######################################## # Heteronuclear T2 relaxation values # ######################################## save_T2_list_1 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode T2_list_1 _Heteronucl_T2_list.Entry_ID 6758 _Heteronucl_T2_list.ID 1 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $conditions_1 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 599.7 _Heteronucl_T2_list.T2_coherence_type 'single quantum' _Heteronucl_T2_list.T2_val_units s _Heteronucl_T2_list.Rex_units s _Heteronucl_T2_list.Details ; 15N transverse T2 relaxation times were measured by the Carr-Purcell-Meiboom-Gill method (????????), using standard water flip-back methods [Grzesiek, S., and Bax, A. (1993) J. Am. Chem. Soc. 115, 12594.]. Spectra was recorded as 128 x 512 complex matrices, with spectral widths of 8385 (1H) and 2200 (15N) Hz, with 16 scans per FID. Relaxation delays collected were: 0.01, 0.03, 0.05, 0.07, 0.09, 0.11, 0.13, 0.15, 0.19, 0.21 s. Duplicate spectra were recorded for 0.01, 0.03 and 0.05 s to estimate the precision of peak intensities. ; _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 9 2D_1H-15N_HSQC_(T2_flag) 1 $sample_1 isotropic 6758 1 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 6758 1 2 $software_2 . . 6758 1 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 12 12 ASP N N 15 0.08807236 0.001711978 . . . . . . . 6758 1 2 . 1 1 13 13 LEU N N 15 0.089688512 0.002127892 . . . . . . . 6758 1 3 . 1 1 16 16 PHE N N 15 0.066338952 0.002519715 . . . . . . . 6758 1 4 . 1 1 17 17 ARG N N 15 0.066331912 0.001770815 . . . . . . . 6758 1 5 . 1 1 18 18 VAL N N 15 0.065505473 0.001707862 . . . . . . . 6758 1 6 . 1 1 19 19 ALA N N 15 0.067892811 0.000885818 . . . . . . . 6758 1 7 . 1 1 20 20 THR N N 15 0.07446959 0.001949123 . . . . . . . 6758 1 8 . 1 1 21 21 TRP N N 15 0.068281292 0.001245233 . . . . . . . 6758 1 9 . 1 1 23 23 LEU N N 15 0.166184731 0.005884923 . . . . . . . 6758 1 10 . 1 1 27 27 SER N N 15 0.060214121 0.001708451 . . . . . . . 6758 1 11 . 1 1 29 29 THR N N 15 0.079291452 0.000898438 . . . . . . . 6758 1 12 . 1 1 35 35 ASN N N 15 0.149637876 0.015087773 . . . . . . . 6758 1 13 . 1 1 36 36 ILE N N 15 0.307285745 0.029380585 . . . . . . . 6758 1 14 . 1 1 41 41 LEU N N 15 0.068901842 0.000880854 . . . . . . . 6758 1 15 . 1 1 42 42 ILE N N 15 0.080729797 0.002871758 . . . . . . . 6758 1 16 . 1 1 43 43 SER N N 15 0.070944628 0.001874264 . . . . . . . 6758 1 17 . 1 1 44 44 GLY N N 15 0.094982998 0.001812116 . . . . . . . 6758 1 18 . 1 1 45 45 GLU N N 15 0.081087217 0.002190597 . . . . . . . 6758 1 19 . 1 1 46 46 ASN N N 15 0.081977964 0.003351364 . . . . . . . 6758 1 20 . 1 1 47 47 ALA N N 15 0.195805839 0.00750818 . . . . . . . 6758 1 21 . 1 1 49 49 ASP N N 15 0.063706441 0.003212734 . . . . . . . 6758 1 22 . 1 1 50 50 ILE N N 15 0.070869713 0.001960847 . . . . . . . 6758 1 23 . 