######################################## # Heteronuclear T2 relaxation values # ######################################## save_283_600_free_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 283_600_free_t2 _Heteronucl_T2_list.Entry_ID 5995 _Heteronucl_T2_list.ID 1 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $283K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5995 1 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 4 4 SER N N 15 57.28 3.30 . . . . . . . 5995 1 2 . 1 1 6 6 THR N N 15 53.50 2.67 . . . . . . . 5995 1 3 . 1 1 7 7 GLY N N 15 53.45 2.29 . . . . . . . 5995 1 4 . 1 1 11 11 ASN N N 15 54.60 7.99 . . . . . . . 5995 1 5 . 1 1 12 12 VAL N N 15 59.21 4.10 . . . . . . . 5995 1 6 . 1 1 13 13 GLU N N 15 53.82 2.29 . . . . . . . 5995 1 7 . 1 1 15 15 ILE N N 15 59.13 3.25 . . . . . . . 5995 1 8 . 1 1 16 16 ASN N N 15 51.90 2.18 . . . . . . . 5995 1 9 . 1 1 17 17 GLY N N 15 52.33 3.60 . . . . . . . 5995 1 10 . 1 1 22 22 ILE N N 15 47.62 4.97 . . . . . . . 5995 1 11 . 1 1 23 23 ILE N N 15 53.86 3.25 . . . . . . . 5995 1 12 . 1 1 26 26 SER N N 15 59.63 5.26 . . . . . . . 5995 1 13 . 1 1 28 28 LYS N N 15 58.33 4.27 . . . . . . . 5995 1 14 . 1 1 30 30 GLU N N 15 54.78 1.57 . . . . . . . 5995 1 15 . 1 1 31 31 LYS N N 15 52.30 4.02 . . . . . . . 5995 1 16 . 1 1 32 32 ILE N N 15 52.68 1.48 . . . . . . . 5995 1 17 . 1 1 33 33 GLU N N 15 54.65 4.76 . . . . . . . 5995 1 18 . 1 1 36 36 GLY N N 15 56.15 3.52 . . . . . . . 5995 1 19 . 1 1 37 37 ASN N N 15 45.66 2.92 . . . . . . . 5995 1 20 . 1 1 39 39 ARG N N 15 50.03 3.46 . . . . . . . 5995 1 21 . 1 1 48 48 LEU N N 15 58.46 3.30 . . . . . . . 5995 1 22 . 1 1 51 51 SER N N 15 62.90 3.57 . . . . . . . 5995 1 23 . 1 1 54 54 LEU N N 15 63.52 4.88 . . . . . . . 5995 1 24 . 1 1 61 61 ASP N N 15 49.55 5.04 . . . . . . . 5995 1 25 . 1 1 71 71 ALA N N 15 60.24 3.88 . . . . . . . 5995 1 26 . 1 1 74 74 THR N N 15 63.21 3.02 . . . . . . . 5995 1 27 . 1 1 79 79 GLU N N 15 53.24 2.30 . . . . . . . 5995 1 28 . 1 1 81 81 SER N N 15 55.61 3.33 . . . . . . . 5995 1 29 . 1 1 84 84 TYR N N 15 59.79 3.91 . . . . . . . 5995 1 30 . 1 1 85 85 ASP N N 15 55.66 6.36 . . . . . . . 5995 1 31 . 1 1 86 86 GLY N N 15 54.72 3.35 . . . . . . . 5995 1 32 . 1 1 89 89 THR N N 15 49.17 2.42 . . . . . . . 5995 1 33 . 1 1 91 91 THR N N 15 44.38 4.14 . . . . . . . 5995 1 34 . 1 1 92 92 ILE N N 15 55.48 8.02 . . . . . . . 5995 1 35 . 1 1 94 94 LYS N N 15 49.70 2.28 . . . . . . . 5995 1 36 . 1 1 96 96 ASP N N 15 52.95 4.60 . . . . . . . 5995 1 37 . 1 1 97 97 TYR N N 15 55.78 3.20 . . . . . . . 5995 1 38 . 1 1 100 100 PHE N N 15 48.30 4.53 . . . . . . . 5995 1 39 . 1 1 101 101 LEU N N 15 50.04 0.46 . . . . . . . 5995 1 40 . 1 1 103 103 ALA N N 15 52.58 5.69 . . . . . . . 5995 1 41 . 1 1 105 105 LEU N N 15 53.03 3.37 . . . . . . . 5995 1 42 . 1 1 107 107 ASN N N 15 60.22 6.23 . . . . . . . 5995 1 43 . 1 1 111 111 GLY N N 15 53.34 3.38 . . . . . . . 5995 1 44 . 1 1 115 115 GLN N N 15 58.13 1.60 . . . . . . . 5995 1 45 . 1 1 116 116 LEU N N 15 48.16 6.07 . . . . . . . 5995 1 46 . 1 1 117 117 MET N N 15 49.98 3.30 . . . . . . . 5995 1 47 . 1 1 118 118 GLY N N 15 49.96 1.66 . . . . . . . 5995 1 48 . 1 1 119 119 LEU N N 15 50.46 3.45 . . . . . . . 5995 1 49 . 1 1 120 120 TYR N N 15 57.69 4.21 . . . . . . . 5995 1 50 . 1 1 121 121 GLY N N 15 55.93 5.93 . . . . . . . 5995 1 51 . 1 1 125 125 ASP N N 15 50.45 1.94 . . . . . . . 5995 1 52 . 1 1 126 126 LEU N N 15 54.95 2.63 . . . . . . . 5995 1 53 . 1 1 127 127 SER N N 15 57.45 3.89 . . . . . . . 5995 1 54 . 1 1 130 130 ILE N N 15 56.24 3.12 . . . . . . . 5995 1 55 . 1 1 131 131 LYS N N 15 53.97 2.19 . . . . . . . 5995 1 56 . 1 1 133 133 ARG N N 15 55.27 3.31 . . . . . . . 5995 1 57 . 1 1 135 135 ALA N N 15 56.38 2.31 . . . . . . . 5995 1 58 . 1 1 136 136 GLN N N 15 59.11 2.63 . . . . . . . 5995 1 59 . 1 1 137 137 LEU N N 15 54.44 3.29 . . . . . . . 5995 1 60 . 1 1 138 138 CYS N N 15 46.63 1.09 . . . . . . . 5995 1 61 . 1 1 140 140 LYS N N 15 54.90 3.90 . . . . . . . 5995 1 62 . 1 1 141 141 HIS N N 15 60.96 3.22 . . . . . . . 5995 1 63 . 1 1 142 142 GLY N N 15 55.38 2.05 . . . . . . . 5995 1 64 . 1 1 144 144 LEU N N 15 62.23 4.46 . . . . . . . 5995 1 65 . 1 1 148 148 ILE N N 15 58.20 3.05 . . . . . . . 5995 1 66 . 1 1 151 151 LEU N N 15 53.01 7.22 . . . . . . . 5995 1 67 . 1 1 160 160 ALA N N 15 95.94 7.32 . . . . . . . 5995 1 68 . 1 1 162 162 GLU N N 15 197.47 16.57 . . . . . . . 5995 1 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_288_600_free_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 288_600_free_t2 _Heteronucl_T2_list.Entry_ID 5995 _Heteronucl_T2_list.ID 2 _Heteronucl_T2_list.Sample_condition_list_ID 2 _Heteronucl_T2_list.Sample_condition_list_label $288K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5995 2 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ALA N N 15 66.08 4.67 . . . . . . . 5995 2 2 . 1 1 4 4 SER N N 15 73.39 3.93 . . . . . . . 5995 2 3 . 1 1 6 6 THR N N 15 61.84 3.71 . . . . . . . 5995 2 4 . 1 1 10 10 PHE N N 15 63.94 2.88 . . . . . . . 5995 2 5 . 1 1 11 11 ASN N N 15 58.87 2.99 . . . . . . . 5995 2 6 . 1 1 12 12 VAL N N 15 71.56 0.53 . . . . . . . 5995 2 7 . 1 1 13 13 GLU N N 15 61.22 5.83 . . . . . . . 5995 2 8 . 1 1 16 16 ASN N N 15 52.87 3.46 . . . . . . . 5995 2 9 . 1 1 17 17 GLY N N 15 66.70 1.43 . . . . . . . 5995 2 10 . 1 1 22 22 ILE N N 15 61.12 7.42 . . . . . . . 5995 2 11 . 1 1 23 23 ILE N N 15 71.59 10.62 . . . . . . . 5995 2 12 . 1 1 24 24 LEU N N 15 62.46 5.12 . . . . . . . 5995 2 13 . 1 1 26 26 SER N N 15 75.20 4.81 . . . . . . . 