###################################
# Assigned chemical shift lists #
###################################
###################################################################
# Chemical Shift Ambiguity Index Value Definitions #
# #
# The values other than 1 are used for those atoms with different #
# chemical shifts that cannot be assigned to stereospecific atoms #
# or to specific residues or chains. #
# #
# Index Value Definition #
# #
# 1 Unique (including isolated methyl protons, #
# geminal atoms, and geminal methyl #
# groups with identical chemical shifts) #
# (e.g. ILE HD11, HD12, HD13 protons) #
# 2 Ambiguity of geminal atoms or geminal methyl #
# proton groups (e.g. ASP HB2 and HB3 #
# protons, LEU CD1 and CD2 carbons, or #
# LEU HD11, HD12, HD13 and HD21, HD22, #
# HD23 methyl protons) #
# 3 Aromatic atoms on opposite sides of #
# symmetrical rings (e.g. TYR HE1 and HE2 #
# protons) #
# 4 Intraresidue ambiguities (e.g. LYS HG and #
# HD protons or TRP HZ2 and HZ3 protons) #
# 5 Interresidue ambiguities (LYS 12 vs. LYS 27) #
# 6 Intermolecular ambiguities (e.g. ASP 31 CA #
# in monomer 1 and ASP 31 CA in monomer 2 #
# of an asymmetrical homodimer, duplex #
# DNA assignments, or other assignments #
# that may apply to atoms in one or more #
# molecule in the molecular assembly) #
# 9 Ambiguous, specific ambiguity not defined #
# #
###################################################################
save_chem_shift_list_1
_Assigned_chem_shift_list.Sf_category assigned_chemical_shifts
_Assigned_chem_shift_list.Sf_framecode chem_shift_list_1
_Assigned_chem_shift_list.Entry_ID 7278
_Assigned_chem_shift_list.ID 1
_Assigned_chem_shift_list.Sample_condition_list_ID 1
_Assigned_chem_shift_list.Sample_condition_list_label $conditions_1
_Assigned_chem_shift_list.Chem_shift_reference_ID 1
_Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_referencing
_Assigned_chem_shift_list.Chem_shift_1H_err .
_Assigned_chem_shift_list.Chem_shift_13C_err .
_Assigned_chem_shift_list.Chem_shift_15N_err .
_Assigned_chem_shift_list.Chem_shift_31P_err .
_Assigned_chem_shift_list.Chem_shift_2H_err .
_Assigned_chem_shift_list.Chem_shift_19F_err .
_Assigned_chem_shift_list.Error_derivation_method .
_Assigned_chem_shift_list.Details .
_Assigned_chem_shift_list.Text_data_format .
_Assigned_chem_shift_list.Text_data .
loop_
_Chem_shift_experiment.Experiment_ID
_Chem_shift_experiment.Experiment_name
_Chem_shift_experiment.Sample_ID
