54 . . . . . 5995 7 63 . 1 1 113 113 THR N N 15 628.13 23.55 . . . . . 5995 7 64 . 1 1 115 115 GLN N N 15 639.30 16.20 . . . . . 5995 7 65 . 1 1 116 116 LEU N N 15 651.76 14.97 . . . . . 5995 7 66 . 1 1 117 117 MET N N 15 658.37 19.65 . . . . . 5995 7 67 . 1 1 118 118 GLY N N 15 674.46 21.46 . . . . . 5995 7 68 . 1 1 121 121 GLY N N 15 644.63 18.13 . . . . . 5995 7 69 . 1 1 123 123 GLU N N 15 691.78 29.06 . . . . . 5995 7 70 . 1 1 125 125 ASP N N 15 696.51 12.58 . . . . . 5995 7 71 . 1 1 126 126 LEU N N 15 730.02 18.06 . . . . . 5995 7 72 . 1 1 127 127 SER N N 15 721.90 29.37 . . . . . 5995 7 73 . 1 1 129 129 ASP N N 15 656.09 10.38 . . . . . 5995 7 74 . 1 1 130 130 ILE N N 15 668.40 11.23 . . . . . 5995 7 75 . 1 1 131 131 LYS N N 15 619.79 22.79 . . . . . 5995 7 76 . 1 1 133 133 ARG N N 15 633.45 19.29 . . . . . 5995 7 77 . 1 1 136 136 GLN N N 15 636.89 7.609 . . . . . 5995 7 78 . 1 1 137 137 LEU N N 15 630.09 12.33 . . . . . 5995 7 79 . 1 1 138 138 CYS N N 15 614.82 11.43 . . . . . 5995 7 80 . 1 1 140 140 LYS N N 15 637.57 4.869 . . . . . 5995 7 81 . 1 1 141 141 HIS N N 15 677.46 16.16 . . . . . 5995 7 82 . 1 1 142 142 GLY N N 15 637.73 15.04 . . . . . 5995 7 83 . 1 1 144 144 LEU N N 15 667.92 10.42 . . . . . 5995 7 84 . 1 1 145 145 ARG N N 15 651.78 11.77 . . . . . 5995 7 85 . 1 1 148 148 ILE N N 15 640.75 11.56 . . . . . 5995 7 86 . 1 1 151 151 LEU N N 15 676.15 25.90 . . . . . 5995 7 87 . 1 1 152 152 SER N N 15 644.90 9.480 . . . . . 5995 7 88 . 1 1 153 153 ASN N N 15 661.92 20.04 . . . . . 5995 7 89 . 1 1 155 155 ASN N N 15 643.03 16.10 . . . . . 5995 7 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_302_500_free_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 302_500_free_t1 _Heteronucl_T1_list.Entry_ID 5995 _Heteronucl_T1_list.ID 8 _Heteronucl_T1_list.Sample_condition_list_ID 9 _Heteronucl_T1_list.Sample_condition_list_label $302K _Heteronucl_T1_list.Spectrometer_frequency_1H 500 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5995 8 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 ALA N N 15 606.66 38.51 . . . . . 5995 8 2 . 1 1 4 4 SER N N 15 676.35 59.52 . . . . . 5995 8 3 . 1 1 11 11 ASN N N 15 635.67 53.59 . . . . . 5995 8 4 . 1 1 12 12 VAL N N 15 573.52 18.40 . . . . . 5995 8 5 . 1 1 13 13 GLU N N 15 555.92 17.81 . . . . . 5995 8 6 . 1 1 16 16 ASN N N 15 571.02 10.76 . . . . . 5995 8 7 . 1 1 17 17 GLY N N 15 546.61 24.99 . . . . . 