1 1 51 51 LEU N N 15 0.078386492 0.001311929 . . . . . . . 6758 1 24 . 1 1 52 52 ALA N N 15 0.186015365 0.00782065 . . . . . . . 6758 1 25 . 1 1 53 53 VAL N N 15 0.092935939 0.00193262 . . . . . . . 6758 1 26 . 1 1 55 55 GLU N N 15 0.069431908 0.0012185 . . . . . . . 6758 1 27 . 1 1 56 56 ALA N N 15 0.072778085 0.001709811 . . . . . . . 6758 1 28 . 1 1 62 62 THR N N 15 0.075640104 0.001886487 . . . . . . . 6758 1 29 . 1 1 63 63 ALA N N 15 0.070589564 0.001545415 . . . . . . . 6758 1 30 . 1 1 64 64 VAL N N 15 0.07160195 0.001120562 . . . . . . . 6758 1 31 . 1 1 65 65 ASP N N 15 0.069315441 0.001373922 . . . . . . . 6758 1 32 . 1 1 66 66 THR N N 15 0.070383874 0.002042632 . . . . . . . 6758 1 33 . 1 1 67 67 GLY N N 15 0.066601841 0.002720808 . . . . . . . 6758 1 34 . 1 1 68 68 ARG N N 15 0.071415309 0.000976068 . . . . . . . 6758 1 35 . 1 1 69 69 VAL N N 15 0.070678871 0.001465476 . . . . . . . 6758 1 36 . 1 1 70 70 ILE N N 15 0.072137581 0.00127739 . . . . . . . 6758 1 37 . 1 1 72 72 SER N N 15 0.055565434 0.000409624 . . . . . . . 6758 1 38 . 1 1 74 74 GLY N N 15 0.104101603 0.001846313 . . . . . . . 6758 1 39 . 1 1 75 75 ILE N N 15 0.057685763 0.000943256 . . . . . . . 6758 1 40 . 1 1 78 78 ARG N N 15 0.074584008 0.001554839 . . . . . . . 6758 1 41 . 1 1 79 79 GLU N N 15 0.07181999 0.002603599 . . . . . . . 6758 1 42 . 1 1 80 80 LEU N N 15 0.06652342 0.002934048 . . . . . . . 6758 1 43 . 1 1 81 81 ILE N N 15 0.196463654 0.036305602 . . . . . . . 6758 1 44 . 1 1 84 84 LEU N N 15 0.082231432 0.002412471 . . . . . . . 6758 1 45 . 1 1 85 85 SER N N 15 0.124183494 0.004347907 . . . . . . . 6758 1 46 . 1 1 86 86 THR N N 15 0.093116806 0.002457164 . . . . . . . 6758 1 47 . 1 1 89 89 ARG N N 15 0.106564365 0.001881391 . . . . . . . 6758 1 48 . 1 1 91 91 GLN N N 15 0.100687697 0.00176817 . . . . . . . 6758 1 49 . 1 1 92 92 GLN N N 15 0.077987304 0.001375886 . . . . . . . 6758 1 50 . 1 1 96 96 TYR N N 15 0.063358909 0.00308804 . . . . . . . 6758 1 51 . 1 1 100 100 VAL N N 15 0.086428929 0.002350268 . . . . . . . 6758 1 52 . 1 1 101 101 ASP N N 15 0.065453593 0.006084329 . . . . . . . 6758 1 53 . 1 1 103 103 LEU N N 15 0.106884426 0.000837049 . . . . . . . 6758 1 54 . 1 1 104 104 GLY N N 15 0.067407702 0.001924078 . . . . . . . 6758 1 55 . 1 1 105 105 GLY N N 15 0.103942541 0.005449894 . . . . . . . 6758 1 56 . 1 1 107 107 VAL N N 15 0.073850335 0.001359123 . . . . . . . 6758 1 57 . 1 1 111 111 LEU N N 15 0.072835864 0.003697481 . . . . . . . 6758 1 58 . 1 1 112 112 VAL N N 15 0.095336155 0.00309001 . . . . . . . 6758 1 59 . 1 1 113 113 SER N N 15 0.069980475 0.002279603 . . . . . . . 6758 1 60 . 1 1 114 114 ASN N N 15 0.064511551 0.004770274 . . . . . . . 6758 1 61 . 1 1 116 116 ARG N N 15 0.068900418 0.001005209 . . . . . . . 6758 1 62 . 1 1 117 117 ALA N N 15 0.125903357 0.006375275 . . . . . . . 6758 1 63 . 1 1 118 118 ASP N N 15 0.06622999 0.001528951 . . . . . . . 