5995 2 14 . 1 1 28 28 LYS N N 15 64.48 2.55 . . . . . . . 5995 2 15 . 1 1 30 30 GLU N N 15 67.07 3.70 . . . . . . . 5995 2 16 . 1 1 31 31 LYS N N 15 57.78 5.67 . . . . . . . 5995 2 17 . 1 1 32 32 ILE N N 15 57.06 4.02 . . . . . . . 5995 2 18 . 1 1 33 33 GLU N N 15 66.75 3.78 . . . . . . . 5995 2 19 . 1 1 35 35 ASN N N 15 64.28 2.47 . . . . . . . 5995 2 20 . 1 1 36 36 GLY N N 15 63.74 2.76 . . . . . . . 5995 2 21 . 1 1 37 37 ASN N N 15 57.06 4.83 . . . . . . . 5995 2 22 . 1 1 38 38 PHE N N 15 60.02 1.73 . . . . . . . 5995 2 23 . 1 1 39 39 ARG N N 15 56.10 3.75 . . . . . . . 5995 2 24 . 1 1 40 40 LEU N N 15 50.26 4.72 . . . . . . . 5995 2 25 . 1 1 46 46 HIS N N 15 67.06 2.59 . . . . . . . 5995 2 26 . 1 1 48 48 LEU N N 15 69.63 5.53 . . . . . . . 5995 2 27 . 1 1 51 51 SER N N 15 69.12 3.09 . . . . . . . 5995 2 28 . 1 1 53 53 VAL N N 15 66.78 3.02 . . . . . . . 5995 2 29 . 1 1 54 54 LEU N N 15 74.51 0.41 . . . . . . . 5995 2 30 . 1 1 55 55 LYS N N 15 63.38 2.66 . . . . . . . 5995 2 31 . 1 1 58 58 THR N N 15 37.24 2.34 . . . . . . . 5995 2 32 . 1 1 60 60 ARG N N 15 63.37 2.49 . . . . . . . 5995 2 33 . 1 1 61 61 ASP N N 15 58.62 5.16 . . . . . . . 5995 2 34 . 1 1 62 62 GLU N N 15 24.18 4.72 . . . . . . . 5995 2 35 . 1 1 64 64 CYS N N 15 55.26 3.68 . . . . . . . 5995 2 36 . 1 1 66 66 GLU N N 15 48.51 2.84 . . . . . . . 5995 2 37 . 1 1 68 68 SER N N 15 65.66 5.05 . . . . . . . 5995 2 38 . 1 1 69 69 MET N N 15 63.62 2.76 . . . . . . . 5995 2 39 . 1 1 71 71 ALA N N 15 68.50 2.54 . . . . . . . 5995 2 40 . 1 1 72 72 ASP N N 15 71.91 6.51 . . . . . . . 5995 2 41 . 1 1 74 74 THR N N 15 73.37 5.72 . . . . . . . 5995 2 42 . 1 1 75 75 GLU N N 15 74.48 3.68 . . . . . . . 5995 2 43 . 1 1 76 76 LYS N N 15 63.09 5.00 . . . . . . . 5995 2 44 . 1 1 77 77 ALA N N 15 63.62 5.40 . . . . . . . 5995 2 45 . 1 1 79 79 GLU N N 15 60.17 3.08 . . . . . . . 5995 2 46 . 1 1 80 80 TYR N N 15 62.49 3.02 . . . . . . . 5995 2 47 . 1 1 81 81 SER N N 15 66.07 2.80 . . . . . . . 5995 2 48 . 1 1 82 82 VAL N N 15 56.62 10.61 . . . . . . . 5995 2 49 . 1 1 84 84 TYR N N 15 70.71 4.76 . . . . . . . 5995 2 50 . 1 1 85 85 ASP N N 15 63.62 2.07 . . . . . . . 5995 2 51 . 1 1 86 86 GLY N N 15 66.54 5.45 . . . . . . . 5995 2 52 . 1 1 88 88 ASN N N 15 68.06 5.18 . . . . . . . 5995 2 53 . 1 1 89 89 THR N N 15 68.16 3.82 . . . . . . . 5995 2 54 . 1 1 91 91 THR N N 15 40.40 3.45 . . . . . . . 5995 2 55 . 1 1 92 92 ILE N N 15 60.34 2.85 . . . . . . . 5995 2 56 . 1 1 94 94 LYS N N 15 56.09 2.99 . . . . . . . 5995 2 57 . 1 1 95 95 THR N N 15 50.92 3.66 . . . . . . . 5995 2 58 . 1 1 96 96 ASP N N 15 64.26 3.55 . . . . . . . 5995 2 59 . 1 1 97 97 TYR N N 15 63.55 5.20 . . . . . . . 5995 2 60 . 1 1 99 99 ASN N N 15 83.59 4.58 . . . . . . . 5995 2 61 . 1 1 100 100 PHE N N 15 62.95 9.41 . . . . . . . 5995 2 62 . 1 1 101 101 LEU N N 15 57.55 4.38 . . . . . . . 5995 2 63 . 1 1 102 102 MET N N 15 65.06 4.17 . . . . . . . 5995 2 64 . 1 1 103 103 ALA N N 15 64.40 3.99 . . . . . . . 5995 2 65 . 1 1 105 105 LEU N N 15 53.72 1.69 . . . . . . . 5995 2 66 . 1 1 107 107 ASN N N 15 66.77 2.55 . . . . . . . 5995 2 67 . 1 1 108 108 GLU N N 15 74.67 2.27 . . . . . . . 5995 2 68 . 1 1 111 111 GLY N N 15 66.10 5.24 . . . . . . . 5995 2 69 . 1 1 113 113 THR N N 15 73.22 4.83 . . . . . . . 5995 2 70 . 1 1 115 115 GLN N N 15 73.63 4.35 . . . . . . . 5995 2 71 . 1 1 116 116 LEU N N 15 67.34 4.88 . . . . . . . 5995 2 72 . 1 1 117 117 MET N N 15 48.37 6.46 . . . . . . . 5995 2 73 . 1 1 118 118 GLY N N 15 61.49 2.24 . . . . . . . 5995 2 74 . 1 1 119 119 LEU N N 15 57.14 3.69 . . . . . . . 5995 2 75 . 1 1 120 120 TYR N N 15 59.24 2.85 . . . . . . . 5995 2 76 . 1 1 121 121 GLY N N 15 54.12 3.85 . . . . . . . 5995 2 77 . 1 1 125 125 ASP N N 15 52.40 3.73 . . . . . . . 5995 2 78 . 1 1 126 126 LEU N N 15 68.70 2.37 . . . . . . . 5995 2 79 . 1 1 127 127 SER N N 15 71.83 9.50 . . . . . . . 5995 2 80 . 1 1 130 130 ILE N N 15 60.77 4.26 . . . . . . . 5995 2 81 . 1 1 131 131 LYS N N 15 68.89 1.16 . . . . . . . 5995 2 82 . 1 1 133 133 ARG N N 15 61.99 2.99 . . . . . . . 5995 2 83 . 1 1 135 135 ALA N N 15 65.11 3.83 . . . . . . . 5995 2 84 . 1 1 136 136 GLN N N 15 64.41 6.25 . . . . . . . 5995 2 85 . 1 1 137 137 LEU N N 15 60.88 3.46 . . . . . . . 5995 2 86 . 1 1 138 138 CYS N N 15 64.24 3.18 . . . . . . . 5995 2 87 . 1 1 140 140 LYS N N 15 63.96 2.89 . . . . . . . 5995 2 88 . 1 1 141 141 HIS N N 15 78.70 3.08 . . . . . . . 5995 2 89 . 1 1 142 142 GLY N N 15 61.61 2.77 . . . . . . . 5995 2 90 . 1 1 144 144 LEU N N 15 77.05 2.06 . . . . . . . 5995 2 91 . 1 1 145 145 ARG N N 15 66.03 2.25 . . . . . . . 5995 2 92 . 1 1 146 146 GLU N N 15 62.15 6.05 . . . . . . . 5995 2 93 . 1 1 148 148 ILE N N 15 70.58 3.75 . . . . . . . 5995 2 94 . 1 1 151 151 LEU N N 15 63.03 5.67 . . . . . . . 5995 2 95 . 1 1 155 155 ASN N N 15 50.56 4.58 . . . . . . . 5995 2 96 . 1 1 157 157 CYS N N 15 67.42 3.78 . . . . . . . 5995 2 97 . 1 1 158 158 LEU N N 15 70.61 6.30 . . . . . . . 5995 2 98 . 1 1 162 162 GLU N N 15 112.02 2.17 . . . . . . . 5995 2 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_298_600_free_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 298_600_free_t2 _Heteronucl_T2_list.Entry_ID 5995 _Heteronucl_T2_list.ID 3 _Heteronucl_T2_list.Sample_condition_list_ID 4 _Heteronucl_T2_list.Sample_condition_list_label $298K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5995 3 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ALA N N 15 70.93 4.31 . . . . . . . 5995 3 2 . 1 1 4 4 SER N N 15 90.48 9.50 . . . . . . . 5995 3 3 . 1 1 11 11 ASN N N 15 86.89 4.75 . . . . . . . 