5995 8 8 . 1 1 19 19 TRP N N 15 610.35 16.67 . . . . . 5995 8 9 . 1 1 20 20 HIS N N 15 576.19 24.00 . . . . . 5995 8 10 . 1 1 21 21 THR N N 15 632.84 79.69 . . . . . 5995 8 11 . 1 1 22 22 ILE N N 15 572.39 26.95 . . . . . 5995 8 12 . 1 1 23 23 ILE N N 15 583.98 12.17 . . . . . 5995 8 13 . 1 1 26 26 SER N N 15 548.14 21.40 . . . . . 5995 8 14 . 1 1 27 27 ASP N N 15 615.39 5.014 . . . . . 5995 8 15 . 1 1 30 30 GLU N N 15 555.69 17.25 . . . . . 5995 8 16 . 1 1 31 31 LYS N N 15 534.41 16.46 . . . . . 5995 8 17 . 1 1 32 32 ILE N N 15 564.66 14.46 . . . . . 5995 8 18 . 1 1 33 33 GLU N N 15 579.61 12.38 . . . . . 5995 8 19 . 1 1 35 35 ASN N N 15 602.21 42.13 . . . . . 5995 8 20 . 1 1 36 36 GLY N N 15 572.15 13.72 . . . . . 5995 8 21 . 1 1 37 37 ASN N N 15 549.25 16.81 . . . . . 5995 8 22 . 1 1 39 39 ARG N N 15 600.14 21.73 . . . . . 5995 8 23 . 1 1 40 40 LEU N N 15 650.55 31.26 . . . . . 5995 8 24 . 1 1 41 41 PHE N N 15 632.12 54.40 . . . . . 5995 8 25 . 1 1 42 42 LEU N N 15 614.53 45.01 . . . . . 5995 8 26 . 1 1 48 48 LEU N N 15 557.55 8.453 . . . . . 5995 8 27 . 1 1 51 51 SER N N 15 592.96 13.20 . . . . . 5995 8 28 . 1 1 52 52 LEU N N 15 631.31 19.81 . . . . . 5995 8 29 . 1 1 54 54 LEU N N 15 577.83 13.35 . . . . . 5995 8 30 . 1 1 57 57 HIS N N 15 638.77 12.53 . . . . . 5995 8 31 . 1 1 58 58 THR N N 15 597.50 10.32 . . . . . 5995 8 32 . 1 1 60 60 ARG N N 15 577.59 19.30 . . . . . 5995 8 33 . 1 1 64 64 CYS N N 15 554.77 18.69 . . . . . 5995 8 34 . 1 1 65 65 SER N N 15 581.93 34.05 . . . . . 5995 8 35 . 1 1 66 66 GLU N N 15 554.96 21.31 . . . . . 5995 8 36 . 1 1 68 68 SER N N 15 631.03 34.58 . . . . . 5995 8 37 . 1 1 69 69 MET N N 15 620.06 8.210 . . . . . 5995 8 38 . 1 1 70 70 VAL N N 15 533.04 14.36 . . . . . 5995 8 39 . 1 1 71 71 ALA N N 15 537.02 26.70 . . . . . 5995 8 40 . 1 1 72 72 ASP N N 15 459.50 61.78 . . . . . 5995 8 41 . 1 1 74 74 THR N N 15 574.95 27.19 . . . . . 5995 8 42 . 1 1 76 76 LYS N N 15 619.86 12.38 . . . . . 5995 8 43 . 1 1 77 77 ALA N N 15 576.38 9.525 . . . . . 5995 8 44 . 1 1 79 79 GLU N N 15 576.27 18.86 . . . . . 5995 8 45 . 1 1 81 81 SER N N 15 549.86 22.53 . . . . . 5995 8 46 . 1 1 86 86 GLY N N 15 579.59 18.92 . . . . . 5995 8 47 . 1 1 88 88 ASN N N 15 591.05 3.924 . . . . . 5995 8 48 . 1 1 89 89 THR N N 15 593.22 13.58 . . . . . 5995 8 49 . 1 1 92 92 ILE N N 15 725.26 56.74 . . . . . 5995 8 50 . 1 1 94 94 LYS N N 15 570.47 15.22 . . . . . 