_Chem_shift_experiment.Sample_label
_Chem_shift_experiment.Sample_state
_Chem_shift_experiment.Entry_ID
_Chem_shift_experiment.Assigned_chem_shift_list_ID
1 '1H-15N HSQC' 1 $sample_1 isotropic 7278 1
2 HMQC-NOESY-HSQC 1 $sample_1 isotropic 7278 1
stop_
loop_
_Atom_chem_shift.ID
_Atom_chem_shift.Assembly_atom_ID
_Atom_chem_shift.Entity_assembly_ID
_Atom_chem_shift.Entity_ID
_Atom_chem_shift.Comp_index_ID
_Atom_chem_shift.Seq_ID
_Atom_chem_shift.Comp_ID
_Atom_chem_shift.Atom_ID
_Atom_chem_shift.Atom_type
_Atom_chem_shift.Atom_isotope_number
_Atom_chem_shift.Val
_Atom_chem_shift.Val_err
_Atom_chem_shift.Assign_fig_of_merit
_Atom_chem_shift.Ambiguity_code
_Atom_chem_shift.Occupancy
_Atom_chem_shift.Resonance_ID
_Atom_chem_shift.Auth_entity_assembly_ID
_Atom_chem_shift.Auth_asym_ID
_Atom_chem_shift.Auth_seq_ID
_Atom_chem_shift.Auth_comp_ID
_Atom_chem_shift.Auth_atom_ID
_Atom_chem_shift.Details
_Atom_chem_shift.Entry_ID
_Atom_chem_shift.Assigned_chem_shift_list_ID
1 . 1 1 2 2 LEU H H 1 8.698 0.01 . 1 . . . . 2 L HN . 7278 1
2 . 1 1 2 2 LEU N N 15 125.722 0.1 . 1 . . . . 2 L N . 7278 1
3 . 1 1 3 3 LYS H H 1 8.720 0.01 . 1 . . . . 3 K HN . 7278 1
4 . 1 1 3 3 LYS N N 15 124.362 0.1 . 1 . . . . 3 K N . 7278 1
5 . 1 1 4 4 GLN H H 1 8.300 0.01 . 1 . . . . 4 Q HN . 7278 1
6 . 1 1 4 4 GLN N N 15 123.183 0.1 . 1 . . . . 4 Q N . 7278 1
7 . 1 1 5 5 VAL H H 1 8.763 0.01 . 1 . . . . 5 V HN . 7278 1
8 . 1 1 5 5 VAL N N 15 122.661 0.1 . 1 . . . . 5 V N . 7278 1
9 . 1 1 6 6 GLU H H 1 8.627 0.01 . 1 . . . . 6 E HN . 7278 1
10 . 1 1 6 6 GLU N N 15 124.813 0.1 . 1 . . . . 6 E N . 7278 1
11 . 1 1 7 7 ILE H H 1 8.549 0.01 . 1 . . . . 7 I HN . 7278 1
12 . 1 1 7 7 ILE N N 15 122.330 0.1 . 1 . . . . 7 I N . 7278 1
13 . 1 1 8 8 PHE H H 1 9.190 0.01 . 1 . . . . 8 F HN . 7278 1
14 . 1 1 8 8 PHE N N 15 128.929 0.1 . 1 . . . . 8 F N . 7278 1
15 . 1 1 9 9 THR H H 1 8.102 0.01 . 1 . . . . 9 T HN . 7278 1
16 . 1 1 9 9 THR N N 15 110.369 0.1 . 1 . . . . 9 T N . 7278 1
17 . 1 1 10 10 ASP H H 1 9.072 0.01 . 1 . . . . 10 D HN . 7278 1
18 . 1 1 10 10 ASP N N 15 121.772 0.1 . 1 . . . . 10 D N . 7278 1
19 . 1 1 11 11 GLY H H 1 8.684 0.01 . 1 . . . . 11 G HN . 7278 1
20 . 1 1 11 11 GLY N N 15 107.621 0.1 . 1 . . . . 11 G N . 7278 1
21 . 1 1 12 12 SER H H 1 8.821 0.01 . 1 . . . . 12 S HN . 7278 1
22 . 1 1 12 12 SER N N 15 114.518 0.1 . 1 . . . . 12 S N . 7278 1
23 . 1 1 13 13 CYS H H 1 8.467 0.01 . 1 . . . . 13 C HN . 7278 1