5995 3 4 . 1 1 12 12 VAL N N 15 85.37 5.14 . . . . . . . 5995 3 5 . 1 1 13 13 GLU N N 15 72.79 3.63 . . . . . . . 5995 3 6 . 1 1 16 16 ASN N N 15 73.54 2.74 . . . . . . . 5995 3 7 . 1 1 17 17 GLY N N 15 84.17 2.49 . . . . . . . 5995 3 8 . 1 1 18 18 GLU N N 15 50.38 2.34 . . . . . . . 5995 3 9 . 1 1 19 19 TRP N N 15 50.06 2.23 . . . . . . . 5995 3 10 . 1 1 20 20 HIS N N 15 61.70 1.63 . . . . . . . 5995 3 11 . 1 1 22 22 ILE N N 15 77.94 5.23 . . . . . . . 5995 3 12 . 1 1 23 23 ILE N N 15 85.40 2.93 . . . . . . . 5995 3 13 . 1 1 24 24 LEU N N 15 79.50 3.63 . . . . . . . 5995 3 14 . 1 1 26 26 SER N N 15 88.45 4.52 . . . . . . . 5995 3 15 . 1 1 27 27 ASP N N 15 82.69 3.70 . . . . . . . 5995 3 16 . 1 1 28 28 LYS N N 15 86.29 4.37 . . . . . . . 5995 3 17 . 1 1 30 30 GLU N N 15 85.93 2.18 . . . . . . . 5995 3 18 . 1 1 31 31 LYS N N 15 78.33 2.66 . . . . . . . 5995 3 19 . 1 1 32 32 ILE N N 15 77.42 4.15 . . . . . . . 5995 3 20 . 1 1 33 33 GLU N N 15 82.87 4.28 . . . . . . . 5995 3 21 . 1 1 36 36 GLY N N 15 88.96 4.55 . . . . . . . 5995 3 22 . 1 1 37 37 ASN N N 15 38.02 2.01 . . . . . . . 5995 3 23 . 1 1 38 38 PHE N N 15 82.80 4.58 . . . . . . . 5995 3 24 . 1 1 39 39 ARG N N 15 78.58 3.63 . . . . . . . 5995 3 25 . 1 1 40 40 LEU N N 15 71.50 2.93 . . . . . . . 5995 3 26 . 1 1 41 41 PHE N N 15 91.38 4.08 . . . . . . . 5995 3 27 . 1 1 48 48 LEU N N 15 89.78 2.87 . . . . . . . 5995 3 28 . 1 1 51 51 SER N N 15 94.44 6.05 . . . . . . . 5995 3 29 . 1 1 53 53 VAL N N 15 81.83 3.28 . . . . . . . 5995 3 30 . 1 1 54 54 LEU N N 15 89.99 4.69 . . . . . . . 5995 3 31 . 1 1 55 55 LYS N N 15 80.44 3.34 . . . . . . . 5995 3 32 . 1 1 57 57 HIS N N 15 51.15 3.20 . . . . . . . 5995 3 33 . 1 1 58 58 THR N N 15 64.99 1.97 . . . . . . . 5995 3 34 . 1 1 60 60 ARG N N 15 92.03 2.74 . . . . . . . 5995 3 35 . 1 1 62 62 GLU N N 15 39.55 3.33 . . . . . . . 5995 3 36 . 1 1 64 64 CYS N N 15 86.70 3.75 . . . . . . . 5995 3 37 . 1 1 66 66 GLU N N 15 89.16 2.02 . . . . . . . 5995 3 38 . 1 1 68 68 SER N N 15 83.47 3.70 . . . . . . . 5995 3 39 . 1 1 69 69 MET N N 15 79.47 3.94 . . . . . . . 5995 3 40 . 1 1 70 70 VAL N N 15 68.91 3.38 . . . . . . . 5995 3 41 . 1 1 71 71 ALA N N 15 87.38 3.60 . . . . . . . 5995 3 42 . 1 1 72 72 ASP N N 15 87.78 4.24 . . . . . . . 5995 3 43 . 1 1 74 74 THR N N 15 95.05 4.05 . . . . . . . 5995 3 44 . 1 1 75 75 GLU N N 15 89.53 5.26 . . . . . . . 5995 3 45 . 1 1 76 76 LYS N N 15 82.14 3.59 . . . . . . . 5995 3 46 . 1 1 79 79 GLU N N 15 78.81 3.23 . . . . . . . 5995 3 47 . 1 1 81 81 SER N N 15 84.35 4.06 . . . . . . . 5995 3 48 . 1 1 82 82 VAL N N 15 80.26 2.89 . . . . . . . 5995 3 49 . 1 1 84 84 TYR N N 15 90.88 2.99 . . . . . . . 5995 3 50 . 1 1 85 85 ASP N N 15 67.40 3.26 . . . . . . . 5995 3 51 . 1 1 86 86 GLY N N 15 85.83 4.22 . . . . . . . 5995 3 52 . 1 1 88 88 ASN N N 15 82.12 2.86 . . . . . . . 5995 3 53 . 1 1 89 89 THR N N 15 83.48 3.65 . . . . . . . 5995 3 54 . 1 1 91 91 THR N N 15 65.08 7.07 . . . . . . . 5995 3 55 . 1 1 92 92 ILE N N 15 79.45 4.69 . . . . . . . 5995 3 56 . 1 1 94 94 LYS N N 15 78.52 3.61 . . . . . . . 5995 3 57 . 1 1 96 96 ASP N N 15 80.64 3.59 . . . . . . . 5995 3 58 . 1 1 97 97 TYR N N 15 80.10 4.17 . . . . . . . 5995 3 59 . 1 1 100 100 PHE N N 15 77.70 3.52 . . . . . . . 5995 3 60 . 1 1 101 101 LEU N N 15 82.14 3.53 . . . . . . . 5995 3 61 . 1 1 103 103 ALA N N 15 80.62 4.30 . . . . . . . 5995 3 62 . 1 1 104 104 HIS N N 15 80.68 3.93 . . . . . . . 5995 3 63 . 1 1 105 105 LEU N N 15 74.55 3.28 . . . . . . . 5995 3 64 . 1 1 106 106 ILE N N 15 81.67 4.32 . . . . . . . 5995 3 65 . 1 1 107 107 ASN N N 15 87.63 4.42 . . . . . . . 5995 3 66 . 1 1 111 111 GLY N N 15 87.88 3.28 . . . . . . . 5995 3 67 . 1 1 113 113 THR N N 15 77.80 4.44 . . . . . . . 5995 3 68 . 1 1 114 114 PHE N N 15 80.61 3.44 . . . . . . . 5995 3 69 . 1 1 115 115 GLN N N 15 84.02 3.82 . . . . . . . 5995 3 70 . 1 1 116 116 LEU N N 15 83.66 3.86 . . . . . . . 5995 3 71 . 1 1 117 117 MET N N 15 79.27 3.85 . . . . . . . 5995 3 72 . 1 1 118 118 GLY N N 15 80.30 2.93 . . . . . . . 5995 3 73 . 1 1 119 119 LEU N N 15 77.27 3.45 . . . . . . . 5995 3 74 . 1 1 120 120 TYR N N 15 78.61 3.02 . . . . . . . 5995 3 75 . 1 1 121 121 GLY N N 15 72.62 3.27 . . . . . . . 5995 3 76 . 1 1 123 123 GLU N N 15 84.49 4.04 . . . . . . . 5995 3 77 . 1 1 125 125 ASP N N 15 77.60 2.67 . . . . . . . 5995 3 78 . 1 1 126 126 LEU N N 15 85.47 3.59 . . . . . . . 5995 3 79 . 1 1 127 127 SER N N 15 91.14 2.46 . . . . . . . 5995 3 80 . 1 1 128 128 SER N N 15 45.81 2.61 . . . . . . . 5995 3 81 . 1 1 129 129 ASP N N 15 88.83 3.69 . . . . . . . 5995 3 82 . 1 1 130 130 ILE N N 15 82.11 4.88 . . . . . . . 5995 3 83 . 1 1 131 131 LYS N N 15 81.57 3.08 . . . . . . . 5995 3 84 . 1 1 133 133 ARG N N 15 81.05 3.14 . . . . . . . 5995 3 85 . 1 1 134 134 PHE N N 15 82.06 3.97 . . . . . . . 5995 3 86 . 1 1 135 135 ALA N N 15 81.45 3.46 . . . . . . . 5995 3 87 . 1 1 136 136 GLN N N 15 88.15 4.38 . . . . . . . 5995 3 88 . 1 1 137 137 LEU N N 15 80.89 3.78 . . . . . . . 5995 3 89 . 1 1 138 138 CYS N N 15 76.65 3.17 . . . . . . . 5995 3 90 . 1 1 140 140 LYS N N 15 79.56 3.27 . . . . . . . 5995 3 91 . 1 1 141 141 HIS N N 15 92.58 3.64 . . . . . . . 5995 3 92 . 1 1 142 142 GLY N N 15 79.94 3.61 . . . . . . . 5995 3 93 . 1 1 143 143 ILE N N 15 40.04 2.90 . . . . . . . 5995 3 94 . 1 1 144 144 LEU N N 15 94.11 4.10 . . . . . . . 5995 3 95 . 1 1 145 145 ARG N N 15 84.17 3.03 . . . . . . . 5995 3 96 . 1 1 146 146 GLU N N 15 83.39 4.27 . . . . . . . 5995 3 97 . 1 1 148 148 ILE N N 15 87.19 3.11 . . . . . . . 5995 3 98 . 