5995 8 51 . 1 1 96 96 ASP N N 15 549.52 16.19 . . . . . 5995 8 52 . 1 1 97 97 TYR N N 15 535.26 18.80 . . . . . 5995 8 53 . 1 1 99 99 ASN N N 15 545.78 20.55 . . . . . 5995 8 54 . 1 1 100 100 PHE N N 15 586.02 13.53 . . . . . 5995 8 55 . 1 1 101 101 LEU N N 15 592.79 15.56 . . . . . 5995 8 56 . 1 1 102 102 MET N N 15 590.68 23.99 . . . . . 5995 8 57 . 1 1 103 103 ALA N N 15 531.04 21.81 . . . . . 5995 8 58 . 1 1 104 104 HIS N N 15 529.05 11.74 . . . . . 5995 8 59 . 1 1 105 105 LEU N N 15 569.66 18.82 . . . . . 5995 8 60 . 1 1 106 106 ILE N N 15 574.93 16.49 . . . . . 5995 8 61 . 1 1 107 107 ASN N N 15 538.01 18.56 . . . . . 5995 8 62 . 1 1 111 111 GLY N N 15 653.63 61.36 . . . . . 5995 8 63 . 1 1 113 113 THR N N 15 580.02 22.49 . . . . . 5995 8 64 . 1 1 115 115 GLN N N 15 556.98 8.826 . . . . . 5995 8 65 . 1 1 116 116 LEU N N 15 569.42 17.56 . . . . . 5995 8 66 . 1 1 117 117 MET N N 15 566.03 16.99 . . . . . 5995 8 67 . 1 1 118 118 GLY N N 15 567.12 11.22 . . . . . 5995 8 68 . 1 1 120 120 TYR N N 15 577.95 18.49 . . . . . 5995 8 69 . 1 1 121 121 GLY N N 15 581.25 13.07 . . . . . 5995 8 70 . 1 1 123 123 GLU N N 15 635.58 17.87 . . . . . 5995 8 71 . 1 1 125 125 ASP N N 15 603.42 5.533 . . . . . 5995 8 72 . 1 1 126 126 LEU N N 15 646.28 11.05 . . . . . 5995 8 73 . 1 1 127 127 SER N N 15 648.04 46.42 . . . . . 5995 8 74 . 1 1 128 128 SER N N 15 614.96 16.07 . . . . . 5995 8 75 . 1 1 129 129 ASP N N 15 567.66 4.495 . . . . . 5995 8 76 . 1 1 130 130 ILE N N 15 558.89 15.65 . . . . . 5995 8 77 . 1 1 131 131 LYS N N 15 560.12 26.28 . . . . . 5995 8 78 . 1 1 133 133 ARG N N 15 580.34 14.45 . . . . . 5995 8 79 . 1 1 136 136 GLN N N 15 547.55 10.55 . . . . . 5995 8 80 . 1 1 137 137 LEU N N 15 558.47 10.16 . . . . . 5995 8 81 . 1 1 138 138 CYS N N 15 566.91 8.943 . . . . . 5995 8 82 . 1 1 140 140 LYS N N 15 551.99 7.600 . . . . . 5995 8 83 . 1 1 141 141 HIS N N 15 588.38 8.594 . . . . . 5995 8 84 . 1 1 142 142 GLY N N 15 568.44 6.729 . . . . . 5995 8 85 . 1 1 143 143 ILE N N 15 685.55 40.55 . . . . . 5995 8 86 . 1 1 144 144 LEU N N 15 597.81 18.97 . . . . . 5995 8 87 . 1 1 145 145 ARG N N 15 587.37 12.71 . . . . . 5995 8 88 . 1 1 148 148 ILE N N 15 551.23 10.02 . . . . . 5995 8 89 . 1 1 151 151 LEU N N 15 608.44 20.65 . . . . . 5995 8 90 . 1 1 153 153 ASN N N 15 594.95 24.68 . . . . . 5995 8 91 . 1 1 157 157 CYS N N 15 549.95 19.70 . . . . . 5995 8 stop_ save_