24 . 1 1 13 13 CYS N N 15 123.754 0.1 . 1 . . . . 13 C N . 7278 1
25 . 1 1 14 14 LEU H H 1 9.047 0.01 . 1 . . . . 14 L HN . 7278 1
26 . 1 1 14 14 LEU N N 15 128.999 0.1 . 1 . . . . 14 L N . 7278 1
27 . 1 1 15 15 GLY H H 1 7.830 0.01 . 1 . . . . 15 G HN . 7278 1
28 . 1 1 15 15 GLY N N 15 108.403 0.1 . 1 . . . . 15 G N . 7278 1
29 . 1 1 18 18 GLY H H 1 8.308 0.01 . 1 . . . . 18 G HN . 7278 1
30 . 1 1 18 18 GLY N N 15 105.967 0.1 . 1 . . . . 18 G N . 7278 1
31 . 1 1 20 20 GLY H H 1 8.948 0.01 . 1 . . . . 20 G HN . 7278 1
32 . 1 1 20 20 GLY N N 15 108.908 0.1 . 1 . . . . 20 G N . 7278 1
33 . 1 1 21 21 GLY H H 1 9.051 0.01 . 1 . . . . 21 G HN . 7278 1
34 . 1 1 21 21 GLY N N 15 107.236 0.1 . 1 . . . . 21 G N . 7278 1
35 . 1 1 22 22 TYR H H 1 7.870 0.01 . 1 . . . . 22 Y HN . 7278 1
36 . 1 1 22 22 TYR N N 15 113.783 0.1 . 1 . . . . 22 Y N . 7278 1
37 . 1 1 23 23 GLY H H 1 9.034 0.01 . 1 . . . . 23 G HN . 7278 1
38 . 1 1 23 23 GLY N N 15 106.776 0.1 . 1 . . . . 23 G N . 7278 1
39 . 1 1 24 24 ALA H H 1 9.515 0.01 . 1 . . . . 24 A HN . 7278 1
40 . 1 1 24 24 ALA N N 15 126.729 0.1 . 1 . . . . 24 A N . 7278 1
41 . 1 1 25 25 ILE H H 1 9.120 0.01 . 1 . . . . 25 I HN . 7278 1
42 . 1 1 25 25 ILE N N 15 121.551 0.1 . 1 . . . . 25 I N . 7278 1
43 . 1 1 26 26 LEU H H 1 9.204 0.01 . 1 . . . . 26 L HN . 7278 1
44 . 1 1 26 26 LEU N N 15 129.527 0.1 . 1 . . . . 26 L N . 7278 1
45 . 1 1 27 27 ARG H H 1 9.894 0.01 . 1 . . . . 27 R HN . 7278 1
46 . 1 1 27 27 ARG N N 15 126.463 0.1 . 1 . . . . 27 R N . 7278 1
47 . 1 1 28 28 TYR H H 1 8.627 0.01 . 1 . . . . 28 Y HN . 7278 1
48 . 1 1 28 28 TYR N N 15 125.627 0.1 . 1 . . . . 28 Y N . 7278 1
49 . 1 1 29 29 ARG H H 1 9.334 0.01 . 1 . . . . 29 R HN . 7278 1
50 . 1 1 29 29 ARG N N 15 127.755 0.1 . 1 . . . . 29 R N . 7278 1
51 . 1 1 30 30 GLY H H 1 8.705 0.01 . 1 . . . . 30 G HN . 7278 1
52 . 1 1 30 30 GLY N N 15 105.675 0.1 . 1 . . . . 30 G N . 7278 1
53 . 1 1 31 31 ARG H H 1 7.995 0.01 . 1 . . . . 31 R HN . 7278 1
54 . 1 1 31 31 ARG N N 15 122.064 0.1 . 1 . . . . 31 R N . 7278 1
55 . 1 1 32 32 GLU H H 1 8.747 0.01 . 1 . . . . 32 E HN . 7278 1
56 . 1 1 32 32 GLU N N 15 123.276 0.1 . 1 . . . . 32 E N . 7278 1
57 . 1 1 33 33 LYS H H 1 9.217 0.01 . 1 . . . . 33 K HN . 7278 1
58 . 1 1 33 33 LYS N N 15 125.729 0.1 . 1 . . . . 33 K N . 7278 1
59 . 1 1 34 34 THR H H 1 8.128 0.01 . 1 . . . . 34 T HN . 7278 1
60 . 1 1 34 34 THR N N 15 115.580 0.1 . 1 . . . . 34 T N . 7278 1