1 1 151 151 LEU N N 15 85.32 4.45 . . . . . . . 5995 3 99 . 1 1 158 158 LEU N N 15 84.44 3.52 . . . . . . . 5995 3 100 . 1 1 162 162 GLU N N 15 158.89 5.71 . . . . . . . 5995 3 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_303_600_free_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 303_600_free_t2 _Heteronucl_T2_list.Entry_ID 5995 _Heteronucl_T2_list.ID 4 _Heteronucl_T2_list.Sample_condition_list_ID 5 _Heteronucl_T2_list.Sample_condition_list_label $303K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5995 4 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ALA N N 15 92.55 3.45 . . . . . . . 5995 4 2 . 1 1 4 4 SER N N 15 87.57 3.18 . . . . . . . 5995 4 3 . 1 1 6 6 THR N N 15 66.30 1.71 . . . . . . . 5995 4 4 . 1 1 11 11 ASN N N 15 78.65 5.55 . . . . . . . 5995 4 5 . 1 1 12 12 VAL N N 15 109.01 4.35 . . . . . . . 5995 4 6 . 1 1 13 13 GLU N N 15 76.44 6.91 . . . . . . . 5995 4 7 . 1 1 16 16 ASN N N 15 62.81 5.09 . . . . . . . 5995 4 8 . 1 1 17 17 GLY N N 15 98.37 4.90 . . . . . . . 5995 4 9 . 1 1 19 19 TRP N N 15 109.17 3.45 . . . . . . . 5995 4 10 . 1 1 20 20 HIS N N 15 52.30 4.73 . . . . . . . 5995 4 11 . 1 1 21 21 THR N N 15 112.76 4.82 . . . . . . . 5995 4 12 . 1 1 22 22 ILE N N 15 99.72 5.08 . . . . . . . 5995 4 13 . 1 1 23 23 ILE N N 15 86.30 5.12 . . . . . . . 5995 4 14 . 1 1 24 24 LEU N N 15 84.58 4.28 . . . . . . . 5995 4 15 . 1 1 26 26 SER N N 15 82.98 5.35 . . . . . . . 5995 4 16 . 1 1 27 27 ASP N N 15 53.48 3.26 . . . . . . . 5995 4 17 . 1 1 28 28 LYS N N 15 77.33 9.39 . . . . . . . 5995 4 18 . 1 1 30 30 GLU N N 15 99.85 5.40 . . . . . . . 5995 4 19 . 1 1 31 31 LYS N N 15 81.93 12.20 . . . . . . . 5995 4 20 . 1 1 32 32 ILE N N 15 76.18 4.85 . . . . . . . 5995 4 21 . 1 1 33 33 GLU N N 15 43.98 5.24 . . . . . . . 5995 4 22 . 1 1 35 35 ASN N N 15 82.45 2.27 . . . . . . . 5995 4 23 . 1 1 36 36 GLY N N 15 100.87 4.43 . . . . . . . 5995 4 24 . 1 1 38 38 PHE N N 15 43.23 7.25 . . . . . . . 5995 4 25 . 1 1 39 39 ARG N N 15 56.57 2.87 . . . . . . . 5995 4 26 . 1 1 40 40 LEU N N 15 49.08 2.65 . . . . . . . 5995 4 27 . 1 1 42 42 LEU N N 15 99.31 6.91 . . . . . . . 5995 4 28 . 1 1 46 46 HIS N N 15 89.63 6.22 . . . . . . . 5995 4 29 . 1 1 48 48 LEU N N 15 89.00 2.72 . . . . . . . 5995 4 30 . 1 1 51 51 SER N N 15 76.91 7.50 . . . . . . . 5995 4 31 . 1 1 52 52 LEU N N 15 108.89 2.42 . . . . . . . 5995 4 32 . 1 1 53 53 VAL N N 15 90.55 7.62 . . . . . . . 5995 4 33 . 1 1 54 54 LEU N N 15 98.66 3.73 . . . . . . . 5995 4 34 . 1 1 55 55 LYS N N 15 116.71 3.10 . . . . . . . 5995 4 35 . 1 1 57 57 HIS N N 15 59.41 3.95 . . . . . . . 5995 4 36 . 1 1 58 58 THR N N 15 66.12 1.55 . . . . . . . 5995 4 37 . 1 1 60 60 ARG N N 15 76.40 3.00 . . . . . . . 5995 4 38 . 1 1 62 62 GLU N N 15 55.95 2.82 . . . . . . . 5995 4 39 . 1 1 64 64 CYS N N 15 92.53 6.85 . . . . . . . 5995 4 40 . 1 1 67 67 LEU N N 15 76.81 7.00 . . . . . . . 5995 4 41 . 1 1 68 68 SER N N 15 96.95 7.05 . . . . . . . 5995 4 42 . 1 1 69 69 MET N N 15 75.41 5.37 . . . . . . . 5995 4 43 . 1 1 70 70 VAL N N 15 84.43 6.57 . . . . . . . 5995 4 44 . 1 1 71 71 ALA N N 15 90.94 7.60 . . . . . . . 5995 4 45 . 1 1 72 72 ASP N N 15 97.30 8.44 . . . . . . . 5995 4 46 . 1 1 74 74 THR N N 15 81.76 5.27 . . . . . . . 5995 4 47 . 1 1 76 76 LYS N N 15 80.66 5.45 . . . . . . . 5995 4 48 . 1 1 77 77 ALA N N 15 71.20 3.84 . . . . . . . 5995 4 49 . 1 1 79 79 GLU N N 15 53.05 3.26 . . . . . . . 5995 4 50 . 1 1 81 81 SER N N 15 78.30 10.87 . . . . . . . 5995 4 51 . 1 1 84 84 TYR N N 15 114.15 6.27 . . . . . . . 5995 4 52 . 1 1 86 86 GLY N N 15 103.63 5.45 . . . . . . . 5995 4 53 . 1 1 88 88 ASN N N 15 77.20 6.98 . . . . . . . 5995 4 54 . 1 1 89 89 THR N N 15 70.33 1.96 . . . . . . . 5995 4 55 . 1 1 92 92 ILE N N 15 98.14 2.66 . . . . . . . 5995 4 56 . 1 1 94 94 LYS N N 15 59.20 2.47 . . . . . . . 5995 4 57 . 1 1 95 95 THR N N 15 85.27 3.66 . . . . . . . 5995 4 58 . 1 1 96 96 ASP N N 15 76.91 3.88 . . . . . . . 5995 4 59 . 1 1 97 97 TYR N N 15 81.00 3.10 . . . . . . . 5995 4 60 . 1 1 98 98 ASP N N 15 82.40 5.00 . . . . . . . 5995 4 61 . 1 1 99 99 ASN N N 15 63.99 3.39 . . . . . . . 5995 4 62 . 1 1 101 101 LEU N N 15 83.13 3.41 . . . . . . . 5995 4 63 . 1 1 102 102 MET N N 15 96.85 7.79 . . . . . . . 5995 4 64 . 1 1 103 103 ALA N N 15 96.91 4.38 . . . . . . . 5995 4 65 . 1 1 104 104 HIS N N 15 79.85 4.05 . . . . . . . 5995 4 66 . 1 1 105 105 LEU N N 15 84.86 4.38 . . . . . . . 5995 4 67 . 1 1 106 106 ILE N N 15 84.60 5.41 . . . . . . . 5995 4 68 . 1 1 107 107 ASN N N 15 82.90 5.37 . . . . . . . 5995 4 69 . 1 1 108 108 GLU N N 15 88.57 5.97 . . . . . . . 5995 4 70 . 1 1 110 110 ASP N N 15 77.30 4.03 . . . . . . . 5995 4 71 . 1 1 111 111 GLY N N 15 88.83 4.12 . . . . . . . 5995 4 72 . 1 1 113 113 THR N N 15 106.70 3.80 . . . . . . . 5995 4 73 . 1 1 114 114 PHE N N 15 92.29 5.23 . . . . . . . 5995 4 74 . 1 1 115 115 GLN N N 15 80.73 3.36 . . . . . . . 5995 4 75 . 1 1 116 116 LEU N N 15 90.98 4.61 . . . . . . . 5995 4 76 . 1 1 117 117 MET N N 15 83.36 4.86 . . . . . . . 5995 4 77 . 1 1 118 118 GLY N N 15 84.62 5.71 . . . . . . . 5995 4 78 . 1 1 119 119 LEU N N 15 103.59 8.99 . . . . . . . 5995 4 79 . 1 1 120 120 TYR N N 15 81.32 3.98 . . . . . . . 5995 4 80 . 1 1 121 121 GLY N N 15 81.55 5.50 . . . . . . . 5995 4 81 . 1 1 123 123 GLU N N 15 119.82 4.03 . . . . . . . 5995 4 82 . 1 1 125 125 ASP N N 15 59.12 1.53 . . . . . . . 5995 4 83 . 1 1 126 126 LEU N N 15 85.55 5.33 . . . . . . . 5995 4 84 . 1 1 127 127 SER N N 15 93.88 3.57 . . . . . . . 5995 4 85 . 1 1 128 128 SER N N 15 71.20 1.67 . . . . . . . 5995 4 86 . 