6758 1 64 . 1 1 119 119 GLU N N 15 0.074082305 0.001572105 . . . . . . . 6758 1 65 . 1 1 120 120 VAL N N 15 0.082444309 0.000994018 . . . . . . . 6758 1 66 . 1 1 121 121 PHE N N 15 0.07090338 0.001532044 . . . . . . . 6758 1 67 . 1 1 122 122 VAL N N 15 0.077364651 0.000757298 . . . . . . . 6758 1 68 . 1 1 123 123 LEU N N 15 0.069618975 0.001707701 . . . . . . . 6758 1 69 . 1 1 124 124 SER N N 15 0.080119217 0.00176544 . . . . . . . 6758 1 70 . 1 1 126 126 VAL N N 15 0.074614616 0.001684569 . . . . . . . 6758 1 71 . 1 1 127 127 ARG N N 15 0.066545111 0.001162447 . . . . . . . 6758 1 72 . 1 1 128 128 GLN N N 15 0.078883016 0.001482163 . . . . . . . 6758 1 73 . 1 1 129 129 GLY N N 15 0.066778409 0.000803771 . . . . . . . 6758 1 74 . 1 1 130 130 GLY N N 15 0.082878881 0.001979067 . . . . . . . 6758 1 75 . 1 1 131 131 ARG N N 15 0.069640793 0.002252001 . . . . . . . 6758 1 76 . 1 1 133 133 LEU N N 15 0.070157222 0.001264717 . . . . . . . 6758 1 77 . 1 1 134 134 LEU N N 15 0.077332942 0.001652881 . . . . . . . 6758 1 78 . 1 1 135 135 GLY N N 15 0.062151177 0.003194634 . . . . . . . 6758 1 79 . 1 1 136 136 ILE N N 15 0.068194682 0.001744191 . . . . . . . 6758 1 80 . 1 1 138 138 ILE N N 15 0.069145773 0.001233147 . . . . . . . 6758 1 81 . 1 1 139 139 GLY N N 15 0.067605939 0.002082901 . . . . . . . 6758 1 82 . 1 1 140 140 ASN N N 15 0.07182257 0.001472406 . . . . . . . 6758 1 83 . 1 1 142 142 ALA N N 15 0.072631136 0.00147972 . . . . . . . 6758 1 84 . 1 1 143 143 PHE N N 15 0.070322004 0.002780617 . . . . . . . 6758 1 85 . 1 1 144 144 PHE N N 15 0.066723604 0.00295164 . . . . . . . 6758 1 86 . 1 1 145 145 THR N N 15 0.069071268 0.001997392 . . . . . . . 6758 1 87 . 1 1 146 146 ALA N N 15 0.068603104 0.00078737 . . . . . . . 6758 1 88 . 1 1 147 147 HIS N N 15 0.067800287 0.004248417 . . . . . . . 6758 1 89 . 1 1 148 148 ALA N N 15 0.066515012 0.002592055 . . . . . . . 6758 1 90 . 1 1 149 149 ILE N N 15 0.064796636 0.001586354 . . . . . . . 6758 1 91 . 1 1 150 150 ALA N N 15 0.066637346 0.001527121 . . . . . . . 6758 1 92 . 1 1 151 151 MET N N 15 0.091343387 0.001914097 . . . . . . . 6758 1 93 . 1 1 152 152 ARG N N 15 0.075187405 0.003035986 . . . . . . . 6758 1 94 . 1 1 153 153 ASN N N 15 0.073246122 0.001060229 . . . . . . . 6758 1 95 . 1 1 154 154 ASN N N 15 0.075376695 0.000866643 . . . . . . . 6758 1 96 . 1 1 155 155 ASP N N 15 0.064421782 0.002259999 . . . . . . . 6758 1 97 . 1 1 156 156 ALA N N 15 0.06404878 0.000934812 . . . . . . . 6758 1 98 . 1 1 158 158 ALA N N 15 0.070451807 0.001056956 . . . . . . . 6758 1 99 . 1 1 159 159 LEU N N 15 0.070226199 0.000907675 . . . . . . . 6758 1 100 . 1 1 160 160 VAL N N 15 0.065396663 0.000607323 . . . . . . . 6758 1 101 . 1 1 161 161 GLU N N 15 0.066609826 0.001446088 . . . . . . . 6758 1 102 . 1 1 162 162 GLU N N 15 0.06772223 0.001312798 . . . . . . . 6758 1 103 . 