61 . 1 1 35 35 PHE H H 1 9.347 0.01 . 1 . . . . 35 F HN . 7278 1
62 . 1 1 35 35 PHE N N 15 121.343 0.1 . 1 . . . . 35 F N . 7278 1
63 . 1 1 36 36 SER H H 1 8.397 0.01 . 1 . . . . 36 S HN . 7278 1
64 . 1 1 36 36 SER N N 15 114.521 0.1 . 1 . . . . 36 S N . 7278 1
65 . 1 1 37 37 ALA H H 1 6.370 0.01 . 1 . . . . 37 A HN . 7278 1
66 . 1 1 37 37 ALA N N 15 121.663 0.1 . 1 . . . . 37 A N . 7278 1
67 . 1 1 38 38 GLY H H 1 8.525 0.01 . 1 . . . . 38 G HN . 7278 1
68 . 1 1 38 38 GLY N N 15 106.773 0.1 . 1 . . . . 38 G N . 7278 1
69 . 1 1 39 39 TYR H H 1 9.695 0.01 . 1 . . . . 39 Y HN . 7278 1
70 . 1 1 39 39 TYR N N 15 123.573 0.1 . 1 . . . . 39 Y N . 7278 1
71 . 1 1 40 40 THR H H 1 8.822 0.01 . 1 . . . . 40 T HN . 7278 1
72 . 1 1 40 40 THR N N 15 114.178 0.1 . 1 . . . . 40 T N . 7278 1
73 . 1 1 41 41 ARG H H 1 7.754 0.01 . 1 . . . . 41 R HN . 7278 1
74 . 1 1 41 41 ARG N N 15 120.504 0.1 . 1 . . . . 41 R N . 7278 1
75 . 1 1 42 42 THR H H 1 8.853 0.01 . 1 . . . . 42 T HN . 7278 1
76 . 1 1 42 42 THR N N 15 125.720 0.1 . 1 . . . . 42 T N . 7278 1
77 . 1 1 43 43 THR H H 1 8.528 0.01 . 1 . . . . 43 T HN . 7278 1
78 . 1 1 43 43 THR N N 15 107.286 0.1 . 1 . . . . 43 T N . 7278 1
79 . 1 1 44 44 ASN H H 1 9.137 0.01 . 1 . . . . 44 N HN . 7278 1
80 . 1 1 44 44 ASN N N 15 121.199 0.1 . 1 . . . . 44 N N . 7278 1
81 . 1 1 45 45 ASN H H 1 8.584 0.01 . 1 . . . . 45 N HN . 7278 1
82 . 1 1 45 45 ASN N N 15 117.084 0.1 . 1 . . . . 45 N N . 7278 1
83 . 1 1 46 46 ARG H H 1 7.356 0.01 . 1 . . . . 46 R HN . 7278 1
84 . 1 1 46 46 ARG N N 15 116.820 0.1 . 1 . . . . 46 R N . 7278 1
85 . 1 1 47 47 MET H H 1 7.738 0.01 . 1 . . . . 47 M HN . 7278 1
86 . 1 1 47 47 MET N N 15 118.636 0.1 . 1 . . . . 47 M N . 7278 1
87 . 1 1 51 51 ALA H H 1 7.700 0.01 . 1 . . . . 51 A HN . 7278 1
88 . 1 1 51 51 ALA N N 15 117.626 0.1 . 1 . . . . 51 A N . 7278 1
89 . 1 1 52 52 ALA H H 1 6.443 0.01 . 1 . . . . 52 A HN . 7278 1
90 . 1 1 52 52 ALA N N 15 114.189 0.1 . 1 . . . . 52 A N . 7278 1
91 . 1 1 55 55 ALA H H 1 6.841 0.01 . 1 . . . . 55 A HN . 7278 1
92 . 1 1 55 55 ALA N N 15 119.995 0.1 . 1 . . . . 55 A N . 7278 1
93 . 1 1 58 58 ALA H H 1 7.083 0.01 . 1 . . . . 58 A HN . 7278 1
94 . 1 1 58 58 ALA N N 15 120.276 0.1 . 1 . . . . 58 A N . 7278 1
95 . 1 1 59 59 LEU H H 1 7.122 0.01 . 1 . . . . 59 L HN . 7278 1
96 . 1 1 59 59 LEU N N 15 118.611 0.1 . 1 . . . . 59 L N . 7278 1
97 . 1 1 60 60 LYS H H 1 8.548 0.01 . 1 . . . . 60 K HN . 7278 1
98 . 1 1 60 60 LYS N N 15 122.767 0.1 . 1 . . . . 60 K N . 7278 1