1 1 129 129 ASP N N 15 109.07 2.57 . . . . . . . 5995 4 87 . 1 1 130 130 ILE N N 15 78.84 2.79 . . . . . . . 5995 4 88 . 1 1 131 131 LYS N N 15 92.06 4.90 . . . . . . . 5995 4 89 . 1 1 133 133 ARG N N 15 75.72 1.51 . . . . . . . 5995 4 90 . 1 1 135 135 ALA N N 15 79.41 5.87 . . . . . . . 5995 4 91 . 1 1 136 136 GLN N N 15 81.22 6.30 . . . . . . . 5995 4 92 . 1 1 137 137 LEU N N 15 58.44 4.40 . . . . . . . 5995 4 93 . 1 1 138 138 CYS N N 15 56.47 14.64 . . . . . . . 5995 4 94 . 1 1 140 140 LYS N N 15 60.12 1.63 . . . . . . . 5995 4 95 . 1 1 141 141 HIS N N 15 44.76 14.16 . . . . . . . 5995 4 96 . 1 1 142 142 GLY N N 15 58.74 1.27 . . . . . . . 5995 4 97 . 1 1 143 143 ILE N N 15 57.57 2.03 . . . . . . . 5995 4 98 . 1 1 144 144 LEU N N 15 97.85 5.83 . . . . . . . 5995 4 99 . 1 1 145 145 ARG N N 15 93.36 6.07 . . . . . . . 5995 4 100 . 1 1 146 146 GLU N N 15 82.93 2.98 . . . . . . . 5995 4 101 . 1 1 148 148 ILE N N 15 79.68 4.16 . . . . . . . 5995 4 102 . 1 1 151 151 LEU N N 15 101.01 5.90 . . . . . . . 5995 4 103 . 1 1 152 152 SER N N 15 94.98 1.65 . . . . . . . 5995 4 104 . 1 1 153 153 ASN N N 15 81.21 5.16 . . . . . . . 5995 4 105 . 1 1 157 157 CYS N N 15 90.56 6.88 . . . . . . . 5995 4 106 . 1 1 158 158 LEU N N 15 85.55 8.34 . . . . . . . 5995 4 107 . 1 1 162 162 GLU N N 15 200.01 7.39 . . . . . . . 5995 4 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_308_600_free_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 308_600_free_t2 _Heteronucl_T2_list.Entry_ID 5995 _Heteronucl_T2_list.ID 5 _Heteronucl_T2_list.Sample_condition_list_ID 6 _Heteronucl_T2_list.Sample_condition_list_label $308K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5995 5 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 4 4 SER N N 15 69.42 3.55 . . . . . . . 5995 5 2 . 1 1 13 13 GLU N N 15 89.17 6.27 . . . . . . . 5995 5 3 . 1 1 16 16 ASN N N 15 84.83 4.50 . . . . . . . 5995 5 4 . 1 1 17 17 GLY N N 15 101.96 2.91 . . . . . . . 5995 5 5 . 1 1 19 19 TRP N N 15 78.09 4.82 . . . . . . . 5995 5 6 . 1 1 22 22 ILE N N 15 96.79 8.13 . . . . . . . 5995 5 7 . 1 1 23 23 ILE N N 15 100.90 5.95 . . . . . . . 5995 5 8 . 1 1 26 26 SER N N 15 98.48 3.43 . . . . . . . 5995 5 9 . 1 1 30 30 GLU N N 15 100.72 6.51 . . . . . . . 5995 5 10 . 1 1 31 31 LYS N N 15 95.97 6.18 . . . . . . . 5995 5 11 . 1 1 32 32 ILE N N 15 87.28 4.37 . . . . . . . 5995 5 12 . 1 1 33 33 GLU N N 15 88.22 6.77 . . . . . . . 5995 5 13 . 1 1 36 36 GLY N N 15 111.28 4.62 . . . . . . . 5995 5 14 . 1 1 38 38 PHE N N 15 99.28 7.08 . . . . . . . 5995 5 15 . 1 1 39 39 ARG N N 15 89.53 5.78 . . . . . . . 5995 5 16 . 1 1 40 40 LEU N N 15 87.59 2.93 . . . . . . . 5995 5 17 . 1 1 48 48 LEU N N 15 105.15 5.81 . . . . . . . 5995 5 18 . 1 1 51 51 SER N N 15 104.14 7.16 . . . . . . . 5995 5 19 . 1 1 53 53 VAL N N 15 97.24 4.39 . . . . . . . 5995 5 20 . 1 1 54 54 LEU N N 15 104.82 5.89 . . . . . . . 5995 5 21 . 1 1 57 57 HIS N N 15 83.84 5.64 . . . . . . . 5995 5 22 . 1 1 60 60 ARG N N 15 101.84 6.04 . . . . . . . 5995 5 23 . 1 1 68 68 SER N N 15 106.45 1.89 . . . . . . . 5995 5 24 . 1 1 69 69 MET N N 15 94.63 5.70 . . . . . . . 5995 5 25 . 1 1 71 71 ALA N N 15 101.87 6.14 . . . . . . . 5995 5 26 . 1 1 74 74 THR N N 15 108.16 6.94 . . . . . . . 5995 5 27 . 1 1 79 79 GLU N N 15 87.51 3.49 . . . . . . . 5995 5 28 . 1 1 81 81 SER N N 15 99.49 4.67 . . . . . . . 5995 5 29 . 1 1 86 86 GLY N N 15 107.48 4.43 . . . . . . . 5995 5 30 . 1 1 89 89 THR N N 15 94.44 10.81 . . . . . . . 5995 5 31 . 1 1 92 92 ILE N N 15 101.91 6.07 . . . . . . . 5995 5 32 . 1 1 94 94 LYS N N 15 108.65 4.12 . . . . . . . 5995 5 33 . 1 1 96 96 ASP N N 15 93.82 7.88 . . . . . . . 5995 5 34 . 1 1 100 100 PHE N N 15 88.94 5.51 . . . . . . . 5995 5 35 . 1 1 101 101 LEU N N 15 97.67 4.37 . . . . . . . 5995 5 36 . 1 1 103 103 ALA N N 15 97.16 3.42 . . . . . . . 5995 5 37 . 1 1 105 105 LEU N N 15 89.63 6.42 . . . . . . . 5995 5 38 . 1 1 107 107 ASN N N 15 95.09 4.10 . . . . . . . 5995 5 39 . 1 1 111 111 GLY N N 15 111.73 14.27 . . . . . . . 5995 5 40 . 1 1 115 115 GLN N N 15 99.90 7.32 . . . . . . . 5995 5 41 . 1 1 116 116 LEU N N 15 103.61 3.98 . . . . . . . 5995 5 42 . 1 1 117 117 MET N N 15 94.11 4.14 . . . . . . . 5995 5 43 . 1 1 118 118 GLY N N 15 95.50 4.01 . . . . . . . 5995 5 44 . 1 1 120 120 TYR N N 15 96.12 3.51 . . . . . . . 5995 5 45 . 1 1 121 121 GLY N N 15 89.74 4.86 . . . . . . . 5995 5 46 . 1 1 123 123 GLU N N 15 112.51 9.63 . . . . . . . 5995 5 47 . 1 1 125 125 ASP N N 15 96.14 5.86 . . . . . . . 5995 5 48 . 1 1 126 126 LEU N N 15 102.18 4.44 . . . . . . . 5995 5 49 . 1 1 127 127 SER N N 15 113.23 6.53 . . . . . . . 5995 5 50 . 1 1 130 130 ILE N N 15 95.09 6.10 . . . . . . . 5995 5 51 . 1 1 133 133 ARG N N 15 91.09 5.08 . . . . . . . 5995 5 52 . 1 1 136 136 GLN N N 15 96.62 5.35 . . . . . . . 5995 5 53 . 1 1 137 137 LEU N N 15 89.94 5.96 . . . . . . . 5995 5 54 . 1 1 138 138 CYS N N 15 85.22 5.45 . . . . . . . 5995 5 55 . 1 1 140 140 LYS N N 15 93.44 6.83 . . . . . . . 5995 5 56 . 1 1 141 141 HIS N N 15 93.32 7.59 . . . . . . . 5995 5 57 . 1 1 142 142 GLY N N 15 91.21 7.83 . . . . . . . 5995 5 58 . 1 1 144 144 LEU N N 15 113.18 4.93 . . . . . . . 5995 5 59 . 1 1 145 145 ARG N N 15 102.95 4.53 . . . . . . . 5995 5 60 . 1 1 148 148 ILE N N 15 100.12 5.50 . . . . . . . 5995 5 61 . 1 1 151 151 LEU N N 15 101.89 3.78 . . . . . . . 5995 5 62 . 1 1 162 162 GLU N N 15 230.75 7.13 . . . . . . . 