1 1 163 163 VAL N N 15 0.065854028 0.001428045 . . . . . . . 6758 1 104 . 1 1 164 164 TYR N N 15 0.065474593 0.00131809 . . . . . . . 6758 1 105 . 1 1 165 165 ASN N N 15 0.062242084 0.001590827 . . . . . . . 6758 1 106 . 1 1 167 167 PHE N N 15 0.063548551 0.001373867 . . . . . . . 6758 1 107 . 1 1 168 168 ARG N N 15 0.065318066 0.001342379 . . . . . . . 6758 1 108 . 1 1 169 169 ASP N N 15 0.072719869 0.000982962 . . . . . . . 6758 1 109 . 1 1 170 170 SER N N 15 0.077939285 0.002045358 . . . . . . . 6758 1 110 . 1 1 171 171 ARG N N 15 0.074453511 0.001446665 . . . . . . . 6758 1 111 . 1 1 172 172 ASP N N 15 0.085752997 0.001186893 . . . . . . . 6758 1 112 . 1 1 174 174 VAL N N 15 0.073348737 0.001511649 . . . . . . . 6758 1 113 . 1 1 176 176 GLN N N 15 0.067717186 0.000931129 . . . . . . . 6758 1 114 . 1 1 177 177 ALA N N 15 0.068353167 0.001011797 . . . . . . . 6758 1 115 . 1 1 178 178 LEU N N 15 0.064877349 0.001370191 . . . . . . . 6758 1 116 . 1 1 179 179 ASN N N 15 0.069863626 0.001692724 . . . . . . . 6758 1 117 . 1 1 180 180 TRP N N 15 0.067193463 0.000652824 . . . . . . . 6758 1 118 . 1 1 181 181 MET N N 15 0.06791725 0.003028888 . . . . . . . 6758 1 119 . 1 1 182 182 ILE N N 15 0.075886928 0.002180131 . . . . . . . 6758 1 120 . 1 1 183 183 LEU N N 15 0.067835242 0.001086071 . . . . . . . 6758 1 121 . 1 1 184 184 GLY N N 15 0.0735186 0.001316575 . . . . . . . 6758 1 122 . 1 1 185 185 ASP N N 15 0.071723149 0.002649518 . . . . . . . 6758 1 123 . 1 1 186 186 PHE N N 15 0.076597831 0.001724812 . . . . . . . 6758 1 124 . 1 1 188 188 ARG N N 15 0.065019929 0.001280319 . . . . . . . 6758 1 125 . 1 1 189 189 GLU N N 15 0.069833378 0.001137432 . . . . . . . 6758 1 126 . 1 1 191 191 ALA N N 15 0.065537671 0.001267505 . . . . . . . 6758 1 127 . 1 1 192 192 ASP N N 15 0.06535606 0.001353301 . . . . . . . 6758 1 128 . 1 1 193 193 LEU N N 15 0.082922865 0.001975427 . . . . . . . 6758 1 129 . 1 1 194 194 GLU N N 15 0.069652434 0.001643222 . . . . . . . 6758 1 130 . 1 1 195 195 MET N N 15 0.07056416 0.00075692 . . . . . . . 6758 1 131 . 1 1 196 196 ASN N N 15 0.068739388 0.001047691 . . . . . . . 6758 1 132 . 1 1 198 198 THR N N 15 0.187938131 0.007286671 . . . . . . . 6758 1 133 . 1 1 199 199 VAL N N 15 0.178759765 0.019189481 . . . . . . . 6758 1 134 . 1 1 202 202 ARG N N 15 0.242494786 0.019690264 . . . . . . . 6758 1 135 . 1 1 203 203 ARG N N 15 0.155395326 0.011079894 . . . . . . . 6758 1 136 . 1 1 204 204 ALA N N 15 0.167492965 0.010382842 . . . . . . . 6758 1 137 . 1 1 205 205 SER N N 15 0.218727444 0.016223921 . . . . . . . 6758 1 138 . 1 1 206 206 GLU N N 15 0.203591351 0.009546463 . . . . . . . 6758 1 139 . 1 1 207 207 ILE N N 15 0.248855266 0.011839747 . . . . . . . 6758 1 140 . 1 1 208 208 ILE N N 15 0.254310564 0.021963057 . . . . . . . 6758 1 141 . 1 1 209 209 SER N N 15 0.160934709 0.01148503 . . . . . . . 6758 1 142 . 