99 . 1 1 61 61 GLU H H 1 7.664 0.01 . 1 . . . . 61 E HN . 7278 1
100 . 1 1 61 61 GLU N N 15 117.382 0.1 . 1 . . . . 61 E N . 7278 1
101 . 1 1 62 62 HIS H H 1 8.417 0.01 . 1 . . . . 62 H HN . 7278 1
102 . 1 1 62 62 HIS N N 15 119.596 0.1 . 1 . . . . 62 H N . 7278 1
103 . 1 1 63 63 CYS H H 1 10.997 0.01 . 1 . . . . 63 C HN . 7278 1
104 . 1 1 63 63 CYS N N 15 126.965 0.1 . 1 . . . . 63 C N . 7278 1
105 . 1 1 64 64 GLU H H 1 8.692 0.01 . 1 . . . . 64 E HN . 7278 1
106 . 1 1 64 64 GLU N N 15 123.039 0.1 . 1 . . . . 64 E N . 7278 1
107 . 1 1 65 65 VAL H H 1 8.833 0.01 . 1 . . . . 65 V HN . 7278 1
108 . 1 1 65 65 VAL N N 15 126.072 0.1 . 1 . . . . 65 V N . 7278 1
109 . 1 1 67 67 LEU H H 1 8.624 0.01 . 1 . . . . 67 L HN . 7278 1
110 . 1 1 67 67 LEU N N 15 135.444 0.1 . 1 . . . . 67 L N . 7278 1
111 . 1 1 68 68 SER H H 1 8.775 0.01 . 1 . . . . 68 S HN . 7278 1
112 . 1 1 68 68 SER N N 15 121.622 0.1 . 1 . . . . 68 S N . 7278 1
113 . 1 1 69 69 THR H H 1 8.599 0.01 . 1 . . . . 69 T HN . 7278 1
114 . 1 1 69 69 THR N N 15 120.144 0.1 . 1 . . . . 69 T N . 7278 1
115 . 1 1 70 70 ASP H H 1 8.989 0.01 . 1 . . . . 70 D HN . 7278 1
116 . 1 1 70 70 ASP N N 15 129.384 0.1 . 1 . . . . 70 D N . 7278 1
117 . 1 1 71 71 SER H H 1 8.705 0.01 . 1 . . . . 71 S HN . 7278 1
118 . 1 1 71 71 SER N N 15 117.902 0.1 . 1 . . . . 71 S N . 7278 1
119 . 1 1 72 72 GLN H H 1 9.541 0.01 . 1 . . . . 72 Q HN . 7278 1
120 . 1 1 72 72 GLN N N 15 131.938 0.1 . 1 . . . . 72 Q N . 7278 1
121 . 1 1 73 73 TYR H H 1 9.004 0.01 . 1 . . . . 73 Y HN . 7278 1
122 . 1 1 73 73 TYR N N 15 124.882 0.1 . 1 . . . . 73 Y N . 7278 1
123 . 1 1 74 74 VAL H H 1 7.555 0.01 . 1 . . . . 74 V HN . 7278 1
124 . 1 1 74 74 VAL N N 15 116.743 0.1 . 1 . . . . 74 V N . 7278 1
125 . 1 1 75 75 ARG H H 1 6.905 0.01 . 1 . . . . 75 R HN . 7278 1
126 . 1 1 75 75 ARG N N 15 117.469 0.1 . 1 . . . . 75 R N . 7278 1
127 . 1 1 76 76 GLN H H 1 8.126 0.01 . 1 . . . . 76 Q HN . 7278 1
128 . 1 1 76 76 GLN N N 15 121.449 0.1 . 1 . . . . 76 Q N . 7278 1
129 . 1 1 77 77 GLY H H 1 7.181 0.01 . 1 . . . . 77 G HN . 7278 1
130 . 1 1 77 77 GLY N N 15 104.605 0.1 . 1 . . . . 77 G N . 7278 1
131 . 1 1 78 78 ILE H H 1 8.126 0.01 . 1 . . . . 78 I HN . 7278 1
132 . 1 1 78 78 ILE N N 15 120.774 0.1 . 1 . . . . 78 I N . 7278 1
133 . 1 1 79 79 THR H H 1 8.120 0.01 . 1 . . . . 79 T HN . 7278 1
134 . 1 1 79 79 THR N N 15 112.829 0.1 . 1 . . . . 79 T N . 7278 1
stop_
save_