5995 5 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_291_500_free_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 291_500_free_t2 _Heteronucl_T2_list.Entry_ID 5995 _Heteronucl_T2_list.ID 6 _Heteronucl_T2_list.Sample_condition_list_ID 7 _Heteronucl_T2_list.Sample_condition_list_label $291K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 500 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5995 6 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 4 4 SER N N 15 81.61 5.66 . . . . . . . 5995 6 2 . 1 1 6 6 THR N N 15 64.49 3.54 . . . . . . . 5995 6 3 . 1 1 7 7 GLY N N 15 79.78 3.99 . . . . . . . 5995 6 4 . 1 1 11 11 ASN N N 15 77.08 3.44 . . . . . . . 5995 6 5 . 1 1 12 12 VAL N N 15 74.47 4.27 . . . . . . . 5995 6 6 . 1 1 13 13 GLU N N 15 67.26 4.98 . . . . . . . 5995 6 7 . 1 1 15 15 ILE N N 15 76.07 4.40 . . . . . . . 5995 6 8 . 1 1 16 16 ASN N N 15 66.50 1.50 . . . . . . . 5995 6 9 . 1 1 17 17 GLY N N 15 77.19 5.73 . . . . . . . 5995 6 10 . 1 1 22 22 ILE N N 15 59.48 2.89 . . . . . . . 5995 6 11 . 1 1 23 23 ILE N N 15 72.48 2.77 . . . . . . . 5995 6 12 . 1 1 26 26 SER N N 15 77.43 4.37 . . . . . . . 5995 6 13 . 1 1 27 27 ASP N N 15 60.89 3.50 . . . . . . . 5995 6 14 . 1 1 30 30 GLU N N 15 77.30 2.30 . . . . . . . 5995 6 15 . 1 1 31 31 LYS N N 15 70.73 4.33 . . . . . . . 5995 6 16 . 1 1 32 32 ILE N N 15 80.48 8.05 . . . . . . . 5995 6 17 . 1 1 33 33 GLU N N 15 78.73 4.48 . . . . . . . 5995 6 18 . 1 1 36 36 GLY N N 15 80.64 5.51 . . . . . . . 5995 6 19 . 1 1 37 37 ASN N N 15 64.00 6.57 . . . . . . . 5995 6 20 . 1 1 39 39 ARG N N 15 78.38 2.08 . . . . . . . 5995 6 21 . 1 1 40 40 LEU N N 15 61.62 6.47 . . . . . . . 5995 6 22 . 1 1 47 47 VAL N N 15 80.08 1.80 . . . . . . . 5995 6 23 . 1 1 48 48 LEU N N 15 77.27 4.86 . . . . . . . 5995 6 24 . 1 1 51 51 SER N N 15 84.34 3.46 . . . . . . . 5995 6 25 . 1 1 53 53 VAL N N 15 70.42 3.58 . . . . . . . 5995 6 26 . 1 1 54 54 LEU N N 15 75.35 4.83 . . . . . . . 5995 6 27 . 1 1 55 55 LYS N N 15 73.64 3.89 . . . . . . . 5995 6 28 . 1 1 60 60 ARG N N 15 81.60 2.68 . . . . . . . 5995 6 29 . 1 1 64 64 CYS N N 15 60.26 2.66 . . . . . . . 5995 6 30 . 1 1 67 67 LEU N N 15 74.53 2.76 . . . . . . . 5995 6 31 . 1 1 68 68 SER N N 15 74.68 2.19 . . . . . . . 5995 6 32 . 1 1 69 69 MET N N 15 73.81 6.10 . . . . . . . 5995 6 33 . 1 1 71 71 ALA N N 15 77.80 5.16 . . . . . . . 5995 6 34 . 1 1 72 72 ASP N N 15 74.16 4.08 . . . . . . . 5995 6 35 . 1 1 74 74 THR N N 15 82.89 6.82 . . . . . . . 5995 6 36 . 1 1 76 76 LYS N N 15 73.96 3.35 . . . . . . . 5995 6 37 . 1 1 77 77 ALA N N 15 86.25 7.30 . . . . . . . 5995 6 38 . 1 1 79 79 GLU N N 15 75.51 3.30 . . . . . . . 5995 6 39 . 1 1 80 80 TYR N N 15 75.59 6.26 . . . . . . . 5995 6 40 . 1 1 81 81 SER N N 15 79.55 3.85 . . . . . . . 5995 6 41 . 1 1 86 86 GLY N N 15 77.90 3.75 . . . . . . . 5995 6 42 . 1 1 88 88 ASN N N 15 75.12 2.78 . . . . . . . 5995 6 43 . 1 1 89 89 THR N N 15 64.09 7.83 . . . . . . . 5995 6 44 . 1 1 91 91 THR N N 15 70.62 11.0 . . . . . . . 5995 6 45 . 1 1 92 92 ILE N N 15 70.44 5.89 . . . . . . . 5995 6 46 . 1 1 94 94 LYS N N 15 69.50 5.01 . . . . . . . 5995 6 47 . 1 1 96 96 ASP N N 15 81.23 5.82 . . . . . . . 5995 6 48 . 1 1 97 97 TYR N N 15 72.21 6.38 . . . . . . . 5995 6 49 . 1 1 98 98 ASP N N 15 64.85 5.16 . . . . . . . 5995 6 50 . 1 1 100 100 PHE N N 15 63.03 2.88 . . . . . . . 5995 6 51 . 1 1 101 101 LEU N N 15 70.02 4.27 . . . . . . . 5995 6 52 . 1 1 102 102 MET N N 15 71.75 3.94 . . . . . . . 5995 6 53 . 1 1 103 103 ALA N N 15 72.61 2.85 . . . . . . . 5995 6 54 . 1 1 104 104 HIS N N 15 76.75 5.84 . . . . . . . 5995 6 55 . 1 1 105 105 LEU N N 15 68.88 5.25 . . . . . . . 5995 6 56 . 1 1 107 107 ASN N N 15 70.30 2.80 . . . . . . . 5995 6 57 . 1 1 108 108 GLU N N 15 77.65 2.21 . . . . . . . 5995 6 58 . 1 1 111 111 GLY N N 15 84.46 7.28 . . . . . . . 5995 6 59 . 1 1 113 113 THR N N 15 80.88 6.56 . . . . . . . 5995 6 60 . 1 1 115 115 GLN N N 15 70.72 1.72 . . . . . . . 5995 6 61 . 1 1 116 116 LEU N N 15 82.67 3.48 . . . . . . . 5995 6 62 . 1 1 117 117 MET N N 15 73.03 5.03 . . . . . . . 5995 6 63 . 1 1 118 118 GLY N N 15 67.57 4.21 . . . . . . . 5995 6 64 . 1 1 121 121 GLY N N 15 70.52 6.09 . . . . . . . 5995 6 65 . 1 1 123 123 GLU N N 15 67.17 5.35 . . . . . . . 5995 6 66 . 1 1 125 125 ASP N N 15 68.84 2.91 . . . . . . . 5995 6 67 . 1 1 126 126 LEU N N 15 76.53 1.26 . . . . . . . 5995 6 68 . 1 1 127 127 SER N N 15 78.27 1.89 . . . . . . . 5995 6 69 . 1 1 129 129 ASP N N 15 77.14 3.35 . . . . . . . 5995 6 70 . 1 1 130 130 ILE N N 15 76.62 4.05 . . . . . . . 5995 6 71 . 1 1 131 131 LYS N N 15 75.25 5.01 . . . . . . . 5995 6 72 . 1 1 133 133 ARG N N 15 71.88 3.66 . . . . . . . 5995 6 73 . 1 1 136 136 GLN N N 15 76.33 2.86 . . . . . . . 5995 6 74 . 1 1 137 137 LEU N N 15 74.79 3.17 . . . . . . . 5995 6 75 . 1 1 138 138 CYS N N 15 70.59 1.96 . . . . . . . 5995 6 76 . 1 1 140 140 LYS N N 15 74.39 3.57 . . . . . . . 5995 6 77 . 1 1 141 141 HIS N N 15 77.54 3.89 . . . . . . . 5995 6 78 . 1 1 142 142 GLY N N 15 80.80 5.79 . . . . . . . 5995 6 79 . 1 1 144 144 LEU N N 15 77.79 3.19 . . . . . . . 5995 6 80 . 1 1 145 145 ARG N N 15 76.81 3.51 . . . . . . . 5995 6 81 . 1 1 148 148 ILE N N 15 74.28 2.52 . . . . . . . 5995 6 82 . 1 1 151 151 LEU N N 15 68.00 5.04 . . . . . . . 5995 6 83 . 1 1 153 153 ASN N N 15 79.52 5.27 . . . . . . . 5995 6 84 . 1 1 158 158 LEU N N 15 76.58 2.21 . . . . . . . 5995 6 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_297_500_free_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 297_500_free_t2 _Heteronucl_T2_list.Entry_ID 5995 _Heteronucl_T2_list.ID 7 _Heteronucl_T2_list.Sample_condition_list_ID 8 _Heteronucl_T2_list.Sample_condition_list_label $297K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 500 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5995 7 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ALA N N 15 93.19 7.28 . . . . . . . 