1 1 211 211 ALA N N 15 0.28534741 0.015088221 . . . . . . . 6758 1 143 . 1 1 213 213 ALA N N 15 0.26347684 0.015175596 . . . . . . . 6758 1 144 . 1 1 214 214 THR N N 15 0.329804426 0.027134466 . . . . . . . 6758 1 145 . 1 1 216 216 THR N N 15 0.151947973 0.012312281 . . . . . . . 6758 1 146 . 1 1 219 219 ARG N N 15 0.151745068 0.015848952 . . . . . . . 6758 1 147 . 1 1 222 222 ASP N N 15 0.058429645 0.001583198 . . . . . . . 6758 1 148 . 1 1 223 223 TYR N N 15 0.052924614 0.001117171 . . . . . . . 6758 1 149 . 1 1 224 224 ALA N N 15 0.06472073 0.00122928 . . . . . . . 6758 1 150 . 1 1 225 225 VAL N N 15 0.06717947 0.001078052 . . . . . . . 6758 1 151 . 1 1 226 226 ALA N N 15 0.068273833 0.001635704 . . . . . . . 6758 1 152 . 1 1 227 227 GLY N N 15 0.071447454 0.001065707 . . . . . . . 6758 1 153 . 1 1 228 228 ASN N N 15 0.067412246 0.001156518 . . . . . . . 6758 1 154 . 1 1 230 230 VAL N N 15 0.074338941 0.001755873 . . . . . . . 6758 1 155 . 1 1 231 231 ALA N N 15 0.076175966 0.002052931 . . . . . . . 6758 1 156 . 1 1 232 232 PHE N N 15 0.085596651 0.0016162 . . . . . . . 6758 1 157 . 1 1 233 233 ARG N N 15 0.071660958 0.000902717 . . . . . . . 6758 1 158 . 1 1 235 235 SER N N 15 0.08241713 0.00281765 . . . . . . . 6758 1 159 . 1 1 237 237 LEU N N 15 0.077232005 0.002039333 . . . . . . . 6758 1 160 . 1 1 238 238 GLN N N 15 0.067187594 0.002110554 . . . . . . . 6758 1 161 . 1 1 239 239 ALA N N 15 0.076793119 0.001427824 . . . . . . . 6758 1 162 . 1 1 240 240 GLY N N 15 0.065577641 0.00127577 . . . . . . . 6758 1 163 . 1 1 241 241 ILE N N 15 0.065997888 0.001229003 . . . . . . . 6758 1 164 . 1 1 242 242 VAL N N 15 0.074534532 0.002017562 . . . . . . . 6758 1 165 . 1 1 243 243 TYR N N 15 0.073553208 0.001469486 . . . . . . . 6758 1 166 . 1 1 244 244 GLY N N 15 0.073696312 0.001063335 . . . . . . . 6758 1 167 . 1 1 246 246 ARG N N 15 0.102758025 0.002022041 . . . . . . . 6758 1 168 . 1 1 247 247 ARG N N 15 0.11003279 0.002849316 . . . . . . . 6758 1 169 . 1 1 248 248 THR N N 15 0.098531875 0.002056567 . . . . . . . 6758 1 170 . 1 1 249 249 GLN N N 15 0.095273483 0.001759256 . . . . . . . 6758 1 171 . 1 1 250 250 ILE N N 15 0.113897811 0.003217407 . . . . . . . 6758 1 172 . 1 1 251 251 SER N N 15 0.075640677 0.002881844 . . . . . . . 6758 1 173 . 1 1 252 252 SER N N 15 0.094182356 0.003627677 . . . . . . . 6758 1 174 . 1 1 255 255 PHE N N 15 0.088278395 0.007117786 . . . . . . . 6758 1 175 . 1 1 257 257 VAL N N 15 0.062168564 0.001330757 . . . . . . . 6758 1 176 . 1 1 258 258 GLY N N 15 0.067191206 0.001585531 . . . . . . . 6758 1 177 . 1 1 259 259 VAL N N 15 0.063625779 0.002472006 . . . . . . . 6758 1 178 . 1 1 260 260 SER N N 15 0.063666287 0.001709855 . . . . . . . 6758 1 179 . 1 1 261 261 ARG N N 15 0.070217816 0.001470883 . . . . . . . 6758 1 180 . 1 1 262 262 ARG N N 15 0.080624355 0.001353609 . . . . . . . 6758 1 stop_ save_