5995 7 2 . 1 1 4 4 SER N N 15 86.77 4.27 . . . . . . . 5995 7 3 . 1 1 6 6 THR N N 15 82.18 14.2 . . . . . . . 5995 7 4 . 1 1 7 7 GLY N N 15 89.33 7.87 . . . . . . . 5995 7 5 . 1 1 11 11 ASN N N 15 88.16 7.28 . . . . . . . 5995 7 6 . 1 1 12 12 VAL N N 15 86.42 2.61 . . . . . . . 5995 7 7 . 1 1 13 13 GLU N N 15 73.51 1.16 . . . . . . . 5995 7 8 . 1 1 15 15 ILE N N 15 80.70 3.27 . . . . . . . 5995 7 9 . 1 1 16 16 ASN N N 15 68.57 1.93 . . . . . . . 5995 7 10 . 1 1 17 17 GLY N N 15 88.59 3.53 . . . . . . . 5995 7 11 . 1 1 21 21 THR N N 15 74.19 11.4 . . . . . . . 5995 7 12 . 1 1 22 22 ILE N N 15 78.33 3.64 . . . . . . . 5995 7 13 . 1 1 23 23 ILE N N 15 82.03 2.26 . . . . . . . 5995 7 14 . 1 1 26 26 SER N N 15 46.23 3.27 . . . . . . . 5995 7 15 . 1 1 27 27 ASP N N 15 91.43 4.28 . . . . . . . 5995 7 16 . 1 1 30 30 GLU N N 15 86.02 4.16 . . . . . . . 5995 7 17 . 1 1 31 31 LYS N N 15 78.73 3.52 . . . . . . . 5995 7 18 . 1 1 32 32 ILE N N 15 86.61 6.07 . . . . . . . 5995 7 19 . 1 1 33 33 GLU N N 15 85.28 3.29 . . . . . . . 5995 7 20 . 1 1 36 36 GLY N N 15 89.27 2.81 . . . . . . . 5995 7 21 . 1 1 37 37 ASN N N 15 84.40 4.39 . . . . . . . 5995 7 22 . 1 1 39 39 ARG N N 15 77.37 4.22 . . . . . . . 5995 7 23 . 1 1 40 40 LEU N N 15 56.19 3.42 . . . . . . . 5995 7 24 . 1 1 42 42 LEU N N 15 61.16 3.36 . . . . . . . 5995 7 25 . 1 1 47 47 VAL N N 15 87.86 3.43 . . . . . . . 5995 7 26 . 1 1 48 48 LEU N N 15 88.31 2.12 . . . . . . . 5995 7 27 . 1 1 51 51 SER N N 15 94.27 4.52 . . . . . . . 5995 7 28 . 1 1 52 52 LEU N N 15 83.87 3.67 . . . . . . . 5995 7 29 . 1 1 54 54 LEU N N 15 85.01 3.61 . . . . . . . 5995 7 30 . 1 1 57 57 HIS N N 15 75.36 6.40 . . . . . . . 5995 7 31 . 1 1 60 60 ARG N N 15 89.19 7.16 . . . . . . . 5995 7 32 . 1 1 64 64 CYS N N 15 85.71 3.54 . . . . . . . 5995 7 33 . 1 1 65 65 SER N N 15 92.98 4.00 . . . . . . . 5995 7 34 . 1 1 66 66 GLU N N 15 85.04 3.09 . . . . . . . 5995 7 35 . 1 1 67 67 LEU N N 15 81.31 2.86 . . . . . . . 5995 7 36 . 1 1 68 68 SER N N 15 83.20 3.23 . . . . . . . 5995 7 37 . 1 1 69 69 MET N N 15 82.86 3.64 . . . . . . . 5995 7 38 . 1 1 71 71 ALA N N 15 86.32 5.61 . . . . . . . 5995 7 39 . 1 1 72 72 ASP N N 15 77.63 3.99 . . . . . . . 5995 7 40 . 1 1 74 74 THR N N 15 93.57 4.04 . . . . . . . 5995 7 41 . 1 1 77 77 ALA N N 15 91.76 3.23 . . . . . . . 5995 7 42 . 1 1 79 79 GLU N N 15 80.89 3.85 . . . . . . . 5995 7 43 . 1 1 80 80 TYR N N 15 92.51 12.7 . . . . . . . 5995 7 44 . 1 1 81 81 SER N N 15 85.04 3.38 . . . . . . . 5995 7 45 . 1 1 86 86 GLY N N 15 82.29 3.39 . . . . . . . 5995 7 46 . 1 1 88 88 ASN N N 15 84.34 2.17 . . . . . . . 5995 7 47 . 1 1 89 89 THR N N 15 79.14 4.43 . . . . . . . 5995 7 48 . 1 1 91 91 THR N N 15 51.85 3.59 . . . . . . . 5995 7 49 . 1 1 92 92 ILE N N 15 74.87 4.47 . . . . . . . 5995 7 50 . 1 1 94 94 LYS N N 15 81.8 3.72 . . . . . . . 5995 7 51 . 1 1 95 95 THR N N 15 78.90 4.02 . . . . . . . 5995 7 52 . 1 1 96 96 ASP N N 15 73.01 0.14 . . . . . . . 5995 7 53 . 1 1 97 97 TYR N N 15 88.02 2.45 . . . . . . . 5995 7 54 . 1 1 100 100 PHE N N 15 63.84 3.49 . . . . . . . 5995 7 55 . 1 1 101 101 LEU N N 15 79.79 4.69 . . . . . . . 5995 7 56 . 1 1 102 102 MET N N 15 82.12 2.68 . . . . . . . 5995 7 57 . 1 1 103 103 ALA N N 15 77.07 1.02 . . . . . . . 5995 7 58 . 1 1 104 104 HIS N N 15 84.96 4.98 . . . . . . . 5995 7 59 . 1 1 105 105 LEU N N 15 73.10 3.60 . . . . . . . 5995 7 60 . 1 1 107 107 ASN N N 15 79.76 3.60 . . . . . . . 5995 7 61 . 1 1 108 108 GLU N N 15 58.54 3.06 . . . . . . . 5995 7 62 . 1 1 111 111 GLY N N 15 95.31 9.55 . . . . . . . 5995 7 63 . 1 1 113 113 THR N N 15 79.45 2.82 . . . . . . . 5995 7 64 . 1 1 115 115 GLN N N 15 84.27 3.30 . . . . . . . 5995 7 65 . 1 1 116 116 LEU N N 15 81.96 2.50 . . . . . . . 5995 7 66 . 1 1 117 117 MET N N 15 81.22 4.00 . . . . . . . 5995 7 67 . 1 1 118 118 GLY N N 15 83.06 3.15 . . . . . . . 5995 7 68 . 1 1 121 121 GLY N N 15 84.43 3.20 . . . . . . . 5995 7 69 . 1 1 123 123 GLU N N 15 81.97 4.29 . . . . . . . 5995 7 70 . 1 1 125 125 ASP N N 15 79.18 2.61 . . . . . . . 5995 7 71 . 1 1 126 126 LEU N N 15 85.89 3.32 . . . . . . . 5995 7 72 . 1 1 127 127 SER N N 15 91.48 3.58 . . . . . . . 5995 7 73 . 1 1 129 129 ASP N N 15 80.70 3.70 . . . . . . . 5995 7 74 . 1 1 130 130 ILE N N 15 84.37 3.44 . . . . . . . 5995 7 75 . 1 1 131 131 LYS N N 15 81.83 2.51 . . . . . . . 5995 7 76 . 1 1 133 133 ARG N N 15 84.14 2.90 . . . . . . . 5995 7 77 . 1 1 136 136 GLN N N 15 85.23 2.61 . . . . . . . 5995 7 78 . 1 1 137 137 LEU N N 15 85.25 3.09 . . . . . . . 5995 7 79 . 1 1 138 138 CYS N N 15 81.29 3.32 . . . . . . . 5995 7 80 . 1 1 140 140 LYS N N 15 83.43 2.87 . . . . . . . 5995 7 81 . 1 1 141 141 HIS N N 15 85.66 3.25 . . . . . . . 5995 7 82 . 1 1 142 142 GLY N N 15 90.41 2.92 . . . . . . . 5995 7 83 . 1 1 144 144 LEU N N 15 91.81 3.99 . . . . . . . 5995 7 84 . 1 1 145 145 ARG N N 15 88.81 2.57 . . . . . . . 5995 7 85 . 1 1 148 148 ILE N N 15 88.66 3.50 . . . . . . . 5995 7 86 . 1 1 151 151 LEU N N 15 81.23 6.13 . . . . . . . 5995 7 87 . 1 1 152 152 SER N N 15 84.18 3.20 . . . . . . . 5995 7 88 . 1 1 153 153 ASN N N 15 95.67 4.25 . . . . . . . 5995 7 89 . 1 1 155 155 ASN N N 15 72.05 1.46 . . . . . . . 5995 7 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_302_500_free_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 302_500_free_t2 _Heteronucl_T2_list.Entry_ID 5995 _Heteronucl_T2_list.ID 8 _Heteronucl_T2_list.Sample_condition_list_ID 9 _Heteronucl_T2_list.Sample_condition_list_label $302K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 500 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5995 8 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ALA N N 15 99.22 4.66 . . . . . . . 5995 8 2 . 1 1 4 4 SER N N 15 98.25 6.56 . . . . . . . 5995 8 3 . 1 1 11 11 ASN N N 15 113.9 6.57 . . . . . . . 5995 8 4 . 1 1 12 12 VAL N N 15 94.84 4.84 . . . . . . . 5995 8 5 . 1 1 13 13 GLU N N 15 87.49 3.30 . . . . . . . 5995 8 6 . 1 1 16 16 ASN N N 15 84.76 3.29 . . . . . . . 5995 8 7 . 1 1 17 17 GLY N N 15 97.23 5.73 . . . . . . . 5995 8 8 . 1 1 19 19 TRP N N 15 75.38 2.94 . . . . . . . 5995 8 9 . 1 1 20 20 HIS N N 15 39.95 3.54 . . . . . . . 5995 8 10 . 1 1 21 21 THR N N 15 94.59 16.1 . . . . . . . 5995 8 11 . 1 1 22 22 ILE N N 15 102.1 4.64 . . . . . . . 5995 8 12 . 1 1 23 23 ILE N N 15 95.19 3.84 . . . . . . . 5995 8 13 . 1 1 26 26 SER N N 15 63.30 4.09 . . . . . . . 5995 8 14 . 1 1 27 27 ASP N N 15 98.38 5.91 . . . . . . . 5995 8 15 . 1 1 30 30 GLU N N 15 93.08 5.08 . . . . . . . 5995 8 16 . 1 1 31 31 LYS N N 15 88.20 3.80 . . . . . . . 5995 8 17 . 1 1 32 32 ILE N N 15 97.11 4.56 . . . . . . . 5995 8 18 . 1 1 33 33 GLU N N 15 99.13 4.53 . . . . . . . 5995 8 19 . 1 1 35 35 ASN N N 15 93.73 5.12 . . . . . . . 5995 8 20 . 1 1 36 36 GLY N N 15 100.1 5.26 . . . . . . . 5995 8 21 . 1 1 37 37 ASN N N 15 93.25 4.81 . . . . . . . 5995 8 22 . 1 1 39 39 ARG N N 15 89.86 4.81 . . . . . . . 5995 8 23 . 1 1 40 40 LEU N N 15 90.77 3.81 . . . . . . . 5995 8 24 . 1 1 41 41 PHE N N 15 68.31 1.70 . . . . . . . 5995 8 25 . 1 1 42 42 LEU N N 15 83.30 3.29 . . . . . . . 5995 8 26 . 1 1 48 48 LEU N N 15 96.35 2.87 . . . . . . . 5995 8 27 . 1 1 51 51 SER N N 15 104.1 5.53 . . . . . . . 5995 8 28 . 1 1 52 52 LEU N N 15 92.98 7.92 . . . . . . . 5995 8 29 . 1 1 54 54 LEU N N 15 95.67 3.06 . . . . . . . 5995 8 30 . 1 1 57 57 HIS N N 15 85.97 4.52 . . . . . . . 5995 8 31 . 1 1 58 58 THR N N 15 69.40 0.57 . . . . . . . 5995 8 32 . 1 1 60 60 ARG N N 15 96.82 4.96 . . . . . . . 5995 8 33 . 1 1 64 64 CYS N N 15 97.37 3.80 . . . . . . . 5995 8 34 . 1 1 65 65 SER N N 15 105.3 5.72 . . . . . . . 5995 8 35 . 1 1 66 66 GLU N N 15 81.65 6.12 . . . . . . . 5995 8 36 . 1 1 68 68 SER N N 15 102.9 3.17 . . . . . . . 5995 8 37 . 1 1 69 69 MET N N 15 92.22 3.99 . . . . . . . 5995 8 38 . 1 1 70 70 VAL N N 15 92.52 1.96 . . . . . . . 5995 8 39 . 1 1 71 71 ALA N N 15 98.89 5.42 . . . . . . . 5995 8 40 . 1 1 72 72 ASP N N 15 83.21 5.88 . . . . . . . 5995 8 41 . 1 1 74 74 THR N N 15 109.1 2.42 . . . . . . . 5995 8 42 . 1 1 76 76 LYS N N 15 94.66 4.24 . . . . . . . 5995 8 43 . 1 1 77 77 ALA N N 15 107.5 4.05 . . . . . . . 5995 8 44 . 1 1 79 79 GLU N N 15 92.63 3.86 . . . . . . . 5995 8 45 . 1 1 81 81 SER N N 15 93.29 3.34 . . . . . . . 5995 8 46 . 1 1 86 86 GLY N N 15 96.79 3.13 . . . . . . . 5995 8 47 . 1 1 88 88 ASN N N 15 96.31 4.17 . . . . . . . 5995 8 48 . 1 1 89 89 THR N N 15 88.67 7.81 . . . . . . . 5995 8 49 . 1 1 92 92 ILE N N 15 90.63 4.19 . . . . . . . 5995 8 50 . 1 1 94 94 LYS N N 15 90.82 5.24 . . . . . . . 5995 8 51 . 1 1 96 96 ASP N N 15 83.50 4.37 . . . . . . . 5995 8 52 . 1 1 97 97 TYR N N 15 84.17 3.84 . . . . . . . 5995 8 53 . 1 1 99 99 ASN N N 15 92.83 4.12 . . . . . . . 5995 8 54 . 1 1 100 100 PHE N N 15 86.41 3.60 . . . . . . . 5995 8 55 . 1 1 101 101 LEU N N 15 90.11 3.36 . . . . . . . 5995 8 56 . 1 1 102 102 MET N N 15 86.60 3.33 . . . . . . . 5995 8 57 . 1 1 103 103 ALA N N 15 91.66 5.11 . . . . . . . 5995 8 58 . 1 1 104 104 HIS N N 15 92.65 4.40 . . . . . . . 5995 8 59 . 1 1 105 105 LEU N N 15 86.39 4.86 . . . . . . . 5995 8 60 . 1 1 106 106 ILE N N 15 86.41 5.56 . . . . . . . 5995 8 61 . 1 1 107 107 ASN N N 15 93.88 3.66 . . . . . . . 5995 8 62 . 1 1 111 111 GLY N N 15 108.5 5.44 . . . . . . . 5995 8 63 . 1 1 113 113 THR N N 15 85.82 5.15 . . . . . . . 5995 8 64 . 1 1 115 115 GLN N N 15 98.81 3.37 . . . . . . . 5995 8 65 . 1 1 116 116 LEU N N 15 96.10 4.08 . . . . . . . 5995 8 66 . 1 1 117 117 MET N N 15 91.06 4.29 . . . . . . . 5995 8 67 . 1 1 118 118 GLY N N 15 89.67 4.57 . . . . . . . 5995 8 68 . 1 1 120 120 TYR N N 15 84.10 4.16 . . . . . . . 5995 8 69 . 1 1 121 121 GLY N N 15 89.84 4.74 . . . . . . . 5995 8 70 . 1 1 123 123 GLU N N 15 90.11 6.08 . . . . . . . 5995 8 71 . 1 1 125 125 ASP N N 15 90.82 3.43 . . . . . . . 5995 8 72 . 1 1 126 126 LEU N N 15 99.89 5.74 . . . . . . . 5995 8 73 . 1 1 127 127 SER N N 15 102.1 5.86 . . . . . . . 5995 8 74 . 1 1 128 128 SER N N 15 63.67 3.74 . . . . . . . 5995 8 75 . 1 1 129 129 ASP N N 15 94.23 3.68 . . . . . . . 5995 8 76 . 1 1 130 130 ILE N N 15 93.91 4.74 . . . . . . . 5995 8 77 . 1 1 131 131 LYS N N 15 92.03 3.46 . . . . . . . 5995 8 78 . 1 1 133 133 ARG N N 15 90.89 3.24 . . . . . . . 5995 8 79 . 1 1 136 136 GLN N N 15 92.52 3.14 . . . . . . . 5995 8 80 . 1 1 137 137 LEU N N 15 92.99 4.60 . . . . . . . 5995 8 81 . 1 1 138 138 CYS N N 15 80.34 4.08 . . . . . . . 5995 8 82 . 1 1 140 140 LYS N N 15 93.13 3.41 . . . . . . . 5995 8 83 . 1 1 141 141 HIS N N 15 95.70 4.79 . . . . . . . 5995 8 84 . 1 1 142 142 GLY N N 15 96.09 3.93 . . . . . . . 5995 8 85 . 1 1 143 143 ILE N N 15 65.56 3.72 . . . . . . . 5995 8 86 . 1 1 144 144 LEU N N 15 103.0 4.37 . . . . . . . 5995 8 87 . 1 1 145 145 ARG N N 15 100.1 4.74 . . . . . . . 5995 8 88 . 1 1 148 148 ILE N N 15 97.43 3.66 . . . . . . . 5995 8 89 . 1 1 151 151 LEU N N 15 91.11 6.10 . . . . . . . 5995 8 90 . 1 1 153 153 ASN N N 15 100.6 5.02 . . . . . . . 5995 8 91 . 1 1 157 157 CYS N N 15 91.73 4.33 . . . . . . . 5995 8 stop_ save_